• 한국응용과학기술학회지
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• 제32권2호
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• pp.240-247
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• 2015

석탄회를 NaOH로 용융시킨 후 수열 처리에 의하여 제올라이트 A를 합성하였다. NaOH/석탄회의 비, 용융 온도, $NaAlO_2$의 첨가량, 수열 처리 온도 및 시간이 생성된 제올라이트의 종류와 결정도에 미치는 영향에 대하여 연구하였다. 결정도가 높은 제올라이트의 생성에 필요한 최적의 NaOH/석탄회의 중량비는 1.2, 최적의 용융 온도는 $550^{\circ}C$이었다. 용융된 석탄회로부터 $Si^{4+}$ 와 $Al^{3+}$의 용출은 교반 시간의 영향을 받지 않았다. 생성된 제올라이트의 형태는 첨가한 $NaAlO_2$의 영향을 받는 것으로 나타났다. 적은 양의 $NaAlO_2$를 첨가하면 제올라이트 X가 생성되나 $NaAlO_2$의 양이 증가하면 단일상의 제올라이트 A가 생성되었다. 수열처리 시간과 온도가 증가하면 제올라이트 A는 hydroxysodalite로 변화 하였다. 승온 속도를 낮춰 반응 온도까지의 도달시간을 증가시키면 결정도가 좋은 제올라이트 A를 얻을 수 있었다.

• Fisheries and Aquatic Sciences
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• 제25권1호
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• pp.31-39
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• 2022

To clarify the factors influencing the physical properties of fish after heat treatments, we investigated changes in the properties of proteins in the dorsal ordinary and dark muscle of yellowtail (Seriola quinqueradiata) heated under different conditions commonly used for the purposes of food hygiene. High-temperature/short-time heating (85℃ for 90 s and 75℃ for 60 s) affected the protein solubility more than low-temperature/long-time heating (63℃ for 30 min). Sodium dodecyl sulphate-polyacrylamide gel electrophoresis and differential scanning calorimetry showed that low-temperature/long-time heating reduced the degree of actin denaturation in fish compared with that by other heating conditions. In addition, collagen solubility was enhanced with low-temperature/long-time heating. Therefore, these results suggest that differences in the degree of actin and collagen denaturation are responsible for the enhanced meat tenderness and diminished meat shrinkage, resulting from low-temperature/long-time heating.

• Korean Membrane Journal
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• 제7권1호
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• pp.19-27
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• 2005

PP hollow fiber membrane was hydrophilized by EVOH dip coating followed by low temperature plasma treatment and UV irradiation. EVOH coating attained high water flux without any prewetting but its stability did not guaranteed at high water permeation rate. At high water permeation rate, water flux declined gradually due to swelling and delamination of the EVOH coating layer causing pore blocking effect. However, plasma treatment reduces the swelling, which suppress delamination of the EVOH coating layer from PP support result in relieving the flux decline. Also, UV irradiation helped the crosslinking of the EVOH coating layer to enhance the performance at low water permeation rate. FT-IR and ESCA analyses reveal that EVOH dip coating performed homogeneously through not only membrane surface but also matrix. Thermogram of EVOH film modified plasma treatment and W irradiation show that crosslinking density of EVOH layer increased. Chemical modification by plasma treatment and UV irradiation stabilized the hydrophilic coating layer to increase the critical flux of the submerged membrane.

• 한국자원식물학회지
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• 제35권1호
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• pp.36-43
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• 2022

본 연구는 동아시아 특산식물 애기닥나무의 자원식물로서 활용을 위한 대량증식법 개발을 위해 실시하였다. 종자의 발아특성을 알아보기 위해 광·온도조건, GA₃ 처리, 저온층적처리를 실시하였다. 온도조건 실험에서 4, 15/6, 20/10, 25/15℃에서 발아율은 각각 0, 42.5, 44.4, 91.7%였다. 따라서 애기닥나무 종자의 발아 최적온도는 25/15℃였다. 온도조건에 따라 발아가 제한되었지만, GA₃ 처리를 통해 상대적으로 낮은 온도조건에서도 발아율을 높일 수 있었다. 저온층적처리를 통해 발아소요일수를 단축할 수 있었으며. 이를 통해 애기닥나무 종자를 conditional dormancy 유형으로 분류하였다. 본 연구결과를 통하여 적정 발아 온도조건은 25/15℃이며, 상대적으로 낮은 온도조건에서도 GA₃처리로 종자기반 대량증식이 가능하며, 향후 산업적인 활용에 도움이 될 것이라 판단된다.

• 한국의류산업학회지
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• 제19권5호
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• pp.646-652
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• 2017

In order to clarify an availability of water treatment for persimmon extract dyeing, effect of color developing by water treatment process on cotton fabrics dyed with persimmon extract was investigated. Dyed fabrics were dipped still water and circulation water in various temperature. Concerning water color developing, still water color developing and circulation water color developing have been examined, and the temperature of water has been apprehended to prepare an effective basis of water color development. The surface color based on circulation water color development displays low values of $a^{\ast}$ and $b^{\ast}$, and the range of the c value(Munsell chroma) is narrow and has the value of 2 to 3, thus displays the coloration of a dark tone. The effect of temperature in water color development was insignificant, due to the small difference in temperature from $20^{\circ}C$ to $40^{\circ}C$. At $80^{\circ}C$, remarkable color development manifested, which is evidence of the high influence of temperature. The effects of circulation were clear at low temperatures, and the effects of temperature highly manifested at high temperatures. Circulation water color development display great color development at all temperatures to allow industrial color development with the absence of sunlight, thereby having an effect of energy reduction and developing color in dark tones, however this also is a strength of persimmon extract concerning color diversification, and is judged to have great value of industrial and practical application.

• 한국표면공학회지
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• 제52권4호
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• pp.194-202
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• 2019

A systematic investigation was made on the influence of processing parameters such as gas composition and treatment temperature on the surface characteristics of hardened layers of low temperature plasma nitrided 316L Austenitic Stainless Steel. Various nitriding processes were conducted by changing temperature ($370^{\circ}C$ to $430^{\circ}C$) and changing $N_2$ percentage (10% to 25%) for 15 hours in the glow discharge environment of a gas mixture of $N_2$ and $H_2$ in a plasma nitriding system. In this process a constant pressure of 4 Torr was maintained. Increasing nitriding temperature from $370^{\circ}C$ to $430^{\circ}C$, increases the thickness of S phase layer and the surface hardness, and also makes an improvement in corrosion resistance, irrespective of nitrogen percent. On the other hand, increasing nitrogen percent from 10% to 25% at $430^{\circ}C$ decreases corrosion resistance although it increases the surface hardness and the thickness of S phase layer. Therefore, optimized condition was selected as nitriding temperature of $430^{\circ}C$ with 10% nitrogen, as at this condition, the treated sample showed better corrosion resistance. Moreover to further increase the thickness of S phase layer and surface hardness without compromising the corrosion behavior, further research was conducted by fixing the $N_2$ content at 10% with introducing various amount of $CH_4$ content from 0% to 5% in the nitriding atmosphere. The best treatment condition was determined as 10% $N_2$ and 5% $CH_4$ content at $430^{\circ}C$, where the thickness of S phase layer of about $17{\mu}m$ and a surface hardness of $980HV_{0.1}$ were obtained (before treatment $250HV_{0.1}$ hardness). This specimen also showed much higher pitting potential, i.e. better corrosion resistance, than specimens treated at different process conditions and the untreated one.

• 공업화학
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• 제32권1호
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• pp.83-90
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• 2021

본 연구에서는 저온 열처리 탄소의 물리·화학적 특성이 이차전지 음극재로서의 전기화학적 거동에 미치는 영향에 대하여 고찰하였다. 석유계 핏치의 코크스화를 위하여 600 ℃ 열처리를 수행하였으며 제조된 코크스는 700~1500 ℃로 탄화 온도를 달리하여 저온 열처리 탄소 음극재로 제조되었다. 탄소 음극재의 물리 화학적 특성은 N2 흡·탈착 등온선, X-ray diffraction (XRD), 라만 분광(Raman spectroscopy), 원소 분석 등을 통하여 확인하였으며,저온 열처리 탄소의 음극 특성은 반쪽 전지를 통한 용량, 초기 쿨롱 효율(ICE, initial Coulomb efficiency), 율속, 수명 등의 전기화학적 특성을 통하여 고찰하였다. 저온 열처리 탄소의 결정 구조는 1500 ℃ 이하에서 결정자의 크기와 진밀도가 증가하였으며 비표면적은 감소하였다. 저온 열처리 탄소의 물리화학적 특성 변화에 따라 음극재의 전기화학 특성이 변화하였는데 수명 특성은 H/C 원소 비, 초기 쿨롱 효율은 비표면적, 율속 특성은 진밀도의 특성에 기인하는 것으로 판단되었다.

• 열처리공학회지
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• 제3권4호
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• pp.41-52
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• 1990

This research has been performed in order to investigate the effect of prior deformation on the Ms temperature and reversed As of Fe-Ni alloy. The Ms temperature rose with increment of strain to 30% but lowered over 50%. It can be analysed that martensitic transformation was promoted by partial dislocation in low strain, but suppressed by dislocation cell structures in high strain. The As temperature was substantially increased with higher deformation to 20% but slowly above 50%. It may be caused that as the transition bands formed by deformation constrained shear strain, therefore austenitic transformation was hindered.

• 열처리공학회지
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• 제26권1호
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• pp.1-6
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• 2013

The B2-ordered NiAl has attracted much attention as one of the candidates as a next generation high temperature material, because it has a high melting temperature, a low specific gravity and an excellent high temperature oxidation resistance. However, the application of NiAl to structural materials needs the improvement of its brittleness at room temperature. The study was carried out on the relation between several properties of NiAl and some variation of Ni content within NiAl phase, which means deviations from the stoichiometric composition. The main results were as follows; (i) Good ductility was obtained at the testing temperature more than 1073 K irrespective of Ni content. (ii) Increasing Ni content offered preferable tensile properties. (iii) Every NiAl with varying Ni contents showed the superior oxidation resistance.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2004년도 추계학술발표대회 개요집
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• pp.43-45
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• 2004

Brazing between cemented carbides and steel for tool investigated by copper alloy brazing filler. Copper alloy filler was high liquidus temperature($990^{\circ}C$), therefor the shank(steel) occurred softening. Because brazing sample was necessary to heat treatment after brazing process. This experiment, influence of austenite time and purge temperature on heat treatment were investigated. As a result, these treatments obtained to high deflective strength In case of austenite time was short and purge temperature was low. Especially, nitride precipitated brazing layers was strongly influenced by the deflective strength.