• 대한화학회지
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• 제43권4호
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• pp.430-437
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• 1999

흐름주입 분석법(FIA)에 의한 간접 요오드화 UV 검출법으로 총 잔류염소를 신속하게 정량하는 방법을 연구하였다. FIA장치를 최적화하기 위해 용리액의 pH, 요오드화 이온의 농도, 혼합 및 반응코일의 길이,시료주입량 및 유속, 온도 및 검출파장에 대한 변화를 관찰하였다. pH 8.3에서 하이포아염소산 이온은 요오드화 이온을 선택적으로 산화시키고 자신은 염화이온으로 환원되었다. 방해이온을 제거하기 위한 가리움제로서 에틸렌다이아민이 가장 좋은 효율을 나타내었다. 하이포아염소산 이온의 검정곡선은 0.03-0.3 mg/L의 농도 범위에서 0.999이상의 직선성을 나타내었고, 검출한계는 0.007 mg/L이었다. 이러한 분석조건하에서 몇몇 전주근교 상수중 총 잔류염소의 농도를 정량하였다.

• 한국입자에어로졸학회지
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• 제13권4호
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• pp.159-164
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• 2017

The detection efficiency and characteristics of an optical particle counter (OPC), with various sample nozzle outlet diameters, were experimentally investigated. The OPC system, which was built with original design, was made up of a diode laser, two photodetectors, and a variety of optics such as a beam splitter and a concave mirror. The cone-shaped sampling nozzle was designed to be changeable to alter the outlet diameter, within the range of 1 to 3 mm. For samples, sets of polystyrene latex (PSL) standard particle with various sizes of 1 to $3{\mu}m$, were used. As a result, detection efficiency of the OPC greatly decreased with larger nozzle outlet diameter. Moreover, increased nozzle outlet diameter means broader sample flow, thus caused light interference and multiple scattering which results in abnormal high peaks in scattered light signal. The ratio of abnormal peaks to regular signal of single particle increased with larger nozzle outlet diameter.

• 한국군사과학기술학회지
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• 제14권3호
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• pp.405-413
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• 2011

Defense Systems Test Center in ADD supports increasingly various missile test requirements such as higher altitude event, multi target operation and low-altitude, high velocity target tracking. In this paper, we have proposed the development of instrumentation radar tracking status simulator based on virtual reality. This simulator can predict the tracking status and risk of failure using several modeling algorithms. It consists of target model, radar model, environment model and several algorithms includes the multipath interference effects. Simulation results show that the predict tracking status and signal are similar to the test results of the live flight test. This simulator predicts and analyze all of the status and critical parameters such as the optimal site location, servo response, optimal flight trajectory, LOS(Line of Sight). This simulator provides the mission plan with a powerful M&S tool to rehearse and analyze instrumentation tracking radar measurement plan for live flight test at DSTC(Defense Systems Test Center).

• Journal of Power Electronics
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• 제13권1호
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• pp.170-176
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• 2013

Power converters produce a vast range of harmonics, subharmonics and interharmonics. Harmonics analyzing tools based on the Fast Fourier Transform (FFT) assume that only harmonics are present and the periodicity intervals are fixed, while these periodicity intervals are variable and long in the presence of interharmonics. Using FFT may lead to invalid and undesired results due to the above mentioned issues. They can also lead to problems such as frequency blending, spectral leakage and the picket-fence effect. In this paper, the group-harmonic weighting (GHW) approach has been presented to identify the interharmonics in a power system. Afterwards, a modified GHW has been introduced to calculate the proper bandwidth for analyzing the various values of interharmonics. Modifying this method leads to more precise results in the FFT of a waveform containing inter harmonics especially in power systems with a fundamental frequency drift or frequency interference. Numerical simulations have been performed to prove the efficiency of the presented algorithm in interharmonics detection and to increase the accuracy of the FFT and the GWH methods.

• 한국통신학회논문지
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• 제36권2C호
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• pp.93-98
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• 2011

현재 매우 빠른 속도로 늘어나고 있는 인터넷 수요를 충족시키기 위하여 새로운 통신 대안이 필요하다. 이런 대안들 중에 하나가 바로 광대역 고속 전력선 통신이다. 전력선 통신은 전력을 전달하는 도체에 신호를 같이 실어 보내는 통신 방법이다. 하지만 전력선을 그대로 사용한다는 단점 때문에 기존의 사용되는 통신 시스템과의 간섭이 발생한다. 이런 간섭을 제거하기 위하여 일반적인 방법으로는 Notch 필터를 주로 사용한다. 반면 다른 방법의 하나로 Wavelet OFDM이 사용된다. 본 논문에서는 Wavelet OFDM에서 사용되는 CMFB구조에 CIC 필터를 적용하여 그 부협의 값을 더욱 낮추어 성능을 높이는 방법을 제안한다.

• Bulletin of the Korean Chemical Society
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• 제30권12호
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• pp.3034-3038
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• 2009

A simple, rapid, practical and sensitive spectofluorimetric method was developed for the determination of trace amount of heparin (Hep). Under the Optimum conditions, we studied the interaction between NFLX-Ce$^{3+}$-Hep complex by using absorption and fluorescence spectra. It was observed that Hep remarkably enhance the fluorescence intensity of the NFLX-Ce$^{3+}$ complex at ${\lambda}$= 356 nm in the buffer solution of pH = 7.60 and the enhancement effect is shown to relate with the concentration of Hep. The linear range and detection limit for the determination of Hep was obtained. By the Rosenthal graphic method, the association constant (K) and binding numbers (N) of Hep with probe were investigated. This method is relatively free of interference from coexisting substances and successfully applied for the determination of heparin in heparin sodium injection samples. A suitable mechanism of fluorescence enhancement between NFLX-Ce$^{3+}$ and the NFLX-Ce$^{3+}$-Hep systems were proposed and discussed.

• Bulletin of the Korean Chemical Society
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• 제30권7호
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• pp.1516-1520
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• 2009

A sensitive technique for the determination of trace Co(II) in various samples after column preconcentration by adsorbing onto silica gel loaded with 1-nitroso-2-naphthol was developed. Several experimental conditions, such as pH of sample solution, the amount of silica gel loaded with 1-nitroso-2-naphthol, the flow rate for adsorption and so forth, were optimized. The interfering effects of diverse concomitant ions were investigated. Fe(III) interfered with more than any other ions, but the interference by Fe(III) was completely eliminated by adjusting the amount of silica gel loaded with 1-nitroso-2-naphthol to 0.30 g. The dynamic range, the correlation coefficient ($R^2$), and the detection limit obtained by the proposed technique were 3.0-140.0 ng m$L^{-1}$, 0.9942, and 1.81 ng m$L^{-1}$, respectively. For validating the technique, the aqueous samples (tap water, reservoir water, stream water, and wastewater) and the plastic samples were used as real samples. Recovery yields of 93.0-107.0% were obtained. These measured data were not different from ICP-MS data at the 95% confidence level by F test. Based on the results of the experiment, it has been found that the proposed technique can be applied to the determination of Co(II) in various real samples.

• Bulletin of the Korean Chemical Society
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• 제28권2호
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• pp.183-187
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• 2007

A simple and sensitive extractive spectrophotometric method has been described for the determination of buprenorphine either in raw material or in pharmaceutical formulations. The developed method is based on the formation of a colored ion-pair complex (1 : 1 drug/dye) of buprenorphine and bromocresol green (BCG) in buffer pH 3 and extracting in chloroform. The extracted complex shows absorbance maxima at 415 nm. Beer's law is obeyed in the concentration range of 1.32-100.81 μ g mL-1. The proposed method has been applied successfully for the determination of drug in commercial sublingual tablets and injectable dosage form. No significant interference was observed from the excipients commonly used as pharmaceutical aids with the assay procedure.

• Journal of Magnetics
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• 제14권3호
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• pp.124-128
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• 2009

Magnetic nanoparticles were synthesized by using the sonochemical method with oleic acid as a surfactant. The average size of the magnetite nanoparticles was controlled by varying the ratio R=[$H_2O$]/[surfactant] in the range of 2 to 9 nm. To prepare chitosan-coated magnetite nanoparticles, chitosan solution was added to a magnetite colloid suspension under ultrasonication at room temperature for 20 min. The chitosan-coated magnetite nanoparticles were characterized by several techniques. Atomic force microscopy (AFM) was used to image the chitosan-coated nanoparticles. Magnetic hysteresis measurement was performed by using a superconducting quantum interference device (SQUID) magnetometer to investigate the magnetic properties of the magnetite nanoparticles and the chitosan-coated magnetite nanoparticles. The SQUID measurements revealed the superparamagnetism of both nanoparticles. The T1- and T2-weighted MR images of these chitosan-coated magnetite colloidal suspensions were obtained with a 4.7 T magnetic resonance imaging (MRI) system. The chitosancoated magnetite colloidal suspensions exhibited enhanced MRI contrasts in vitro.

• 제어로봇시스템학회논문지
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• 제16권5호
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• pp.433-439
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• 2010

This paper proposes a beacon color code scheduling algorithm for the localization of multiple robots in a multi-block workspace. With the developments of intelligent robotics and ubiquitous technology, service robots are applicable for the wide area such as airports and train stations where multiple indoor GPS systems are required for the localization of the mobile robots. Indoor localization schemes using ultrasonic sensors have been widely studied due to its cheap price and high accuracy. However, ultrasonic sensors have some shortages of short transmission range and interferences with other ultrasonic signals. In order to use multiple robots in wide workspace concurrently, it is necessary to resolve the interference problem among the multiple robots in the localization process. This paper proposes an indoor localization system for concurrent multiple robots localization in a wide service area which is divided into multi-block for the reliable sensor operation. The beacon color code scheduling algorithm is developed to avoid the signal interferences and to achieve efficient localization with high accuracy and short sampling time. The performance of the proposed localization system is verified through the simulations and the real experiments.