• Title/Summary/Keyword: Interference Range

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Flotation-Spectrophotometric Determination of Ag(I) at the 10-7 mol L-1 Level Using Iodide and Ferroin as an Ion-associate

  • Hosseini, Mohammad Saeid;Hashemi-Moghaddam, Hamid
    • Bulletin of the Korean Chemical Society
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    • v.26 no.10
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    • pp.1529-1532
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    • 2005
  • A simple and cost effective method for separation and preconcentration of Ag(I) at the $10^{-7}\;mol\;L^{-1}$ level in the environmental and mineral samples is present. The method is based on the flotation of Ag(I)-iodide complex as an ion-associate with ferroin in pH of 4 from a large volume of an aqueous solution (500 mL) using nheptane. The floated layer was then dissolved in dimethylsulfoxide (DMSO) for the subsequent spectrophotometric determination. Beer's law was obeyed over a range of 2.0 ${\times}$ $10^{-7}$-4.0 ${\times}$ $10^{-6}$ mol $L^{-1}$ with the apparent molar absorptivity of 2.67 ${\times}$ $10^5$ L $mol^{-1}\;cm^{-1}$. The detection limit (n = 5) was 4 ${\times}$ $10^{-8}$ mol $L^{-1}$, and RSD (n = 5) obtained for 2.0 ${\times}$ $10^{-6}$ mol $L^{-1}$ of Ag(I) was 2.2%. The interference effects of a number of elements was studied and found that only $Hg^{2+}$ at low concentration, and $Pb^{2+}$, $Cd^{2+}$, $Cu^{2+}$, and $Fe^{3+}$ ions at moderately high concentrations were interfered. To overcome on these interference effects, the solution was treated with EDTA at a buffering pH of 4 and passed through a column containing Amberlite IR-120 ionexchanger resin, just before the flotation process. The proposed method was applied to determine of Ag(I) in a synthetic waste water, a photographic washing sample and a geological sample and the results was compared with those obtained from the flame atomic absorption spectrometry. The results were satisfactorily comparable with together, so that the applicability of the proposed method was confirmed in encountering with the real samples.

Development of the EM Wave Absorber Using MnZn-Ferrite and Sendust for Wireless LAN at 2.4 GHz (MnZn-Ferrite와 Sendust를 이용한 2.4 GHz 무선LAN용 전파흡수체 개발)

  • Lee, Dae-Hee;Choi, Chang-Mook;Choi, Dong-Han;Kim, Dong-Il
    • Journal of Navigation and Port Research
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    • v.31 no.10
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    • pp.865-868
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    • 2007
  • Recently, wireless LANs are often applied in home or office because of its various of convenience. Frequency range of wireless LANs specified by IEEE 802.11b is at 2.4 GHz. The bluetooth, the microwave oven, and the PDA(Personal Digital Assistants) uses, however, the same frequency band. So problems will be produced in these environments, such as multi-pass interference and system-to-system interference. These problems can be eliminated by using EM wave absorber. In this paper, we designed and fabricated EM wave absorber using MnZn-Ferrite, Sendust, and CPE( Chlorinated Polyethylene). The EM wave absorber with the ratio of material (MnZn-Ferrite : Sendust : CPE = 64 : 16 : 20 wt.%) has thickness of 3.7 mm and absorption ability more than 17 dB at 2.4 GHz.

Determination of Inorganic Elements in Women Blood Serum using Instrumental Neutron Activation Analysis (중성자방사화분석법을 이용한 성인여성 혈청중의 무기 원소 분석)

  • Moon, Jong-Hwa;Chung, Yong-Sam;Lee, Ok-Hee
    • Analytical Science and Technology
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    • v.15 no.6
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    • pp.509-513
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    • 2002
  • In this study, instrumental neutron activation analysis was used to assess the concentration level of inorganic trace elements in Korean women blood serum. It was found out that high concentration of Na and Cl incurs analytical interference, but 12 elements of Br, Ca, Cl, Co, Cr, Cs, Fe, K, Na, Rb, Se, Zn can be determined under the condition of interference minimization. Serum samples collected from 63 women were analyzed and the concentration level and range of the elements were evaluated. NIST SRMs were analyzed simultaneously for analytical quality control. The average values of Na and Cl determined in serum samples are around 3000 mg/L, Ca is 100 mg/L and K is 200 mg/L. Besides, Br, Se and Zn have concentration level of 6.0, 0.1 and 1.0 mg/L, respectively. It was found that there is no significant difference between the present values and reported values.

Analysis of the Warm Shrink Fitting Process for Assembling the Part(Shaft and Output Gear) (단품(축/OUTPUT 기어)조립을 위한 온간압입공정 해석)

  • Kim, Tae-Jin;Kang, Hee-Jun;Kim, Chul;Chu, Suck-Jae;Kim, Ho-Yun
    • Journal of the Korean Society for Precision Engineering
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    • v.25 no.6
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    • pp.47-54
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    • 2008
  • Fitting process carried out in the automobile transmission assembly line is classified into three classes; heat fitting, press fitting, and their combined fitting. Heat fitting is a method that heats gear to a suitable range under the tempering temperature and squeezes it toward the outer diameter of shaft. Its stress depends on the yield strength of gear. Press fitting is a method that generally squeezes gear toward that of shaft at room temperature by a press. Another method heats warmly gear and safely squeezes it toward that of shaft. Warm shrink fitting process for the automobile transmission part is now gradually increased, but the parts (shaft/gear) assembled by this process produced dimensional changes in both the outer diameter and profile of the gear. So that it may cause noise and vibration between gears. In order to solve these problems, we need an analysis of warm shrink fitting process, in which design parameters are involved; contact pressure according to fitting interference between outer diameter of shaft and inner diameter of gear, fitting temperature, and profile tolerance of gear. In this study, an closed form equation to predict contact pressure and fitting load was proposed in order to develop an optimization technique of the warm shrink fitting process and verified its reliability through the experimental results measured in the field and FEM, that is, thermal-structural coupled field analysis. Actual loads measured in the field was in good agreements with the results obtained by the theoretical and finite element analysis.

A Study on the Development of Power-Line EMI Filter for the Prevention of Conduction Noise by Coil Loads. (코일성 부하에 의한 전도 노이즈 방지 목적의 전원용 EMI필터 개발 연구)

  • Kim, Byeong Jun;Joo, Jae-hun;Kim, Jin Ae;Baek, Pan Keun;Choi, Jung-Keyng
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2009.05a
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    • pp.175-179
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    • 2009
  • this paper proposes a filter design that makes to be satisfied EMC spec. in reliability test of analogue switch for electronic equipment and air conditioning load unit. A designed electromagnetic wave filter was applied to minimize an mutual interference and surrounding environment and improve the product's quality being satisfied to EMC standard. By simulation, using a spectrum analyzer at the 30MHz~1GHz band, ISO/JASO standard frequency range, and simplified EMI chamber, energy distribution of a specific frequency band was analyzed and the capacity of the element which composed the filter was determined in order to implement the most suitable electromagnetic wave filter.In fact, it was certificated that noise decrease by filter addition to the analogue switch for electronic equipment and air conditioning load unit in Certification Authority, and confirmed that the unit is carried out a normal action without electromagnetic wave interference.

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Performance analysis of Coaxial Propeller for Multicopter Type PAV (Personal Air Vehicle) (멀티콥터형 PAV(Personal Air Vehicle)의 동축반전 프로펠러에 대한 성능해석)

  • Kim, Young Tae;Park, Chang Hwan;Kim, Hak Yoon
    • Journal of Aerospace System Engineering
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    • v.13 no.3
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    • pp.56-63
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    • 2019
  • Performance analyses were performed on a propeller developed for use in a PAV (Personal Air Vehicle) under 600 kg Maximum Take-Off Weight (MTOW). The actuator disc theory and CFD analyses were used to estimate the hovering time with regards to MTOW variation for a given battery weight. The interference induced power factor kint was introduced to account for the effect of flow interference between the propellers and to estimate the performance of counter-rotating propellers. The Maximum Figure of Merit (FM) value of the propeller pitch was determined and the design RPM range for the required power inversely obtained from the CFD results. Previous research indicate that the flight time of large multi-copter is limited by the available battery energy density. Similarly, the propeller pitch settings and spacing are important factors in reducing the kint value.

A Study on the Behavior of Surface Settlement due to the Excavation of Twin TBM Tunnels in the Clay Grounds (점토지반에서 TBM 병렬터널 굴진 시 지표침하거동에 대한 연구)

  • You, Kwangho;Jung, Suntae
    • Journal of the Korean GEO-environmental Society
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    • v.20 no.2
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    • pp.29-40
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    • 2019
  • Mechanized constructions have been frequently increased in soft ground below sea bed or river bed, for urban tunnel construction, and for underpinning the lower part of major structures in order to construct a safer tunnel considering various risk factors during the tunnel construction. However, it is difficult to estimate the subsidence behavior of the ground surface due to excavation and needs to be easily predicted. Thus, in this study, when a twin tunnel is constructed in the soft ground, it is proposed a simpler equation relating to the settlement behavior and a corrected formula applicable to soft ground and large diameter shield tunnels based on the previously proposed theory by Peck (1969). For this purpose, it was analyzed to long-term measurement values such as the amount of maximum settlement, the subsidence range by ground conditions, and interference volume loss due to the parallel construction, etc. As a result, a equation was suggested to predict the amount of maximum settlement in the soft sediment clay ground where is located at the upper part of the excavation site. It is turned out that the proposed equation is more suitable for measurement data in Korea than Peck (1969)'s.

Distance Estimation Based on RSSI and RBF Neural Network for Location-Based Service (위치 서비스를 위한 RBF 신경회로망과 RSSI 기반의 거리추정)

  • Byeong-Ro Lee;Ju-Won Lee
    • The Journal of Korea Institute of Information, Electronics, and Communication Technology
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    • v.16 no.5
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    • pp.265-271
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    • 2023
  • Recently, location information services are gradually expanding due to the development of information and communication technology. RSSI is widely used to extract indoor and outdoor locations. The indoor and outdoor location estimation methods using RSSI are less accurate due to the influence of radio wave paths, interference, and surrounding wireless devices. In order to improve this problem, a distance estimation method that takes into account the wireless propagation environment is necessary. Therefore, in this study, we propose a distance estimation algorithm that takes into account the radio wave environment. The proposed method estimates the distance by learning RSSI input and output considering the RBF neural network and the propagation environment. To evaluate the performance of the proposed method, the performance of estimating the location of the receiver within a range of up to 55[m] using a BLE beacon transmitter and receiver was compared with the average filter and Kalman filter. As a result, the distance estimation accuracy of the proposed method was 6.7 times higher than that of the average filter and Kalman filter. As shown in the results of this performance evaluation, if the method of this study is applied to location services, more accurate location estimation will be possible.

EMI (Electromagnetic Interference) Shielding Properties of Barium-Based Ferrite Thin Films Prepared by Spin Spray Method (스핀 스프레이 방식으로 제조된 바륨계 페라이트 박막의 EMI (Electromagnetic Interference) 차폐 특성)

  • Hye Ryeong Oh;Yeon-Ju Park;Woo-Sung Lee;Chan-Sei Yoo;Myong-Jae Yoo;Intae Seo
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.37 no.2
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    • pp.195-201
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    • 2024
  • The low-temperature deposition of BaNi(2-x)CoxFe16O27 thin films with a Ba hexaferrite structure for electromagnetic shielding was studied. The BaNi(2-x)CoxFe16O27 thin films produced through the spin spray process were suitable for thin film deposition on a flexible substrate because it crystallized well at low temperature below 90℃. The change in shielding characteristics depending on the Co content of the BaNi(2-x)CoxFe16O27 thin film was investigated, and excellent shielding characteristics with S21 of -1 dB were obtained in a wide frequency range of 26~40 GHz when the Co content was 0.4 or more. The purpose of this study is to analyze changes in shielding properties caused by change in Co content in relation to phase changes in BaNi(2-x)CoxFe16O27 and obtain basic data for developing excellent flexible electromagnetic wave shielding materials.

Temperature Control of Injection Molding Machine using PI Controller with Input Restriction (PI 제어기의 입력제한을 이용한 사출 성형기 온도제어)

  • Jang, Yu-Jin
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.56 no.3
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    • pp.604-610
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    • 2007
  • Injection molding is the most common method of shaping plastic resins for manufacturing a variety of parts. This injection molding is accomplished by injection molding machines (IMM) which consists of a hewer, a reciprocating screw, barrel assembly, and an injection nozzle. The plastic resin is fed to the machine through the hopper and it should be heated to the target melting temperature, which depends on material properties, as closely as possible with very small temperature overshoot in the barrel. Since the barrel, which has temperature dependent specific heat and thermal conductivity in the operating temperature range, is heated by the several electric heater bands, it is not an easy task to control the temperature of the barrel owing to the interference of neighboring heaters and its material properties. Though PID controller with auto-tuning capability is widely adopted in the nm, the auto-tuning process should be carried out whenever the operating temperature is changed significantly. Recently, though the predictive controller is developed and shows good performance, it has drawbacks: 1. Since the heat transfer modeling process is very complicated and should be carried out again when the barrel is changed, it is somewhat inappropriate in the field. 2. The controller performance is not validated in whole operating temperature range. In this paper, cascade type simple PI controller with input restriction is proposed to find the possibility of controlling the barrel temperature in the whole operating temperature range. It is shown by experiment that the proposed controller shows good performance. This result can be applied to design of PI controller with auto-tuning capability.