• Journal of the Korean Vacuum Society
• /
• v.10 no.2
• /
• pp.201-206
• /
• 2001

The evolution of textures in Fe-Ni alloy thin films fabricated by PVD using a sputtering method was investigated with parameters such as deposition time and chemical composition. The textures of the as-deposited films were characterized by fibre-type. In Invar alloy(Fe-36.5 wt%Ni) thin film, the <110>//ND fibre texture as a starting component changed to the <210>//ND fibre texture with increasing deposition time. In Permalloy(Fe-81 wt%Ni) thin film, a mixture of the <221>//ND and <311>//ND fibres developed at the early stage of deposition, and then transformed to the <210>//ND fibre with increasing deposition time. These texture changes were discussed in terms of relationship with the microstructural evolution of the films.

• Design & Manufacturing
• /
• v.14 no.3
• /
• pp.44-49
• /
• 2020

One of display trends today is development of high pixel density. To get high PPI, a small size of pixel must be developed. RGB pixel is arranged by evaporation process which determines pixel size. Normally, a fine metal mask (FMM; Invar alloy) has been used for evaporation process and it has advantages such as good strength, and low thermal expansion coefficient at low temperature. A FMM has been manufactured by chemical etching which has limitation to controlling the pattern shape and size. One of alternative method for patterning FMM is laser micromachining. Femtosecond laser is normally considered to improve those disadvantages for laser micromachining process due to such short pulse duration. In this paper, a femtosecond laser drilling for thickness of 16 ㎛ FMM is examined. Additionally, we introduce experimental results for controlling taper angle of hole by vibration module adapted in laser system. We used Ti:Sapphire based femtosecond laser with attenuating optics, co-axial illumination, vision system, 3-axis linear stage and vibration module. By controlling vibration amplitude, entrance and exit diameters are controllable. Using vibrating objective lens, we can control taper angle when femtosecond laser hole drilling by moving focusing point. The larger amplitude of vibration we control, the smaller taper angle will be carried out.

• Proceedings of the Korean Institute of Surface Engineering Conference
• /
• 2005.11a
• /
• pp.164-165
• /
• 2005

• Proceedings of the Korean Magnestics Society Conference
• /
• 1993.03a
• /
• pp.52-53
• /
• 1993

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2004.07b
• /
• pp.1274-1277
• /
• 2004

최근 에너지 소비구조의 선진화에 따라 전력수요는 매년 10%이상 증가하고 있지만 철탑부지확보 및 환경 문제 둥에 의해 신규 송전선의 건설은 점차 어려워지고 있다. 이에 대한 대책으로 철탑의 교체 없이 송전선의 전류용량간 증가시키는 방안이 우선적으로 고려되어 적용되고 있다. 이미 국내에서도 기존 송전선인 ACSR 전선을 중용량 저이도의 특성을 가진 STACIR/AW(Super Thermal-resistant Aluminum alloy Conductors, aluminum-clad Invar-Reinforced)송전선으로 교체하여 전력 수송량을 증가시키고 있다. STACIR/AW전선은 도체의 내열성을 향상시켜 연속허용온도$(210^{\circ}C)$를 높임으로 전류용량을 증가시키고, ACSR에 사용되는 강심재료인 고탄소강선을 선팽창계수가 낮은 인바강선(INVAR)으로 대체함으로 고온환경에 따른 이도증가를 방지하고 있다. 그러나 STACIR/AW 송전선은 ACSR 송전선에 비하여 연속허용온도가 높고 경간의 거리가 멀기 때문에 열화에 의한 피로특성의 변화 가능성이 높다. 따라서 본 연구에서는 증용량저이도전선의 강심소재인 INVAR/AW강선을 소정의 온도에서 경년 열화하고, 열화시간에 따른 강도와 피로특성의 변화를 조사하여, STACIR/AW전선의 안정적 운전을 위한 재료물성적 관리인자를 도출하고자 하였다.

• Transactions of Materials Processing
• /
• v.16 no.5 s.95
• /
• pp.375-380
• /
• 2007

The bimetals of home appliances are mainly manufactured by cladding process and these are almost consisted with Cu alloy and Ni alloy. But it is very difficult to clad these alloys, because the brittle $Cu_3O_4$ oxide film formed easily on Cu alloy surface during cladding process. Clad rolling and heat treatment processes were applied for the development of bimetals by using the Ni alloy and the 3 types of Cu alloys. Optical microstructure, micro-hardness, specific resistance, and deflection and line profile of newly processed bimetals specimens were observed and measured in this paper. Inter-diffusion was observed between Cu and Ni element in the interface of heat treated Cu alloy and Ni alloy clad material. The C1220 and Invar36 clad material showed the best property of deflection among the 3 kind of clad materials.

• Journal of Welding and Joining
• /
• v.32 no.1
• /
• pp.61-65
• /
• 2014

The purpose of this study is to evaluate the applicability of the element stress to establish S-N design curve for the welded lap joint with thin plates below 2mm thickness. In order to do it, the extensive fatigue tests of the welded lap joints with INVAR alloy were performed. With the results, the deign S-N curves for the lap-weld were established by using the reference stresses such as the nominal stress range at the weld throat area, hot spot stress range and element stress range, and compared with regard to the standard deviation. The standard deviation of S-N curves with element stress range was less than that of S-N curves with other reference stresses. In addition, FEA results show the amount of the element stress is less sensitive to mesh size. Based on the results, it can be concluded that the element stress is to be used as the reference stress for the design S-N curves of the welded lap joint.

• Corrosion Science and Technology
• /
• v.22 no.6
• /
• pp.478-483
• /
• 2023

This study examined the corrosion behavior of bimetal materials composed of Fe-Ni alloy and Fe-Ni-Mo alloy, both suitable for use in electromagnetic switches. Electrochemical polarization and weight loss measurements revealed that, in contrast to Fe-Ni alloy, which exhibited pseudo-passivity behavior, Fe-Ni-Mo alloy had higher anodic current density, displaying only active dissolution and greater weight loss. This indicated a lower corrosion resistance in the Fe-Ni-Mo alloy. Equilibrium calculations for the phase fraction of precipitates suggested that the addition of 1 wt% Mo may lead to the formation of second-phase precipitates, such as Laves and M₆C, in the γ matrix. These precipitates might degrade the homogeneity of the passive film formed on the surface, leading to localized attacks during the corrosion process. Therefore, considering the differences in corrosion kinetics between these bimetal materials, the early degradation caused by galvanic corrosion should be prevented by designing a new alloy, optimizing heat treatment, or implementing periodic in-service maintenance.

• Korean Journal of Materials Research
• /
• v.15 no.4
• /
• pp.246-251
• /
• 2005

Plasma enhanced chemical vapor deposition(PE-CVD) method has an advantage in synthesizing carbon nanotubes(CNTs) at lower temperature compared with thermal enhanced chemical vapor deposition(TE-CVD) method. In this study, CNTs was prepared by using PE-CVD method. The growth rate of CNT was faster more than 100 times on using Invar alloy than iron as catalyst. It was found that chrome silicide was formed at the interface between chrome layer and silicon substrate which should be considered in designing process. Nanoparticles of Invar catalyst were found oxidized on their surfaces with a depth of 10 m. Microstructure was analyzed by scanning electron microscopy, transmission electron microscopy, scanning transmission electron microscopy, and energy dispersive x-ray spectrometry. Based on the result of analysis, growth mechanism at an initial stage was suggested.

• 한국정보디스플레이학회:학술대회논문집
• /
• 2003.07a
• /
• pp.1164-1167
• /
• 2003

Recently CRT is getting flatted, As change of CRT trend from normal type to Flat type, the material of Shadow Mask was also changed from AK(Aluminum Killed) to Invar(Fe-Ni alloy) materials Until now we have used just AK(Aluminum Killed) for normal type TV(not flat type), but main raw material of shadow mask component was changed. . However recently Invar(Fe-Ni alloy) materials, which has advantage of Low Thermal Expansion and High Strength, has been developed as well as applying in mass production as CRT's trend has become more flat and fine pitch. As main raw material of shadow mask component was changed, conditions of process were changed. One of them, the importance of pre-etching process (assistant process for developing & etching) is improved because there are so many particles in the pre-etching bath because of Ni compounds. Since the solubility of Ni in pre-etching solvent is very low related to Fe's, so the compounds of Ni happen to make particles.(the solubility of Fe is twenty times Ni's) that particles happen to make process troubles and NG productions so to clear the particles we had to established high cost filtering system, but it is useless. As time goes by the quantity of particles (Ni compounds) was increased because of the capability of filtering system was not enough, the particles was produced continuous in bath, and it make quality problems. Hence we tried to develop the new pre-etching solution to remove the particles (Ni compounds) and to cost down the filtering system's running cost. But in improving the solution we discovered the new pre-etching solution made the PR developing better. In former solution there were three kinds of chemistry (COOH)2 , H2O2 , H2S04 .first the function of (COOH)2 is drilling the surface of Invar, during this mechanism Ni compounds occurred. Second the function of H202 is removing the PR fringe (half UV exposure zone on PR(PVA)), Third the function of H2S04 is the catalysis of (COOH)2 In those, (COOH)2 was the main reason to make the Ni compounds. So to improve the solutions we had to change (COOH)2 to the other material. the chemistry we improved was a complex chemistry based on H2S04 . after using this chemistry the particles problem was disappeared and there was another advantage cut down the PR fringe. The New solution made the function of H202 better so the PR developing improved. To be direct the catalyst of the new solution helped the H202. anyway First thing after change the solution the quality of shadow Mask for flat color TV was improved & the yield also improved. But the more important thing is how to control the new solution. So we accepted the new concept which was the degree of freshness. The degree of freshness is based on non-reacted solution which was 100% ( the degree of freshness) and calculated the melted Ni quantity as time goes by. So we made the gauging liner plot. In conclusion, many companies tried to make fine pitched Shadow Mask ,generally to make quality jump up it needed a lot of cost & persons .in this case the shift of core material made it possible.