• Title/Summary/Keyword: Ion sensor

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Development of an Enzyme Electrode Biosensor for Lactic Acid Bacteria (효소 전극을 이용한 유산균 측정 바이오센서 개발)

  • Park T. S.;Cho S. I.
    • Journal of Biosystems Engineering
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    • v.30 no.4 s.111
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    • pp.249-253
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    • 2005
  • This study was carried out to develop enzyme biosensor for lactic acid bacteria. Lactic acids produced by lactic acid bacteria (LAB) was measured and good correlation $R^2=0.98$ between LAB count and lactic acids concentration was found. Hydrogen ion produced by L-lactate dehydrogenase (L-LDH) was measured by a potentiometer. Glutamic-pyruvic transminase (GPT) was used for eliminating inhibitor in the reaction. Polyacrylamide gel was used for immobilizing matrix of the sensor. The biosensor was tested and showed good feasibility with $R^2=0.99$ on validation.

Fabrication of Electrospun Cobalt Nanofiber (전기 방사 기반의 코발트 나노 섬유의 제작)

  • Heo, Joonseong;Lim, Geunbae
    • Journal of Sensor Science and Technology
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    • v.24 no.1
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    • pp.35-40
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    • 2015
  • Electrospinning method has easy preparation of nanofibers with a simple and versatile technique. Electrospun nanofiber is widely used by the simple approach and have great potentials in the numerous applicaitons of medicine, photonics, catalysts, sensors, etc. including advantage of their specific characteristics such as large surface to volume ratio. This paper focused on the fabrication of cobalt electrospun nanofibrer for applications such as electronic, optical and mechanical devices by metal based material. We fabricated cobalt nanofibers on aluminum foil by an electrospinning method. The electrospinning process was performed at a high voltage, 8 kV. The distance between the needle tip and the solution surface in the bath was 5 cm. The PVB - cobalt based nitrate solution was filled in a 10 mL syringe connected to a 22 gauge needle. We confirmed electrospun cobalt nanofiber after annealing process by SIMS (Secondary Ion Mass Spectrometry) analysis. The concept design, fabrication and results of mapping measurements are reported.

Electromechanical Simulation of Cellulose Based Biomimetic Electro-Active Paper (생체모방 종이작동기(electro-active paper)의 전기기계적인 구동 시뮬레이션)

  • Jang, Sang-Dong;Kim, Jae-Hwan;Kim, Heung-Soo
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.17 no.12
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    • pp.1179-1183
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    • 2007
  • Electro-Active paper(EAPap) is a new smart material that has a potential to be used in biomimetic actuator and sensor. It is made by cellulose that is abundant material in nature. EAPap is fascinating with its biodegradability, lightweight, large displacement, high mechanical strength and low actuation voltage. Actuating mechanism of EAPap is known to be the combined effects of ion migration and piezoelectricity. However, the electromechanical actuation mechanisms are not yet to be established. This paper presents the modeling of the actuation behavior of water infused cellulose samples and their composite dielectric constants calculated by Maxwell-Wagner theory. Electro-mechanical forces were calculated using Maxwell stress tensor method. Bending deflection was evaluated from simple beam model and compared with experimental observation, and which result in good correlation with each other.

Design of a Portable Electronic Tongue System using Fuzzy C-Means Algorithm (Fuzzy C-Means Algorithm을 이용한 휴대용 전자혀 시스템 설계)

  • Kim, Jeong-Do;Kim, Dong-Jin;Ham, Yu-Kyung;Jung, Young-Chang;Yoon, Chul-Oh
    • Journal of Sensor Science and Technology
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    • v.13 no.6
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    • pp.446-453
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    • 2004
  • A portable electronic tongue (E-Tongue) system using an array of ion-selective electrode (ISE) and personal digital assistants (PDA) for recognizing and analyzing food and drink have been designed. By the employment of PDA, the complex algorithm such as fuzzy c-means algorithm (FCMA) could be used in E-Tongue, PUMA could iteratively solve the cluster centers of pre-determined standard patterns. And the membership between the standard patterns and unknown pattern could be analyzed easily by the present E-Tongue combined with PDA.

Synthesis and Fluorescent Properties of New Host Compound Containing Anthracene Moiety (안트라센이 포함된 새로운 호스트 화합물의 합성과 물성)

  • Chang, Seung-Hyun
    • Journal of Environmental Science International
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    • v.17 no.12
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    • pp.1373-1380
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    • 2008
  • Anthracene appended new host compounds have been synthesized by imine reaction. Fluorescent open chain host compounds Trisanthryl-tris(2-aminoethyl)imine 1 was synthesized from the reaction of tris(2-aminoethyl)amine and anthracene-9-carboxaldehyde in EtOH. Tris-10-chloroanthryl-tris(2-aminoethyl)imine 2 was synthesized from tris(2-aminoethyl)amine and 10-chloro-9-anthraldehyde in EtOH. The structures of all reaction product were identified by $^1H$ NMR, $^{13}C$ NMR, GC/MS, FAB Mass, IR spectrum and DSC. Cation complexation behavior was investigated by fluorescence spectroscopy measurements. The capability of transition metals cation recognition between fluorescent open chain host compound 1, 2 were investigated with $Co^{2+},\;Ni^{2+}\;and\;Cu^{2+}$. The fluorescence intensity was increased by host compounds corresponding guest cations. The relative order of fluorescence intensity changes were $Co^{2+}>Cu^{2+}>Ni^{2+}$. Compound 2 is very sensitive fluorescent sensor of $Co^{2+}$ ion.

Preparation of SnO and SnO, SnO2 fine powder by hydrazine method (Hydrazine법에 의한 SnO, SnO2 미분말의 합성)

  • Kim, Kang-Min;Kim, Ki-Won;Cho, Pyeong-Seok;Lee, Jong-Heun
    • Journal of Sensor Science and Technology
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    • v.14 no.5
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    • pp.297-301
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    • 2005
  • Nanocrystalline SnO and $SnO_{2}$ powder have been prepared by hydrazine method. Sn-Hydrazine complex was formed by the reduction between aqueous $SnCl_{2}$ solution and hydrazine monohydrate. $SnO_{2}$ nano powder was prepared by the decomposition of Sn-Hydrazine complex at $450^{\circ}C$. When NaOH was added to Sn-hydrazine complex, SnO powder with nano-sheet morphology could be prepared. This can be attributed to the role of $OH^{-}$ ion as a reducing agent.

Development of Micro-opto-mechanical Accelerometer using Optical fiber (광섬유를 이용한 미세 광 기계식 가속도 센서의 개발)

  • Lee, Seung-Jae
    • Journal of the Korean Society of Mechanical Technology
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    • v.13 no.4
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    • pp.93-99
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    • 2011
  • This paper presents a new type of optical silicon accelerometer using deep reactive ion etching (DRIE) and micro-stereolithography technology. Optical silicon accelerometer is based on a mass suspended by four vertical beams. A vertical shutter at the end of the mass can only moves along the sensing axis in the optical path between two single-mode optical fibers. The shutter modulates intensity of light from a laser diode reaching a photo detector. With the DRIE technique for (100) silicon, it is possible to etch a vertical shutter and beam. This ensures low sensitivity to accelerations that are not along the sensing axis. The microstructure for sensor packaging and optical fiber fixing was fabricated using micro stereolithography technology. Designed sensors are two types and each resonant frequency is about 15 kHz and 5 kHz.

Studies of Polymer Matrix Effect for Coextraction Type Anion-Selective Optode and Determination of Thiocyanate in Human Saliva

  • Hong, Young-Ki;Cha, Geun-Sig;Shin, Doo-Soon;Nam, Hak-Hyun
    • Bulletin of the Korean Chemical Society
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    • v.15 no.10
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    • pp.836-841
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    • 1994
  • The polymer matrix effect on the selectivity, response rate and reproducibility for coextraction type anion-selective optode membranes were investigated with DOA-plasticized PVC, PVC/hydroxylated PVC, PU/hydroxylated PVC and DOS-plasticized CTA matrices. Optode membranes were prepared with TDMACl and ETH2412 dissolved in one of the four solvent polymeric matrices. The PU/hydroxylated PVC and PVC-based membranes have almost the same selectivity coefficients, while the CTA-based membrane is more selective toward lipophilic anions. The membrane with PU/hydroxylated PVC adhered strongly to a glass surface, and showed highly reproducible and relatively rapid response. Very poor adhesion of PVC/hydroxylated PVC and CTA-based membranes limited the usability of those membranes as sensor components. Based on these results, and considering the biocompatibility for clinical samples, the optode made with PU/hydroxylated PVC was applied to determine the thiocyanate ion in human saliva. The results obtained with this simple device were comparable to those with rather complicated ISE methods.

Effect of corrugation structure and shape on the mechanical stiffness of the diaphragm

  • Kim, Junsoo;Moon, Wonkyu
    • Journal of Sensor Science and Technology
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    • v.30 no.5
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    • pp.273-278
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    • 2021
  • Here, we studied the change in the mechanical stiffness of a diaphragm according to the corrugation pattern. The diaphragm consists of a silicon oxide and nitride double layer; a corrugation pattern was formed by dry etching, and the diaphragm was released by wet etching. The fabrication of the thin film was verified using focused ion beam and scanning electron microscopy images. The mechanical stiffness of the diaphragm was obtained by measuring the surface vibration using a laser Doppler vibrometer while applying external sound pressure. Flat squares, diaphragms with square corrugations, and circular corrugation patterns were measured and compared. The stiffness of the diaphragm with a corrugation structure was found to be smaller than that without a corrugation structure; in particular, circular corrugation showed a better effect because of the high symmetry. Furthermore, the effect of corrugation was theoretically predicted. The proposed corrugated diaphragm showed comparable flexibility with the state-of-the-art MEMS microphone diaphragm.

Electrochemical Determination of Capsaicin by Ionic Liquid Composite-Modified Electrode

  • Kim, Dong-Hwan;Nam, Sungju;Kim, Jaeyoon;Lee, Won-Yong
    • Journal of Electrochemical Science and Technology
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    • v.10 no.2
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    • pp.177-184
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    • 2019
  • An electrochemical detection method for capsaicin has been developed using ionic liquid (IL) doped graphene-titania-Nafion composite-modified electrode. The combination of IL (1-hexyl-3-methylimidazolium with hexafluorophosphate counter ion) in the composite-modified electrode resulted in a significantly increased electrochemical response for capsaicin compared to that obtained at the corresponding electrode without IL. The increased electrochemical signal could be ascribed to the decreased electron transfer resistance through the composite film and also to the effective accumulation of capsaicin on the electrode surface due to ${\pi}-{\pi}$ interaction of the imidazole groups of IL with the aromatic rings of capsaicin. The present IL composite-modified electrode can detect capsaicin with a concentration range from $3.0{\times}10^{-8}M$ to $1.0{\times}10^{-5}M$ with a detection limit of $3.17{\times}10^{-9}M$ (S/N = 3). The present sensor showed good reproducibility (RSD = 3.2%).