• Archives of Metallurgy and Materials
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• v.66 no.4
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• pp.1001-1005
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• 2021

Liquid Metal Extraction process using molten Mg was carried out to obtain Nd-Mg alloys from Nd based permanent magnets at 900℃ for 24 h. with a magnet to magnesium mass ratio of 1:10. Nd was successfully extracted from magnet into Mg resulting in ~4 wt.% Nd-Mg alloy. Nd was recovered from the obtained Nd-Mg alloys based on the difference in their vapor pressures using vacuum distillation. Vacuum distillation experiments were carried out at 800℃ under vacuum of 2.67 Pa at various times for the recovery of high purity Nd. Nd having a purity of more than 99% was recovered at distillation time of 120 min and above. The phase transformations of the Nd-Mg alloy during the process, from Mg₁₂Nd to α-Nd, were confirmed as per the phase diagram at different distillation times. Pure Nd was recovered as a result of two step recycling process; Liquid Metal Extraction followed by Vacuum Distillation.

• Journal of Advanced Marine Engineering and Technology
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• v.20 no.2
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• pp.92-92
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• 1996

Recently, with the rapid development in the oceanic systems such as the oceanic structures and vessel, there occurs much interest in the impingement erosion-corrosion. In this paper, Cu-metal was tested by using of erosion apparatus with water-jet type and was investigated under the behaviour of impingement erosion-corrosion according to various environmental conditions, and the properties of Cu-metal were evaluated through the measurement by weight loss, weight loss rate, protective efficiency. The results were compared with those obtained using Cu-metal applied to cathodic protection and Cu-alloys added to Zn or Al-metal. As a basis of those results, the best protective efficiencies could be taken as using cathodic protection method and Cu-alloy with Al & Zn material addings, and will be suggested as the fundamental data of the anti-impingement erosion-corrosion on Cu-metal of impeller material for oceanic centrifugal pump.

• Journal of Advanced Marine Engineering and Technology
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• v.20 no.2
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• pp.24-31
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• 1996

Recently, with the rapid development in the oceanic systems such as the oceanic structures and vessel, there occurs much interest in the impingement erosion-corrosion. In this paper, Cu-metal was tested by using of erosion apparatus with water-jet type and was investigated under the behaviour of impingement erosion-corrosion according to various environmental conditions, and the properties of Cu-metal were evaluated through the measurement by weight loss, weight loss rate, protective efficiency. The results were compared with those obtained using Cu-metal applied to cathodic protection and Cu-alloys added to Zn or Al-metal. As a basis of those results, the best protective efficiencies could be taken as using cathodic protection method and Cu-alloy with Al & Zn material addings, and will be suggested as the fundamental data of the anti-impingement erosion-corrosion on Cu-metal of impeller material for oceanic centrifugal pump.

• Journal of the Korean Society of Propulsion Engineers
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• v.17 no.6
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• pp.105-112
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• 2013

Turbopump is typically an assembly of rotors and casings, and there are a number of joints between them. Every joint should be leak-proof, so there is always a seal to accomplish the goal. Among various seals, metal seals are advantageous in that they are robust at high pressure, and at wide range of temperature. In this study, flange joints using conical seal made of stainless steel, solid flat metal seal made of copper and metal C seal made of Inconel 718 were structurally designed and analyzed, considering both initial tightening and operating conditions.

• Proceedings of the KSME Conference
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• 2007.05b
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• pp.2638-2641
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• 2007

The magnetohydrodynamic(MHD) pressure drop along a liquid sodium flow was measured in a rectangular duct under a transverse magnetic field. The test section was made of a 3 mm thick stainless steel SUS304 with a $74{\times}5mm^2$ rectangular flow channel. The range of experimental parameters was roughly B=0${\sim}$0.18T and U=0${\sim}$0.9m/s at around $200^{\circ}C$. The differential pressure was measured by a diaphragm seal-type pressure transmitter filled with a high temperature silicon oil within 0.1MPa. The experimental results show a similar pressure drop with the theoretical estimation according to a change of the flow velocity and the magnetic field.

• Journal of Welding and Joining
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• v.13 no.3
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• pp.125-133
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• 1995

Rene80 superalloy was liquid phase diffusion bonded by using pure boron (B) as an insert material. As a basic study for the possibility of practical application of this bonding method, hardness and high temperature tensile strength of the bonded joint and metallurgical analysis were investigated. As experimental results, hardness of the bonded joint was homogenized after bonding and the tensile strength at 1144K was obtained to 90% of that of base metal. But there were some problems to be improved also, that means the joint was hardened after bonding due to increase of B content and elongation was much lower than that of base metal. Flat area and (Mo, Cr, W) boride, which should be harmful for bonding strength, were observed on the fractured surface of the tensile tested specimen.

• Proceedings of the KIEE Conference
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• 2015.07a
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• pp.1235-1236
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• 2015

This paper reports hyperelastically stretchable strain gauges based on liquid metal (eutectic gallium-indium;EGaIn) and a platinum-catalyzed silicone elastomer ($Ecoflex^{TM}$). A custom liquidmetal patterning setup was operated to fabricate liquidmetal straingauge on flexible substrate. The printed strain gauges were tested under cyclic uniaxial stretching, twisting, even bending of human finger. By engineering the orientation of solid wires placed over two terminals of t he printed liquid metal resistor, we stably achieved the stretchability of ~800 % which is the highest value reported so far, to the best of our knowledge.

• Journal of Welding and Joining
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• v.11 no.1
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• pp.73-79
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• 1993

The phenomenon of metal transfer has been investigated for different transfer modes using a digital high speed motion analyzer and an arc shadow-graphing system based on a laser source and related optical system. It was observed that the pinch instability phenomenon did not occur for the globular transfer mode, since the liquid globule was then spherical rateher than a cylindrical liquid bar. On increasing the ratio of carbon dioxide to argon, the transition current from globular to spray transfer generally increased, but it is interesting that the transition was observed to occur at the lowest current in a 5% CO$_{2}$-95% argon gas mixture. For pure carbon dioxide and helium shielding gases, the drop frequency increased slowly with increasing current. At high currents or an argon based shielding gas, the length of liquid bar decreased as the carbon dioxide content increased. The acceleration of a droplet within the arc was determined using the gas drag force theory and was found to be greater than the experimental results.

• Bulletin of the Korean Chemical Society
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• v.26 no.6
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• pp.930-934
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• 2005

A chloroform membrane system containing a given mixture of benzylaza-12-crown-4 and oleic acid is introduced for the selective and efficient transport of $Pb^{2+}$ ion. The transport was capable of moving metal ions ‘up-hill’. In the presence of ${S_2O_3}^{2-}$ion as a suitable metal ion acceptor in the receiving phase, the amount of lead ion transport across the liquid membrane after 150 minutes is (95.0 ${\pm}$ 1.7)%. The selectivity and efficiency of lead transport from aqueous solution containing $Tl^+,\;Ag^+,\;Mg^{2+},\;Ca^{2+},\;Co^{2+},$ $Ni^{2+},\;Cu^{2+},\;Zn^{2+},\;Hg^{2+}$ and $Cd^{2+}$were investigated. In the presence of thiosulfate as a suitable masking agent in the source phase, the interfering effects of $Ag^+\;and\;Cu^{2+}$ were diminished drastically.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09a
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• pp.518-519
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• 2006

A connection between pulse-periodical laser radiation power and stability of liquid-metal contacts between powder particles during selective laser sintering (SLS) is determined based on analysis solving the problem of stability of liquid column in the gravity and capillary forces field. On the grounds of obtained relationships the optimization of pulse-periodical laser radiation power and SLS-process duration is realized, that allows to produce voluminous powder porous materials with pre-determined physical and mechanical properties and surface geometry. Results of metallographic investigations of powder porous materials of titanium powder produced with technological regimes calculated by means of obtained relationships are given in the work