• Title/Summary/Keyword: Low temperature treatment

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Characteristics of STS 304 Rolled Steel by High Temperature Low Cycle Fatigue (고온 저주기 피로에 의한 STS 304 압연강재의 특성연구)

  • Kim, C.H.;Park, Y.M.;Bae, M.K.;Shin, D.C.;Kim, D.W.;Kim, T.G.
    • Journal of the Korean Society for Heat Treatment
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    • v.32 no.1
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    • pp.12-16
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    • 2019
  • In this study, strain-controlled low cycle fatigue test for hot rolled STS304 steel was carried out at $400^{\circ}C$ and $600^{\circ}C$, respectively. High temperature fatigue test was done using an electric furnace attached on the hydraulic fatigue test machine. The results of this study show that STS304 hot rolled steel has excellent static strength and fatigue characteristics. The hysteresis loop at half life was obtained in order to calculate the elastic and plastic strain. Also, Relationship between strain amplitude and fatigue life was examined in order to predict the low cycle fatigue life of STS304 steel by Coffin-Manson equation.

Study on the Effect of Austenite Grain Size and Mn Content on Hardenability in Boron-added Low Carbon alloys Steels (보론 첨가 저탄소합금강에서 Mn함량과 오스테나이트 결정입도가 경화능에 미치는 영향에 관한 연구)

  • Huh, U.Y.;Rho, Y.S.;Choi, M.S.;Kim, Y.H.;Lee, S.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.3 no.4
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    • pp.23-40
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    • 1990
  • This study has been carried out to investigate into some effects of Mn content with varying amounts and austenite grain size on hardenability in boron-added Fe-C-Cr-Mo alloy systems. (1) Austenite grains have been found to hardly grow in the temperature range of $900^{\circ}C$ to $950^{\circ}C$, whereas they grow rapidly in the temperature range of $975^{\circ}C$ to $1100^{\circ}C$. (2) Austenite grain growth is considerably small with increasing holding time at a given austenitizing temperature and is, in particular, hardly found to occur at a temperature of $900^{\circ}C$. (3) The hardenability improves ramarkably as Mn content is increased at three different austenitizing temperatures $900^{\circ}C$, $1000^{\circ}C$ and $1100^{\circ}C$. (4) The maximum hardenability is obtained from steels A, B and C austenitized at the $900^{\circ}C$, although Mn content is varied in each specimen.

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An Experimental Study on Low Nox Combustor Performance at High Pressure and Temperature for 20kW Class Microturbines (20kW급 마이크로터빈용 저공해 연소기의 고압고온 성능실험 연구)

  • Yoon, JeongJung;Oh, Jongsik;Lee, Heonseok
    • 유체기계공업학회:학술대회논문집
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    • 2002.12a
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    • pp.183-190
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    • 2002
  • In order to reduce NOx emissions in the 20kw class microturbines under development, the low NOx characteristics, as being an application to the lean premixed combustion technology, have been investigated. The study has been conducted at the conditions of high temperature and pressure. Air from a compressor with the temperature of 500K to 650K and the pressure of 0.3bar gauge to 0.7bar gauge, was supplied to the combustor through an air preheat-treatment. Sampling exhaust gases were measured at the immediate exit of the combustor. for the effect of temperature on NO and CO emissions. though NOx was increased, CO was decreased with increasing inlet air temperature. With increasing inlet air pressure, NOx and CO were increased also. NOx was decreased, but CO was increased with increasing inlet air mass flow rate. The test has been performed on the equivalent ratios of 0.10 to 0.25 in a lean region. NOx was increased with increasing equivalent ratios, but CO was decreased as an influence of flame temperature. In the very lean region of the equivalent ratio below 0.12, CO was increased suddenly, due to instability. As the results of this study, NOx and CO are found to be reduced to the similar level at the same time when operated at optimal conditions.

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The effect of low temperature aging on the mechanical property & phase stability of Y-TZP ceramics

  • Kim, Hyung-Tae;Han, Jung-Suk;Yang, Jae-Ho;Lee, Jai-Bong;Kim, Sung-Hun
    • The Journal of Advanced Prosthodontics
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    • v.1 no.3
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    • pp.113-117
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    • 2009
  • STATEMENT OF PROBLEM. Recently Yttrium-stabilized tetragonal zirconia polycrystal (Y-TZP) has been introduced due to superior flexural strength and fracture toughness compared to other dental ceramic systems. Although zirconia has outstanding mechanical properties, the phenomenon of decrease in the life-time of zirconia resulted from degradation in flexural strength after low temperature aging has been reported. PURPOSE. The objective of this study was to investigate degradation of flexural strength of Y-TZP ceramics after various low temperature aging treatments and to evaluate the phase stability and micro-structural change after aging by using X-ray diffraction analysis and a scanning electron microscope (SEM). MATERIAL AND METHODS. Y-TZP blocks of Vita In-Ceram YZ (Vita Zahnfabrik, Bad $S\ddot{a}ckingen$, Germany) were prepared in 40 mm (length) $\times$ 4 mm (width) $\times$ 3 mm (height) samples. Specimens were artificially aged in distilled water by heat-treatment at a temperature of 75, 100, 125, 150, 175, 200, and $225^{\circ}C$ for 10 hours, in order to induce the phase transformation at the surface. To measure the mechanical property, the specimens were subjected to a four-point bending test using a universal testing machine (Instron model 3365; Instron, Canton, Mass, USA). In addition, X-ray diffraction analysis (DMAX 2500; Rigaku, Tokyo, Japan) and SEM (Hitachi s4700; Jeol Ltd, Tokyo, Japan) were performed to estimate the phase transformation. The statistical analysis was done using SAS 9.1.3 (SAS institute, USA). The flexural strength data of the experimental groups were analyzed by one-way analysis of variance and to detect statistically significant differences ($\alpha$= .05). RESULTS. The mean flexural strength of sintered Vita In-Ceram YZ without autoclaving was 798 MPa. When applied aging temperature at below $125^{\circ}C$ for 10 hours, the flexural strength of Vita In-Ceram YZ increased up to 1,161 MPa. However, at above $150^{\circ}C$, the flexural strength started to decrease. Although low temperature aging caused the tetragonal-to-monoclinic phase transformation related to temperature, the minimum flexural strength was above 700 MPa. CONCLUSION. The monoclinic phase started to appear after aging treatment above $100^{\circ}C$. With the higher aging temperature, the fraction of monoclinic phase increased. The ratio of monoclinic/tetragonal + monoclinic phase reached a plateau value, circa 75% above $175^{\circ}C$. The point of monoclinic concentration at which the flexural strength begins to decrease was between 12% and 54%.

Effect of flour and frying temperature on quality of Gaeseong-Juak(doughnut of waxy rice) (밀가루와 튀김온도가 개성주악의 품질에 미치는 영향)

  • 김명애
    • Korean journal of food and cookery science
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    • v.16 no.4
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    • pp.316-320
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    • 2000
  • This study was carried out to standardize the recipe of Gaeseong-Juak. The formation and quality of the Juak were investigated under different treatment conditions. 1. The high ratio of medium flour(20%) in the flour mixture resulted in poor swelling. 2. The flour mixture with 10% strong flour showed higher volume of Gaeseong-Juak compared with the 10% mixture of medium flour, but the score of sensory evaluation was low. 3. The addition of Makkoli in the dough did not give significant difference in the formation of Juak, but the sensory score was low. 4. The deep-frying temperature in the range of 150$\^{C}$ to 170$\^{C}$ allowed the greatest swelling of Gaeseong-Juak, but the highest quality score was obtained at 160$\^{C}$ treatment. Overall, the best preparation condition of Gaeseong-Juak was that the mixture of waxy rice flour with 10% medium flour was kneaded with Makkoli and fried at 160$\^{C}$.

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Low Temperature Debinding Process Using Oxygen Plasma for Flexible Printed Electronics

  • Lee, Young-In
    • Journal of Powder Materials
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    • v.19 no.5
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    • pp.343-347
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    • 2012
  • In this study, an oxygen plasma treatment was used as a low temperature debinding method to form a conductive copper feature on a flexible substrate using a direct printing process. To demonstrate this concept, conductive copper patterns were formed on polyimide films using a copper nanoparticle-based paste with polymeric binders and dispersing agents and a screen printing method. Thermal and oxygen plasma treatments were utilized to remove the polymeric vehicle before a sintering of copper nanoparticles. The effect of the debinding methods on the phase, microstructure and electrical conductivity of the screen-printed patterns was systematically investigated by FE-SEM, TGA, XRD and four-point probe analysis. The patterns formed using oxygen plasma debinding showed the well-developed microstructure and the superior electrical conductivity compared with those of using thermal debinding.

A Study of the Oxygen Plasma Treatment on the Serviceability of a Wool Fabric

  • Kan, C.W.;Chan, K.;Yuen, C.W.M.
    • Fibers and Polymers
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    • v.5 no.3
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    • pp.213-218
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    • 2004
  • Low temperature plasma (LTP) treatment using oxygen gas was applied to a wool fabric. The LTP treated wool fabric was tested with several methods: ASTM D5035-1995, ASTM D1424-1996, AATCC Test Method 99-2000, AATCC Test Method 61-2001 lA, AATCC Test Method 15-2002 and AATCC Test Method 8-2001 and the results were compared with the industrial requirements (ASTM D3780-02 and ASTM D4155-0l). The results revealed that the LTP treated wool fabric could fulfil the industrial requirements. The results of the investigation were discussed thoroughly in this paper.

Improvement of Printing Properties of PET Micro Filament Fabrics Using Low Temperature Plasma Technology(I) (저온 plasma 기술에 의한 PET 극세사직물의 날염성 개선(I))

  • 조규민;이종훈
    • Textile Coloration and Finishing
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    • v.7 no.1
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    • pp.1-9
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    • 1995
  • In order to improve dyeability of poly(ethylene terephthalate)(PET) micro filament fabrics, the effect of the prior oxygen low temperature plasma on the subsequent dyeing(deep dyeing, printing) was examined in various conditions. The apparent concentration of dyed PET micro filament fabrics was increased by $O_{2}$plasma treatment. Higher discharge power levels and higher reactor pressure values created more significant effect. The wettability was significantly increased by $O_{2}$ plasma treatment. Therefore, it is predicted that introducing hydrophilic group on the surface of material can improve the apparent concentration of PET micro filament fabrics.

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Isolation of Differentially Expressed Genes by Low Temperature Treatment in Winter Oilseed Rape (Brassica napus L. cv. Tammi)

  • Chun Jong-Un;Seo Dong-Joong;Bae Chang-Hyu
    • Korean Journal of Plant Resources
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    • v.19 no.3
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    • pp.440-446
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    • 2006
  • To investigate flowering related genes in winter-type oilseed rape (Brassica napus L. cv. Tammi), differentially expressed genes were isolated from leaves of the plant after low temperature treatment which is requirements for floral induction. As a result of suppression subtractive hybridization (SSH), 288 clones were randomly selected from SSH library. Using reverse Northern blot analysis, 150 of 288 clones were identified to be differentially expressed. Out of these 150 clones, 45 clones showed very high identities with the known genes. Four clones showed very high identities over 90% with metallothionein-like gene that is related to flowering-induced genes. Of these 4 clones, the cDNA clone, rfs-13, revealed high identity with meotallothionein-like protein in Arabidopsis thaliana (98%) and Brassica compestris (89%). Furthermore, gene expressed in immature flower stages was confirmed by Northern blot analysis.

Direct Observation on the Low Temperature Degradation Due to Surface Treatment in Y-TZP (Y-TZP에서 표면 처리에 따른 저온열화 거동의 직접적 관찰)

  • Chung, Tai-Joo;Kim, Hye-Sung
    • Journal of Powder Materials
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    • v.17 no.3
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    • pp.197-202
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    • 2010
  • Low temperature degradation behavior in yttria stabilized tetragonal zirconia polycrystal (Y-TZP) ceramics was microscopically observed from the phase contrast between monoclinic surface and tetragonal matrix. The degradation behavior was dependent on the surface treatment of sintered Y-TZP, even if the sintering history is same. In the mirror polished specimen, the monoclinic layer appeared in a uniform thickness from the surface. On the contrary, for the specimen with coarse scratch, the thickness of degraded surface was more than double especially from the coarse scratch. Since the scratch results in local deformation, the residual stress should be induced around the scratch. With the transformation from tetragonal to monoclinic, the volume expansion exerts a stress on a neighboring grains and promotes a successive phase transformation. Such a autocatalytic effect can be triggered from the part of coarse scratch.