• Journal of Welding and Joining
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• 제30권5호
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• pp.34-39
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• 2012

This study was conducted to investigate the microstructure and mechanical properties of friction stir lap joints. Invar 42 and SS 400 were selected as the experimental materials, and friction stir welding was carried out at a tool rotation speed of 200 rpm and welding speed of 100 mm/min. The application of friction stir welding to Invar 42 effectively reduced the grain size in the stir zone; the average grain size of Invar 42 was reduced from $11.5{\mu}m$ in the base material to $6.4{\mu}m$ in the stir zone, which resulted in an improvement in the mechanical properties of the stir zone. The joint interface between Invar 42 and SS 400 showed a relatively sound weld without voids and cracks, and the intermetallic compounds with $L1_2$ type in lap jointed interface were partially formed with size of 100 nm. Moreover, the hook in the advancing side of Invar 42 was formed from SS 400, which contributed to maintenance of the tensile strength. The evolution of microstructures and mechanical properties of friction stir lap jointed Invar 42 and SS 400 are also discussed herein.

• 한국표면공학회지
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• 제50권6호
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• pp.516-522
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• 2017

We report the growth of carbon nanotubes (CNT) on Invar-42 plates using coal tar pitch (CTP) by chemical vapor deposition (CVD) method. The solid phase CTP is used as an inexpensive carbon source since it produces a bunch of hydrocarbon gases such as $CH_4$ and other $C_xH_v$ by thermal decomposition over $450^{\circ}C$. The Invar-42 is a representative Ni-based ferrous alloy and can be used repetitively as a substrate for CNT growth because Ni and Fe are used as very active catalytic elements. We changed mixing ratio of carrier gases, argon and hydrogen, and temperature of growth region. It was found that the optimum gas ratio and temperature for high quality CNT growth are $Ar:H_2=400:400$ sccm and $1000^{\circ}C$, respectively. In addition, the carbon nanoball (CNB) was also obtained by just changing the mixing ratio to $Ar:H_2=100:600$ sccm. Finally, CTP can be employed as a versatile carbon source to produce various carbon-based nanomaterials, such as CNT and CNB.

• 소성∙가공
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• 제15권8호
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• pp.586-590
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• 2006

42Ni-Fe Invar alloy strips were fabricated using conventional ingot casting and melt drag casting followed by rolling. Mechanical properties such as tensile strength, elongation and blanking deformability of the strips were evaluated. The properties were strongly depended on fabrication methods. Tensile strength and elongation of all strips were in the range of $40-60kg/mm^{2}$ and 26-35%, respectively, which are enough values for the manufacture of the final products. In some of the strips, however, burrs occurred at deformed surface. The properties of strips were explained in terms of microstructure such as grain size and texture formation during rolling. Additionally, strips by melt drag casting method were compared to those by conventional ingot casting.

• 한국진공학회지
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• 제20권6호
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• pp.436-441
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• 2011

각종 전자 방출원 및 디스플레이 응용 분야에서 뛰어난 가능성을 보이고 있는 탄소나노튜브의 전계 방출 특성을 개선하고 전자방출의 신뢰성을 개선하기 위해 탄소나노튜브의 표면에 수 nm 두께의 금속 코팅을 적용하였다. 탄소나노튜브는 실리콘 기판위에 2 nm 두께의 Invar (52% Fe, 42% Ni, 6% Co alloy) 촉매를 사용하여 $450^{\circ}C$의 온도에서 플라즈마 화학기상 증착법으로 성장시켰다. 성장된 탄소나노튜브의 밀도 제어를 위해 성장 후 질소 플라즈마로 일부를 식각한 후 티타늄(Ti) 금속을 탄소나노튜브 표면에 5~150 nm 두께로 스퍼터링 증착하였다. 5 nm로 티타늄을 탄소나노튜브 표면에 코팅한 경우, 코팅 전에 비해 6 V/${\mu}m$의 전계에서 전류밀도가 4배 이상 증가되었으며, 전계 방출 전류의 요동(fluctuation) 또한 40% 이상 감소됨을 확인할 수 있었다. 이는 티타늄의 일함수가 4.3 eV로 탄소나노튜브의 5 eV에 비해 작을 뿐만 아니라, 탄소나노튜브의 약점으로 지적되는 기판과의 접착성과 접촉저항이 티타늄의 표면 코팅으로 인해 크게 개선된 결과로 판단된다.