• Title/Summary/Keyword: Low Temperature Vacuum drying

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A Study on the Development of the Producing Zone Type Marine Dryer (On Weight Reduction Rate and Temperature Variations) (산지형 수산 건조시스템 개발에 관한 연구 (무게 감소율과 온도변동을 중심으로))

  • Kim, Kyong-Suk;Mun, Soo-Beom;Lee, Choon-Wha;Choe, Soon-Yeol;Park, Moon-Kab;Kim, Kyung-Kum
    • Journal of Advanced Marine Engineering and Technology
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    • v.34 no.4
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    • pp.477-484
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    • 2010
  • The majority of currently domestic dried sea foods is holding sanitary safety on storage and distribution, a structural problem to be in quality serious to sun drying. This paper the productive times and the on-site operation that production is fixed are easy, and it have reported the experimental results that carried out on development of a drying system toward field which can keep the highest quality and economy.

Comparative Characterization of AFC Precipitated Using Vacuum Drying, Dilution Precipitation and Spray Drying (감압건조, 희석침전, 분무건조 방식으로 제조된 무회분석탄의 특성)

  • Kwon, Ho Jung;Choi, Ho Kyung;Jo, Wan Taek;Kim, Sang Do;Yoo, Ji Ho;Chun, Dong Hyuk;Rhim, Young Joon;Lim, Jeong Hwan;Lee, Si Hyun;Rhee, Young Woo
    • Korean Chemical Engineering Research
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    • v.54 no.2
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    • pp.234-238
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    • 2016
  • Solid ash-free coal (AFC) samples recovered from solvent-extracted solution by vacuum drying, dilution precipitation and spray drying methods were compared in terms of physical properties and chemical structure. AFC was prepared by using Kideco coal (Indonesian sub-bituminous coal) and polar N-methyl-2-pyrrolidone (NMP) solvent as raw materials. The physical properties of the AFCs were characterized with proximate, ultimate, and calorific value analysis. In analyzing the chemical structure, FTIR and NMR were used. the proximate analysis showed much reduced ash in the AFCs compared to parent raw coal. The FTIR result showed that the extraction solvent was not fully removed from the AFC prepared by vacuum drying. However, the solvent was not detected in the AFC recovered by using dilution precipitation. Dilution precipitation has advantages over the other two methods, since it can be done at relatively low temperature and separate ash-free coal from extraction solvent more effectively.

Hydrated Vanadium Pentoxide/Graphene Oxide Nanobelts for Enhanced Electrochemical Performance

  • Hyegyeong Hwang;Jinsung Kwak
    • Korean Journal of Materials Research
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    • v.34 no.8
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    • pp.387-394
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    • 2024
  • Transition metal oxide-based materials have mainly been studied as electrodes for energy storage devices designed to meet essential energy demands. Among transition metal oxide-based materials, hydrated vanadium pentoxide (V2O5·nH2O), a vanadium oxide material, has demonstrated great electrochemical performance in the electrodes of energy storage devices. Graphene oxide (GO), a carbon-based material with high surface area and high electrical conductivity, has been added to V2O5·nH2O to compensate for its low electrical conductivity and structural instability. Here, V2O5·nH2O/GO nanobelts are manufactured with water without adding acid to ensure that the GO is uniformly dispersed, using a microwave-assisted hydrothermal synthesis. The resulting V2O5·nH2O/GO nanobelts exhibited a high specific capacitance of 206 F/g and more stable cycling performance than V2O5·nH2O without GO. The drying conditions of the carbon paper electrodes also resulted in more stable cycling performance when conducted at high vacuum and high temperature, compared with low vacuum and room temperature conditions. The improvement in electrochemical performance due to the addition of GO and the drying conditions of carbon paper electrodes indicate their great potential value as electrodes in energy storage devices.

Preparation of Seasoned and Semi-dried Horse Mackerel by Cold Air Drying and Quality of Its Product during Partially Frozen Storage (냉풍건조에 의한 전갱이 조미 반건품(半乾品)의 제조 및 빙결점 동결 저장 중 품질안정성)

  • Yang, Seung-Taek
    • Korean Journal of Food Science and Technology
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    • v.29 no.5
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    • pp.925-931
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    • 1997
  • An attempt was made in this study to investigate the possibility of processing seasoned and semi-dried horse mackerel (Tracharus japonnicus) and to examine its keeping quality, by analyzing the factors such as water content, pH, volatile basic nitrogen, viable cell count, peroxide value, color value and sensory evaluation. For processing of the seasoned and semi-dried product, optimum conditions of drying temperature and drying time were $20^{\circ}C$ and 4 hr, respectively, under $50{\pm}5%$ of relative humidity and 2 m/sec of air blast speed. The shelf-life of the products, vacuum-packaging method in nylon/polyethylene/linear low density polyethylene $(0.015/0.045/0.04\;{\mu}m)$ film bag, was 42 days during storage at $-3{\pm}0.5^{\circ}C$, while that of unpackaged one was only 28 days.

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FRAPCON analysis of cladding performance during dry storage operations

  • Richmond, David J.;Geelhood, Kenneth J.
    • Nuclear Engineering and Technology
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    • v.50 no.2
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    • pp.306-312
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    • 2018
  • There is an increasing need in the United States and around the world to move used nuclear fuel from wet storage in fuel pools to dry storage in casks stored at independent spent fuel storage installations or interim storage sites. Under normal conditions, the Nuclear Regulatory Commission limits cladding temperature to $400^{\circ}C$ for high-burnup (>45 GWd/mtU) fuel, with higher temperatures allowed for low-burnup fuel. An analysis was conducted with FRAPCON-4.0 on three modern fuel designs with three representative used nuclear fuel storage temperature profiles that peaked at $400^{\circ}C$. Results were representative of the majority of US light water reactor fuel. They conservatively showed that hoop stress remains below 90 MPa at the licensing temperature limit. Results also show that the limiting case for hoop stress may not be at the highest rod internal pressure in all cases but will be related to the axial temperature and oxidation profiles of the rods at the end of life and in storage.

Selective Growth of Nanosphere Assisted Vertical Zinc Oxide Nanowires with Hydrothermal Method

  • Lee, Jin-Su;Nam, Sang-Hun;Yu, Jung-Hun;Yun, Sang-Ho;Boo, Jin-Hyo
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.08a
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    • pp.252.2-252.2
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    • 2013
  • ZnO nanostructures have a lot of interest for decades due to its varied applications such as light-emitting devices, power generators, solar cells, and sensing devices etc. To get the high performance of these devices, the factors of nanostructure geometry, spacing, and alignment are important. So, Patterning of vertically- aligned ZnO nanowires are currently attractive. However, many of ZnO nanowire or nanorod fabrication methods are needs high temperature, such vapor phase transport process, metal-organic chemical vapor deposition (MOCVD), metal-organic vapor phase epitaxy, thermal evaporation, pulse laser deposition and thermal chemical vapor deposition. While hydrothermal process has great advantages-low temperature (less than $100^{\circ}C$), simple steps, short time consuming, without catalyst, and relatively ease to control than as mentioned various methods. In this work, we investigate the dependence of ZnO nanowire alignment and morphology on si substrate using of nanosphere template with various precursor concentration and components via hydrothermal process. The brief experimental scheme is as follow. First synthesized ZnO seed solution was spun coated on to cleaned Si substrate, and then annealed $350^{\circ}C$ for 1h in the furnace. Second, 200nm sized close-packed nanospheres were formed on the seed layer-coated substrate by using of gas-liquid-solid interfacial self-assembly method and drying in vaccum desicator for about a day to enhance the adhesion between seed layer and nanospheres. After that, zinc oxide nanowires were synthesized using a low temperature hydrothermal method based on alkali solution. The specimens were immersed upside down in the autoclave bath to prevent some precipitates which formed and covered on the surface. The hydrothermal conditions such as growth temperature, growth time, solution concentration, and additives are variously performed to optimize the morphologies of nanowire. To characterize the crystal structure of seed layer and nanowires, morphology, and optical properties, X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), Raman spectroscopy, and photoluminescence (PL) studies were investigated.

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Improvement of Drainage at Wet Pulp Mold Process (습식 펄프몰드 생산공정의 탈수성 향상을 위한 연구)

  • Sung Yong Joo;Ryu Jeong-Yong;Kim Hyung Jin;Kim Tae Keun;Song Bong-Keun
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.36 no.3
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    • pp.52-59
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    • 2004
  • The greater Increase of the demand for environmental friendly materials especially for packaging industry leads to the larger interest in the reusable and recycable materials such as pulp mold. Although the pulp mold has great characteristics for packaging, some deficiency compared with other packaging material like EPS(Expandable Polystyrene) need to be overcome, for example, the relative higher cost. In this report, since the water drainage rate at the forming zone of a wet pulp mold process could have a great influence on the economical efficiency not only by increasing machine speed but also reducing the drying energy, the optimum ways for increasing drainage were investigated The mechanism of vacuum drainage In pulp mold forming was successfully evaluated by using RDA(Retention and Darinage Analyzer). Since the conditions of stock were greatly affected by the pulping time of low consistency pulper, the optimum pupling time was investigated with considerations of all stock preparation processes. The change of stock temperature and the addition of polyelectrolyte could improve the vacuum drainage rate. It was founded that the wire mesh types of mold former had a little influence on the retention because of the relatively mild vacuum drainage. However, the bigger size of dewatering hole showed better drainage rate and could reduce the plugging and con lamination of mold.

Synthesis of Cu-coated Ni-based Bulk Metallic Glass Powders by Gas Atomization and Spray Drying Process

  • Kim, Byoung-Kee;Kim, Yong-Jin;Kim, Jin-Chun
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.936-936
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    • 2006
  • Bulk amorphous materials have been intensively studied to apply for various advanced industry fields due to their high mechanical, chemical and electrical properties. These materials have been produced by several techniques such as mechanical alloying, melt spinning and gas atomization, etc. Among them, the atomization is the most potential technique for commercialization due to high cooling rate during solidification of the melt and mass productivity. However, the amorphous powders still have some limitations because of their low ductility and toughness. Therefore, intensive efforts have to be carried out to increase the ductility and toughness. In this study, the Ni-based amorphous powder was produced by the gas atomization process. And in order to increase the ductile toughness, ductile Cu phase was coated on the Ni amorphous powder by spray drying process. The characteristics of the as-synthesis powders have been examined and briefly mentioned. The master alloy with $Ni_{57}Zr_{20}Ti_{16}Si_2Sn_3$ was prepared by vacuum induction melting furnace with graphite crucible and mold. The atomization was conducted at $1450^{\circ}C$ under the vacuum of $10^{-2}$ torr. The gas pressure during atomization was varied from 35 to 50 bars. After making the Ni amorphous powders, the spray drying was processed to produce the Cu -coated Ni amorphous composite powder. The amorphous powder and Cu nitrate solution were mixed together with a small amount of binder and then it was sprayed at temperature of $130^{\circ}C$ and rotating speed of 15,000 R.P.M.

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Storage Stability of Freeze Dried Loach for Instant Choo-o-tang (즉석 추어탕을 냉동 건조미꾸라지의 저장성)

  • 류홍수;문숙임;이수정;문갑순
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.28 no.1
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    • pp.153-160
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    • 1999
  • Storage stability of boiled and freeze dried loach and antioxidative effect of Zanthoxylum schinifolium were studied to confirm the possibility in development of instant choo o tang(Korean traditional loach soup). Packaging and storage temperature did not cause a measurable change in in vitro protein digestibility and trypsin indigestible substrate within 45 days of storage but remarkable quality changes were occurred in all samples stored after 60 days. Vacuum packaging and low temperature storage(4 oC) had some effect in retarding protein quality deterioration due to delaying polyunsaturated fatty acid oxidation. Maximum peroxide value and TBA value were reached in 15 days, and there were a slow(TBA value) and rapid reduction(POV) after peaks were reached. In contrast, increasing brown pigment development and fluorescence intensity continued until 90 days of storage. Treatment of ethanolic extracts from Zanthoxylum schinifolium prior to freeze drying could protect against lipid oxidation of freeze dried loach products.

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Conservation for Wooden Objects and Lacquer Wares Excavated From Sinchang-dong, Gwangju (광주 신창동 저습지 유적 목제 및 칠기의 보존)

  • Kim, Soochul;Park, Youngman
    • Conservation Science in Museum
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    • v.7
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    • pp.43-51
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    • 2006
  • From the low swamp remains in Sinchang-dong, Gwangju, a number of wooden lacquerware along with various wooden artifacts were excavated. These excavated lacquerware have deteriorated and weak wooden parts and the lacquer layer come off from the wooden parts; they are very likely to peel off and crack. Therefore, we impregnated the lacquerware in PEG#4000 40% solution that was effective for vacuum freeze drying and finished freeze-drying below 0°…. We compared the weight of wood and lacquerware right after the freeze-drying with the weight after leaving them in a airtight space with 60% RH (relative humidity). The comparison results showed no change in weight; thereby we confirmed controlling the finishing temperature during freeze-drying could control the moisture in wood after drying and it could stabilize wood against the change in moisture in the atmosphere. according to the analysis of the lacquer fragment, the base layer was pasted on the wooden surface with mixed black pigment and the upper layer was pasted three or four times with the mixture of lacquer and black pigment; or it was pasted without the black base coating.