• 한국화재소방학회논문지
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• 제14권1호
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• pp.8-12
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• 2000

면화류의 열적특성을 조사하기 위하여 시차주사열량계(DSC, Differential Scanning Calorimeter) 및 열중량 분석기(TGA, Thermogravimetric Analysis)를 이용하여 온도에 따른 발열개시온도, 무게감량 등을 조사하였으며, 발화온도 측정방법 중 정온법을 이용하여 요오드가가 각기 다른 유지류에 침윤된 면화류의 발차거동을 조사하였다. 이때 발화온도 측정장치의 반응용기 내부로의 공기 기류의 존재 여부에 따른 발화거동을 함께 조사하였다. 연구결과 합성섬유의 분해온도 폭이 순면인 천연섬유에 비하여 다소 넓음을 알 수 있었다. 한편 발화개시온도의 경우 공기를 주입하지 않는 경우에는 유지의 침윤량 증가에 따라 두 시료 모두 상승하였으나, 공기를 주입하는 경우에는 유지의 침윤량 증가에 따라 상당히 낮아지고 있으며, 특히 건성유를 침윤시킨 경우에는 급속히 감소하고 있음을 확인할 수 있었다.

• 한국연소학회:학술대회논문집
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• 한국연소학회 2002년도 제25회 KOSCI SYMPOSIUM 논문집
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• pp.231-235
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• 2002

A theoretical and experimental study on the combustion process in a constant volume micro combustor is described. Unlike in a macro scale constant volume combustor, the heat loss to the wall plays a major role in flame propagation in a micro micro combustor. In order to analyze the effect of heat loss on combustion phenomena, pressure transition from ignition was measured. A number of cylindrical micro combustors with different diameter and depth were used for experiment to study the effect of length scales and shape factor. The diameter of combustor ranged from 7.5mm to 22.5 mm and the height of cylinder was from 1mm to 4mm. Initial pressure was also varied for the experiment. The diagnostic methods were severely limited due to the size of the apparatus and uncertainties of certain quantities to be measured in a small-scale environment. An analytical method to derive physical quantities that are essential for performance prediction from the pressure measurements is described.

• 대한본초학회지
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• 제20권4호
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• pp.133-140
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• 2005

Objectives : We have been used many herbal medicines after processing to improve the effect, decrease toxicity and side-effect, and change property. We have studied the physico-chemical change and HPLC pattern of Morindae Radix by means of processing method. Methods : This study was investigated the contents of loss on drying, residue on ignition, residue on acid insoluble ignition, 50% ethanol extract and HPLC pattern of Morindae Radix(Morinda officinalis How.) by processed and non-processed. We have conducted Morindae Radix and Damnacanthi Radix which is circulated in herbal medicine market by forgery. Processed Morindae Radix was prepared by heating of added to salt(SP), liquor(LP) and Glycyrrhizae Radix solution(GP) for 20-40 minutes. Results and Conclusions : From this analysis, we found that the content of 50% ethanol extract was increased by processing method. And we were detected distinguishable marker of processed and non-processed from Morindae Radix(Morinda officinalis How.) by HPLC pattern analysis.

• Journal of Ecology and Environment
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• 제45권1호
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• pp.17-23
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• 2021

Background: Montane wetlands are unique wetland ecosystems with distinct physicochemical characteristics, and Molinia japonica often makes dominant communities in montane wetlands in South Korea. In order to figure out the environmental characteristics of M. japonica habitats and the major factors for the growth of M. japonica, field surveys were conducted in five wetlands from September to October 2019. Also, soil was collected at every quadrats installed in surveyed wetlands to analyze the physicochemical features. Results: The relative coverage of M. japonica was higher in low latitude wetlands than in high latitude. Redundancy analysis showed that soil water content had the strongest effect on the growth of M. japonica (F = 23.0, p < 0.001). Soil water content, loss on ignition, and relative light intensity showed a high correlation with the density (R = 0.568, 0.550, 0.547, respectively, p < 0.01) and the coverage of M. japonica (R = 0.495, 0.385, 0.514, respectively, p < 0.01). Soil water content, loss on ignition, and pH were highly correlated with each other. Conclusions: Molinia japonica lives in acidic wetlands at high altitude in temperate zone of low latitude, with peat layer placed on the floor. Also, M. japonica prefers open spaces to secure enough light for photosynthesis. High shoot production of M. japonica resulted in adding new peat material in every year, and this layer enforces the environmental characteristics of M. japonica habitats. This study may provide insights for further understanding of the method how wetlands maintain acidic condition by itself in montane wetlands in temperate zone.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2000년도 봄 학술발표회 논문집
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• pp.159-162
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• 2000

The purpose of this study is to develope an accurate procedure for measuring the glass content of fly ash produced by bituminous coal to assist in predicting their behavior in concrete. Quantitative mineralogical compositions of fly ashes were obtained by internal standard method using powder X-ray diffraction analysis. In the X-ray diffraction method, the specimen and standard fluorite were cautiously mixed and pulverized to 22$\mu$m in wet process so as to avoid the prefered orientation of the crystal and microabsorption effect of X-ray. calibration curve were fitted for several references peaks of four phases:$\alpha$-quartz. mullite, magnetite, hematite. The amount of glass was calculated by subtracting the amount of crystal phase and loss on ignition from the total amount. Glass content determined with this method ranged from 66.7 to 75.wt%.

• 한국화재소방학회논문지
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• 제26권6호
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• pp.99-108
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• 2012

본 연구에서는 최근 빈번히 발생하고 있는 폐타이어의 가공 및 저장상황에서의 산화열에 의한 자연발화현상을 규명하기 위해 폐타이어 분쇄물에 대한 화재 재연실험과 가공 및 저장장소에서 수거한 화재 잔존물에 대한 면밀한 성분 분석 및 발화개시온도, 무게감량, 반응열 등을 분석하였다. 이를 위해 열축적이 용이한 폐타이어 분쇄물 2.5~15 mm 범위의 파쇄된 분쇄물을 대상으로 재연실험 및 DSC 및 TGA, DTA, DTG, GC/MS를 통한 열분석을 시행하여 자연발화의 가능성에 대한 과학적인 개연성을 부여하고자 하였다. 연구결과를 살펴보면 재연실험을 통하여 관찰한 결과 48시간 저장시에 온도의 급상승($178^{\circ}C$) 및 탄화현상, 연기발생이 관찰되었다. 또한 DTA, DTG 분석한 결과 $166.15^{\circ}C$에서 최초 중량감소가 일어나는 것으로 분석되었다. 아울러 DSC 및 TGA를 이용한 폐타이어 분쇄물 1(Unburnt)의 실험결과 $180^{\circ}C$ 부근에서 열분해를 시작하는 것으로 나타나 폐타이어의 발화 개시온도는 $160{\sim}180^{\circ}C$라고 말할 수 있다. 그리고 $305^{\circ}C$에서 최초 원료 무게의 10 % 중량감소가 있었고, 원료 무게의 50 % 중량감소는 $416^{\circ}C$로 분석되었다. 또한 GC/MS와 DSC를 이용한 산화성 및 자기반응성시험에 있어서는 1,3 cyclopentnadiene 등 산화성성분이 다량 검출되었지만 표준물질과 폐타이어 분쇄물과의 열분석실험결과 기준치 이하로 분석되어 자기반응성은 없는 것으로 분석되었다. 따라서 폐타이어의 산화열에 의한 자연발화현상을 방지하기 위해서는 분쇄시 열축적이 적거나 없는 냉동파쇄방식 등의 가공공정으로 전환유도를 고려해야하며 현재 파쇄 분쇄물을 대형 마대(500 kg)로 저장하는 방식에서, 마대를 소형화하여 분쇄물을 분산 저장하는 등의 방법으로 열축적을 방지해야한다.

• 한국세라믹학회지
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• 제23권3호
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• pp.35-43
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• 1986

The equilibrium dsorption of starch on activated alumina and kaolin was studied to provide the fundamental data for investigating the effect of polymer adsorption on the flocculation of solid particles. The new polymer adsor-ption model(PAH-FH) predicting the adsorption equilibria of polymers on the solid surface has been developed using the solution theory and the concepts of Gibbs dividing surface in conjunction with the Flory-Huggins eq-uation and the adsorption behaviors of polymers were examined by this model The accurate adsorption equilibrium data of starch on alumina and kaolin were determined within the tempera-ture range of 298-318K by the ignition loss method. Using these experimenta data the model developed in this study was evaluated. It was shown that this model could predict the adsorption isotherm more accura-tely than the Langmuir model as well as could describe the characteristics of the adsorption equilibria through model parameters.

• Computers and Concrete
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• 제7권1호
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• pp.17-38
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• 2010

This research aimed to investigate the influence of high-volume mineral admixtures (MAs), i.e., fly ash and slag, on the hydration characteristics and microstructures of cement pastes. Degree of cement hydration was quantified by the loss-on-ignition technique and degree of pozzolanic reaction was determined by a selective dissolution method. The influence of MAs on the pore structure of paste was measured by mercury intrusion porosimetry. The results showed that the hydration properties of the blended pastes were a function of water to binder ratio, cement replacement level by MAs, and curing age. Pastes containing fly ash exhibited strongly reduced early strength, especially for mix with 45% fly ash. Moreover, at a similar cement replacement level, slag incorporated cement paste showed higher degrees of cement hydration and pozzolanic reaction than that of fly ash incorporated cement paste. Thus, the present study demonstrates that high substitution rates of slag for cement result in better effects on the short- and long-term hydration properties of cement pastes.

• 항공우주기술
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• 제13권2호
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• pp.167-176
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• 2014

유로의 개폐를 위해 사용되는 파이로밸브는 가볍고 신뢰성이 높은 장점을 가진다. 미국에서는 하이드라진 추진제를 사용하는 일부 위성 유실의 원인을 착화기 연소 가스의 누설로 판단하였고, 블로우바이라 불리는 이러한 누설 문제를 방지하기 위하여 억지끼워맞춤을 하는 피스톤을 개발하고 추가적인 설계변경을 통하여 신뢰성을 향상하였다. 여기서는 미국에서 수행된 파이로밸브 연구에 대한 문헌조사를 AIAA Paper 위주로 수행하였다. 또한 파이로밸브의 일반적인 문제점과 개선방향, 성능비교평가 사례 등을 다루었다.

• 한국공작기계학회:학술대회논문집
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• 한국공작기계학회 1996년도 춘계학술대회 논문집
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• pp.72-78
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• 1996

Based on experimental analysis, the characteristics of pulsating pressure wave propagation is clarified by testing of 4-stroke gasoline engine. The pulsating pressure wave in exhaust system is generated gyulsating gas flow due the working of exhaust valve. The pulsating pressure wave is closely concerned to the loss of engine power according to back pressure and exhaust noise. It is difficult to exactly calculate pulsating pressure wave nonlinear effect. Therefore, in the first step for solving these problems, this paper contains experimental model and analysis method which are applied two-port network analysis. Also, it shows coherence function, frequency response function. back pressure, and gradient of temperature in exhaust system.