• Bulletin of the Korean Chemical Society
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• v.25 no.4
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• pp.549-552
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• 2004

A sensitive, selective and rapid method has been developed for the determination of mercury based on the rapid reaction of mercury(II) with p-sulfobenzylidenethiorhodanine (SBDTR) and the solid phase extraction of the colored chelate with $C_{18}$ disks. In the presence of pH 3.5 sodium acetate-acetic acid buffer solution and Emulsifier-OP medium, SBDTR reacts with mercury(II) to form a red chelate of a molar ratio 1 : 2 (mercury to SBDTR). This chelate was prconcentrated by solid phase extraction with $C_{18}$ disks. An enrichment factor of 50 was achieved. The molar absorptivity of the chelate is $1.28{\times}10^5 L{\cdot}mol^{-1}{\cdot}cm^{-1}$ at 545 nm in measured solution. Beer's law is obeyed in the range of 0.01-3 ${\mu}$g/mL. The relative standard deviation for eleven replicates sample of 0.01 ${\mu}$g/mL is 1.65%. This method was applied to the determination of mercury in tobacco and tobacco additive with good results.

• ETRI Journal
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• v.24 no.2
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• pp.161-171
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• 2002

This paper proposes a novel decision feedback differential phase detection (DF-DPD) for M-ary DPSK. A conventional differential phase detection method for M-ary Differential Phase Shift Keying (DPSK) can simplify the receiver architecture. However, it possesses a poorer bit error rate (BER) performance than coherent detection because of the prior noisy phase sample. Multiple-symbol differential detection methods, such as maximum likelihood differential phase detection, Viterbi-DPD, and DF-DPD using L-1 previous detected symbols, have attempted to improve BER performance. As the detection length, L, increases, the BER performance of the DF-DPD improves but the complexity of the architecture increases dramatically. This paper proposes a simplified DF-DPD architecture replacing the conventional delay and additional architecture with an accumulator. The proposed architecture also improves BER performance by minimizing the current differential phase noise through the accumulation of previous differential phase noise samples. The simulation results show that the BER performance of the proposed architecture approaches that of a coherent detection with differential decoding.

• Proceedings of the KSRS Conference
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• 2000.04a
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• pp.96-101
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• 2000

SAR(Synthetic Aperture Radar) interferometry 기술은 co-registration, 정밀궤도 계산, phase unwrapping, 지형보정과 같은 기술로 구성되어있다. 구속화된 위상값을 절대 위상값으로 변환하는 과정인 phase unwrapping 기술은 정밀지형고도를 얻는데 있어서 핵심기술이다. 본 연구에서는 JERS-1 SAR 영상으로부터 interferogram을 구하고, 이로부터 추출된 위상정보를 이용하여 branch cut(Goldstein et. al, 1988), minimum discontinuity(Flynn, 1997) 그리고 minimum $L^p$-norm(Ghiglia and Romero, 1996)방법 적용결과에 대한 비교 분석을 실시하였다. Goldstein 알고리즘은 수행속동가 매우 빠르지만 residue를 연결한 branch cut에 의해 분활된 영역 내에서, 서로 다른 적분 경로로 인해 위상이 단절되었다. 영상내의 모든 화소에서 절대 위상을 구한 minimum discontinuity와 minimum $L^p$-norm 알고리즘 수행 결과는 상관관계가 0.995로 매우 유사하였는데, 가중된 불연속선의 합을 최소화하는 minimum discontinuity 알고리즘이 minimum $L^p$-norm에 비해 영상 일부 지역에서 발생하는 위상 오차를 전파시키지 않는다는 장점이 있다. Minimum $L^p$-norm 방법은 다른 두 방법과 달리 위상정보 내에 많은 잡음이 있더라도 적절한 해를 구할 수 있다는 장점이 있다. 각 방법은 대상 자료의 특성에 따라 효율성이 있으나 Flynn의 알고리즘이 지역적 특성과 무관하게 가장 효과적임을 알 수 있었다.

• Journal of Technologic Dentistry
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• v.28 no.1
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• pp.27-41
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• 2006

The physical property and phase transformation in a commercial dental casting high gold alloy was investigated as a function of ageing temperature and time using microvickers hardness tester, X-ray diffraction, optical and electron microscopy and EPMA analyser. 1. With increasing ageing time, the hardness of solution-treated gold alloys increased slowly at the initial stage of ageing treatment at an ageing temperature of $300{\sim}400^{\circ}C$, and it reached a maximum value of hardness at the medium stage. Finally, it decreased gradually during further ageing. The maximum value of hardness at was similar with that of the conventional materials and suitable for using as the crown & bridge. 2. During isothermal ageing at a temperature range of $300{\sim}400^{\circ}C$, three phases consisting of the Au-rich ${\alpha}_1$phase with a face-centered cubic structure, the Pt3Zn ${\alpha}_2$phase with an ordered AuCu3(L12) type(f.c.c.) and the Pt-rich ${\alpha}_3$phase with face-centered cubic structure in solution-treated gold alloys were transformed into different three phases consisting of the ${\alpha}_1$phase, the ${\alpha}_3$phase and the PtZn $\beta$phase with an ordered AuCu I(L10) type. 3. The hardening of gold alloys was attributed to the lattice strains of the matrix resulting from the transformation of the ${\alpha}_2$phase to the $\beta$phase. 4. The softening of gold alloys during over-ageing was attributed to the coarsening of the nodules consisting of the $\beta$phase and ${\alpha}_1$matrix.

• 한국생물공학회:학술대회논문집
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• 2002.04a
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• pp.121-125
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• 2002

Rhodococcus rhodochrous IGTSS (ATCC 5396S) can break organo sulfur compounds such as dibenzothiophene. Since the environment for biodesulfurization process is invariably hydrophobic, parameters in hydrophobic systems should be examined. For the model oil, hexadecane-containing 5.43mM dibenzothiophene, the volumetric desulfurization rate was decreased with the oil-to-aqueous phase ratio up to 50%. The rate declined sharply after 48h because the cell activity, which is refreshed by medium exchange, was lost. To supply the exhausted nutrients, medium exchange was performed. At 30% oil phase, most of DBT was removed by medium exchange on 48h, and the rate was 2.03mg $DBT_{removed}/L_{dispersion}-hr.$ At 50% oil phase, medium exchange on 60h was performed and the rate was 1.79mg $DBT_{removed}/L_{dispersion}-hr.$ The 300mL flask system was scaled up to a 5-L bioreactor system. On 60 h, a medium exchange was performed and the rate was 5.28mg $DBT_{removed}/L_{dispersion}-hr.$ and all of DBT was removed. It means that we can use the biodesulfurization process even 10 the high oil-to-water phase by some appropriate methods such as controlled feeding of key nutrients and the dilution or removal of some toxic metabolites by continuous reactor.

• Journal of The Korean Society of Grassland and Forage Science
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• v.5 no.3
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• pp.212-219
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• 1985

The field experiment was conducted to study on the growth analysis of early variety, MTC-1, and late variety, Suweon 19, in response to seeding time at Suweon. The results summarized as follows: 1. Days required for Leaf-Formation(L-phase) of MTC-1 and Suweon 19 was same but that of Node-Thickening(N-phase) was quite different, e.g. late variety has two times longer. The period of Ear-Development (E-phase) in MTC-1 was 41 days and 53 days in Suweon 19. L-and N-phase were shortened by late seeding but E-phase was not influenced by seeding time. 2. Leaf Area Index(LAI) was decreased and Leaf Area Ratio(LAR) was increased by late seeding. Days required to maximum LAR was less by late seeding. Net Assimilation Rate(NAR) of L-, N-, and E-phase was decreased but its tendency in E-phase was remarkable at late seeding. 3. Crop Growth Rate(CGR) was increased gradually in the process of plant growth and it was the highest at Husk-stage. Relative Growth Rate(RGR) was increased in L-phase and was decreased in N- and E-phase, but its tendency in N-phase was great. 4. The period required to the maximum dry matter yield was shortened by late seeding and dry matter yield was increased by early seeding.

• The Transactions of the Korean Institute of Power Electronics
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• v.22 no.1
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• pp.1-8
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• 2017

The optimal gain design method of a three-phase boost converter is proposed in this study. The control system has a two-loop configuration, in which each controller is coupled closely; thus, the optimal design is difficult to achieve using conventional gain-tuning method. The proposed method is adopted to the MATLAB SISO TOOL software and is based on the controller requirements, which are phase margin and cut-off frequency of the open-loop system. The optimal proportional -integral gains can be designed easily using the proposed interactive method of the SISO TOOL. The performance of the proposed system is verified through simulation and experiments.

• The Transactions of the Korean Institute of Power Electronics
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• v.22 no.1
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• pp.53-59
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• 2017

The information on the actual voltages and actual currents of the motor is required for the sensorless control of a permanent magnet synchronous motor without rotor position sensors. In the model-based rotor position estimator of a PM synchronous motor, the reference voltages, which are the outputs of the current controller, are commonly used. The reference voltages in over-modulation regions for high-speed operation differ from the actual voltages applied to the motor. Consequently, the estimated rotor position and rotor speed may fail to track the real rotor position and real rotor speed. In this paper, the sensorless control for a PM synchronous motor in over-modulation regions for high-speed operation is proposed. The three-phase voltages applied to the motor are measured by using additional voltage detection circuits, and the performance of the rotor position estimator based on the measured three-phase voltages is validated through the experimental results.

• Korean Chemical Engineering Research
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• v.56 no.2
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• pp.186-190
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• 2018

For the first time, the characteristics of solid circulation rate ($G_S$) were investigated in a three-phase (gas-liquid-solid) viscous circulating fluidized bed (TPCFB). The solid circulation rate was controlled separately by adjusting the experimental apparatus as well as operating variables. Effects of primary and secondary liquid velocities ($U_{L1}$ and $U_{L2}$), gas velocity ($U_G$), particle size ($d_p$), height of particles piled up in the solid recycle device (h), and viscosity of continuous liquid media (${\mu}_L$) on the value of $G_S$ were determined. The experimental results showed that the value of $G_S$ increased with increases in the values of $U_{L1}$, $U_{L2}$, h and ${\mu}_L$, while it decreased with increasing $U_G$ and $d_p$ in TPCFBs with viscous liquid media. The values of $G_S$ were well correlated in terms of dimensionless groups within this experimental conditions.

• Journal of the Mineralogical Society of Korea
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• v.10 no.2
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• pp.97-104
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• 1997

Based on the method of determination for relative stability of each phase from the difference among the interaction parameters of the phases consisting the mixed layer, the types of interactions between layers were specified and interaction parameter between layers in ordered domain was analytically derived as a function parameter between layers in ordered domain was analytically derived as a function of not only temperature and mole fraction of layers but also ordering parameter. Interaction parameter between the different layers in ordered phase, L is as follows:{{{{ {L }_{1 } (X,Q,T)= { C} over { Q} -4(1-2Q) { L}^{2 } - { RT} over {2} ln { 1} over {2 } - { 2RT} over { { X}_{ s} } ln { { 4QX}`_{s } ^{2 } } over {(1- { X}_{s }- { QX}_{s })( { X}_{s }- {QX }_{s } ) } }}}}L2 is the interaction parameter between ordered and disordered phase in domain and is the mole fraction of the domain which represent the infinite length of mixed layer mineral and Q and C are the reaction progress parameter and arbitrary constant, respectively. This equation was used for the I/S mixed layer clay minerals to infer the relative stability of R1 type I/S mixed layer in the temperature range from 373K to 450K. The result of calculation suggest that, owing to the decrease in interaction parameter with increasing temperature. The interaction parameter decreases more rapidly with decreasing mole fraction of smectite in domain, which is consistent with the fact that the probability of finding the series smectite layer is lo in the domain with small mole fraction of smectite layers in natural system.