• 제목/요약/키워드: KT

검색결과 1,933건 처리시간 0.029초

담배 연기 중 휘발성 유기물질 분석에 대한 측정 불확도 산출 (Measurement Uncertainty for Analysis of Volatile Organic Compound in Cigarette Mainstream Smoke)

  • 가미현;조성일;김미주;이철희;지상운;정종수;김용하;민영근
    • 한국연초학회지
    • /
    • 제28권2호
    • /
    • pp.144-151
    • /
    • 2006
  • A measurement uncertainty for analysis of volatile organic compound (benzene) in cigarette mainstream smoke was carried out. In this study one point re-calibration method was used to estimate uncertainty for benzene. The measurement uncertainty was calculated based on the uncertainty sources of each analysis step, quality appraisal sources, drift and repeatability. As a result, the concentration and expanded uncertainty of benzene in cigarette mainstream smoke were measured as $38.08{\pm}4.36{\mu}g/cig$. Relative uncertainty of drift and repeatability obtained were 5% and 3%, respectively.

Solid-Phase Extraction을 이용한 담배연기 중 Aromatic Amino의 분석 (Analysis of Aromatic Amines in Mainstream Cigarette Smoke Using Solid-Phase Extraction)

  • 김익중;이존태;이정민;민혜정;장기철;김효근;황건중;민영근
    • 한국연초학회지
    • /
    • 제28권2호
    • /
    • pp.152-157
    • /
    • 2006
  • A new procedure has been developed for the quantitation of aromatic amines in mainstream cigarette smoke. Two solid-phase extraction (SPE) clean up steps, using a different retention mechanisms, are required to process the samples. The first step used a cation-exchange cartridge, followed by a second step that used a cartridge with a hydrophobic retention character. The aromatic amines eluted from the second SPE cartridge are derivatized with pentafluoropropionic anhydride. This new method have advantages over other reported techniques, being sensitive, robust, and easily automated. The detection limits were ranged from 0.12 ng/mL for 1-aminonaphthalene to 0.16 ng/mL for 3-aminobiphenyl and the recoveries were from 97 to 106%. Compared with other reports for analysis of 2R4F reference cigarette, this method shows a close analytical data and good repeatability.

Effects of Kinesio Taping on Balance and Gait in Patients with Stroke: A Systematic Review and Meta-Analysis of Studies in Korea

  • Kim, Byeong Geun;Cho, Woon Su;Kim, Yong Seong
    • The Journal of Korean Physical Therapy
    • /
    • 제33권1호
    • /
    • pp.21-27
    • /
    • 2021
  • Purpose: The objective of this study was to investigate the effects of Kinesio taping (KT) for balance and gait in patients with stroke through meta-analysis of studies conducted in Korea. Methods: RISS, Science on, and DBPia were the three databases used to collect articles on KT. Keywords such as "Stroke," "Kinesio taping," "Elasticity taping," and "Taping" were used to search for published articles. We systematically searched from the inception of each database to November 2020. Interventions and comparisons were KT and without KT. Outcome measures were the timed up and go (TUG) and 10-meter walking tests (10MWT). Consequently, six studies were selected for the second screening using meta-analyses. Results: Based on the results of the meta-analysis, comparison between patients with and without KT showed that KT was effective for TUG (ES: 2.51, 95% CI: 2.12 to 2.90); however, it was not effective for 10MWT (ES: 0.79, 95% CI: -0.04 to 1.62). Conclusion: The current evidence suggests that KT is more effective than without KT interventions for balance function in post-stroke patients. However, more well-conducted randomized controlled trials are required in the future.

Octopole Reaction Cell이 장착된 ICP-MS에 의한 분유 중 셀레늄의 정량 (Determination of selenium in milk powder by octopole reaction cell ICP-MS)

  • 조성일;김미주;김용하;민영근;김영상
    • 분석과학
    • /
    • 제19권3호
    • /
    • pp.203-210
    • /
    • 2006
  • Octopole reaction cell inductively coupled plasma mass spectrometer (ORC-ICP-MS)를 이용하여 우유 분말시료 중 극미량의 셀레늄(Se)을 정량하였다. 반응가스로 $H_2$를 사용함으로써 극미량 측정에서 발생되는 다원자 이온 종들과 공존 원소에 의해 발생되는 분자들의 방해를 현저하게 제거하였다. Normal mode에 비해서 $H_2$ cell gas mode는 정확성과 정밀성을 크게 향상시켰으며, 우유 표준시료의 보증 값에 비해 정량한 결과는 평균 102.7%로 약간 높게 나타났고, 5회 정량한 값에 대한 상대표준편차는 7.6%이었다.

판상엽 배합비와 공기희석율이 제품담배 연기성분 및 연소온도 변화에 미치는 영향 (Effects of Reconstituted Tobacco Sheet contents and Ventilation on the Smoke delivery and the Burning Temperature)

  • 성용주;한영림;백신;김시몽;제병권;오인혁;이창국;김수호;신창호;김근수
    • 한국연초학회지
    • /
    • 제30권2호
    • /
    • pp.103-108
    • /
    • 2008
  • The application of RECON(Reconstituted tobacco sheet) and the ventilation technology has been considered as very useful methods for controlling the tar and nicotine deliveries in modern blended tobacco. In this study, the effects of RECON contents in simulated blends on the smoke delivery and burning temperature were evaluated in three different ventilation levels. The ventilation showed a great influence on the burning temperature and smoke deliveries. The nicotine, tar and CO deliveries was greatly reduced by the ventilation. The amount of RECON showed the minor impacts on the smoke delivery. In high ventilation level such as 85 % ventilation, there was no distinct change in smoke deliveries by the amount of RECON.

경피흡수를 위한 케토롤락 하이드로겔의 제제설계 및 평가 (Formulation Design and Evaluation of Ketorolac Tromethamine Hydrogel for Transdermal Delivery System)

  • 조인숙;이계원;이종화;지웅길
    • Journal of Pharmaceutical Investigation
    • /
    • 제33권1호
    • /
    • pp.21-28
    • /
    • 2003
  • Ketorolac tromethamine(KT) is a nonsteroidal agent with potent analgesic and moderate anti-inflammatory activity. The lipid-water partition coefficient of KT was evaluated and KT gel was formulated as a gel containing different pH, different concentrations of polymer (poloxamer 407, carbopol 941), propylene glycol, ethanol and various enhancers. The resulting KT gels were evaluated with respect to their viscosity, in vitro drug permeation rate through hairless mouse skin and stability. In n-octanol and chloroform, the lipid-water partition coefficient of KT was the highest at pH 4 phosphate buffer. The apparent viscosity of KT gel increased with an increase in gel pH, polymer and enhancer concentration. But the apparent viscosity of KT gel decreased with an increase in ethanol concentration. The permeation rate of KT through hairless mouse skin from gels different pH was maximum at pH 4 which is close to KT $pK_{a}$ 3.54. The permeation rate decreased with an increase in polymer, propylene glycol concentration. But the permeation rate increased with an increase in ethanol. The increase of drug concentration from 1 to 3% induced linear increase in permeation rate. The best enhancer was the combination of $Labrasol^{\circledR},\;Transcutol^{\circledR}$, oleic acid and l-menthol. In the accelerated stability test(25, 40 and $50{\circ}C$), pH 5 gel was most stable and pH 4 gel was most unstable for 90 days.