• Title/Summary/Keyword: Inter-laboratory comparison

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Inter-laboratory Comparison of Stable Carbon and Nitrogen Isotopic Composition Data Using Elemental Analyzer-isotope Ratio Mass Spectrometers

  • Kim, Jung-Hyun;Kang, Sujin;Bong, Yeon-Sik;Park, Kwangkyu;Kang, Tae-Woo;Park, Yong-Se;Kim, Dahae;Choi, Seunghyun;Joo, Young Ji;Choi, Bohyung;Nam, Seung-Il;Lee, Sang-Mo;Shin, Kyung-Hoon
    • Journal of Environmental Analysis, Health and Toxicology
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    • v.21 no.4
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    • pp.229-236
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    • 2018
  • In this study, inter-laboratory comparison was done using elemental analyzer-isotope ratio mass spectrometers (EA-IRMSs) to determine carbon and nitrogen contents as well as stable carbon and nitrogen isotopic compositions (${\delta}^{13}C$ and ${\delta}^{15}N$) of five environmental samples containing lake and marine sediments, higher plant leaves, and fish muscle, and one organic analytical standard (Protein (Casein) Standard OAS). Five national laboratories participated in this comparison study, and each laboratory analyzed all five samples and the analytical standard. Results showed that variations in total organic carbon (TOC) and total nitrogen (TN) contents as well as ${\delta}^{13}C_{TOC}$ and ${\delta}^{15}N_{TN}$ values among the laboratories were large compared to the analytical uncertainties. The results highlighted the inhomogeneity of the test samples and thus, the need to select suitable standard reference materials for future inter-laboratory studies. Further inter-laboratory comparison exercises could promote good measurement practices in the acquisition of stable carbon and nitrogen isotopic composition data.

Inter-comparison of temperature measurement capability using standard platinum resistance thermometers (표준백금저항온도계를 이용한 온도측정능력 상호비교)

  • Gam, K.S.;Kang, C.S.;Lee, Y.J.;Lee, K.B.;Kim, Y.G.;Park, S.N.
    • Journal of Sensor Science and Technology
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    • v.18 no.1
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    • pp.86-94
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    • 2009
  • Temperature measurement capability was inter-compared using the transfer standard platinum resistance thermometers(SPRT) among four laboratories of KRISS. The transfer SPRTs were primarily calibrated at the triple point of water and Ga melting point, then used at inter-comparison experiment. Temperature difference of calibration value between temperature laboratory and length laboratory at $20^{\circ}C$ was -0.7 mK and +2.4 mK at density laboratory. Temperature measured near $20^{\circ}C$, $25^{\circ}C$ and $30^{\circ}C$ at fluid flow laboratory was deviated by $34.2{\sim}80.4\;mK$ from the calibration values of the transfer SPRT. Ga melting points was inter-compared among three laboratories, and the difference of Ga melting points against the standard Ga melting point of temperature laboratory were $0.03{\sim}0.54\;mK$ at length laboratory and 0.02 mK at density laboratory.

Reference dosimetry for inter-laboratory comparison on retrospective dosimetry techniques in realistic field irradiation experiment using 192Ir

  • Choi, Yoomi;Kim, Hyoungtaek;Kim, Min Chae;Yu, Hyungjoon;Lee, Hyunseok;Lee, Jeong Tae;Lee, Hanjin;Kim, Young-su;Kim, Han Sung;Lee, Jungil
    • Nuclear Engineering and Technology
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    • v.54 no.7
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    • pp.2599-2605
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    • 2022
  • The Korea Retrospective Dosimetry network (KREDOS) performed an inter-laboratory comparison to confirm the harmonization and reliability of the results of retrospective dosimetry using mobile phone. The mobile phones were exposed to 192Ir while attached to the human phantoms in the field experiment, and the exposure doses read by each laboratory were compared. This paper describes the reference dosimetry performed to present the reference values for inter-comparison and to obtain additional information about the dose distribution. Reference dosimetry included both measurement using LiF:Mg,Cu,Si and calculation via MCNP simulation to allow a comparison of doses obtained with the two different methodologies. When irradiating the phones, LiF elements were attached to the phones and phantoms and irradiated at the same time. The comparison results for the front of the phantoms were in good agreement, with an average relative difference of about 10%, while an average of about 16% relative difference occurred for the back and side of the phantom. The differences were attributed to the different characteristics of the physical and simulated phantoms, such as anatomical structure and constituent materials. Nevertheless, there was about 4% of under-estimation compared to measurements in the overall linear fitting, indicating the calculations were well matched to the measurements.

Damping of Inter-Area Low Frequency Oscillation Using an Adaptive Wide-Area Damping Controller

  • Yao, Wei;Jiang, L.;Fang, Jiakun;Wen, Jinyu;Wang, Shaorong
    • Journal of Electrical Engineering and Technology
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    • v.9 no.1
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    • pp.27-36
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    • 2014
  • This paper presents an adaptive wide-area damping controller (WADC) based on generalized predictive control (GPC) and model identification for damping the inter-area low frequency oscillations in large-scale inter-connected power system. A recursive least-squares algorithm (RLSA) with a varying forgetting factor is applied to identify online the reduced-order linearlized model which contains dominant inter-area low frequency oscillations. Based on this linearlized model, the generalized predictive control scheme considering control output constraints is employed to obtain the optimal control signal in each sampling interval. Case studies are undertaken on a two-area four-machine power system and the New England 10-machine 39-bus power system, respectively. Simulation results show that the proposed adaptive WADC not only can damp the inter-area oscillations effectively under a wide range of operation conditions and different disturbances, but also has better robustness against to the time delay existing in the remote signals. The comparison studies with the conventional lead-lag WADC are also provided.

A Study on Comparison Test of Disk Brake Lining for Rolling Stock (KRRI -CARS) (철도차량용 디스크 브레이크 라이닝의비교시험 연구)

  • Houg Yong-Ki;Kwon Sung-Tae;Chung Jong-Duk;Kim Jung-Nam
    • Proceedings of the KSR Conference
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    • 2004.10a
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    • pp.483-488
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    • 2004
  • The inter-laboratory comparison test which is demanded on the authorized test of ISO/IEC 17025 is the program to guarantee the confidence of test result. This paper, as a part of the inter-laboratory comparison test between South Korea and China, is refered to the characteristic of friction coefficient of disk brake lining for rolling stock according to disk type. Brake tests were carried out under constant brake force and operating sequence by using dynamo-tester according to disk and disk lining types. To establishing the confidence of test result, we calculated A type uncertainty about friction coefficient and investigated the factors about the variation of friction coefficient.

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Proficiency Testing by Inter-Laboratory Comparisons for Braking Lining (제동 라이닝애 대한 시험소간 비교에 의한 숙련도시험)

  • Chung Jong-Duk;Kwon Sung-Tae;Hong Yung-Ki;Kim Won-kyung
    • Proceedings of the KSR Conference
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    • 2003.05a
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    • pp.586-591
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    • 2003
  • This paper describes the result of proficiency testing by inter-laboratory comparisons for braking lining. Proficiency testing provides an objective means of assessing and demonstrating the validity and reliability of test results produced by laboratories. To more accuracy comparison test for braking lining test, they will be made the same test procedure and environment conditions.

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Inter-laboratory Comparison for Analyses of Heavy Metals and Organic Solvent Metabolites in Biological Samples (생체시료 중 중금속 및 유기용제 대사물 분석의 실험실간 정도관리 프로그램)

  • Yang, Jeong Sun;Lee, Mi Young;Park, In Jeong;Kang, Seong-Kyu
    • Analytical Science and Technology
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    • v.13 no.2
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    • pp.258-267
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    • 2000
  • The result of five year's experience on Inter-laboratory Comparison for Analyses of Heavy Metals and Organic Solvent Metabolites in Biological Samples was described. Since 1995, around a hundred laboratories in the Occupational Health have participated this program twice per year by the Industrial Safety and Health Law. Four metals in blood and five organic solvent metabolites in urine were examined. Reference samples were made by spiking standard materials to human blood or urine pools treated previously to give homogeneity and stability for a specific time periods. Some reference samples for organic solvent metabolites were made from workers' urine who were exposed to the organic solvents. Some items such as Lead in blood and Hippuric acid in urine showed good accordance between participants while the other items such as Mercury and N-methylformamide in urine showed poor proficient rate. The results were published in the internet or newspaper to help the consumer of the laboratory's service to get the information on them and to make competition between them. The inter-laboratory's comparison program have done greate role to improve the ability of analysis and reliability of analytical data produced from each laboratory.

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Summary of 2014 JCOMM Pilot Inter-Comparison Project for Seawater Salinity Measurements (2014년 JCOMM 해수 염분 측정 국제 상호비교실험 결과 보고)

  • Lee, Jung-Han;Kim, Eun-Soo;Lee, Yong-Kuk
    • Ocean and Polar Research
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    • v.38 no.3
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    • pp.247-257
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    • 2016
  • The inter-comparison project for seawater salinity measurements, in which 25 laboratories from 16 countries took part, was conducted by JCOMM (Joint WMO/IOC Technical Commission for Oceanography and Marine Meteorology) for the first time in 2014. Two seawater samples of different salinity values ranging from 30-35 and 20-25 for Sample A and Sample B respectively and which had sufficient homogeneity and stability were distributed to all participants. Participants measured the salinity in their own laboratories at least 3 times and reported the results. Statistical treatments were applied to the results to assess discrepancies among laboratories. 20 out of the 25 laboratories used laboratory salinometers and statistics for this group were denoted as belonging to group ${\alpha}$; while 5 out of the 25 laboratories used hand-held measuring instruments and statistics for this group were denoted as belonging to group ${\beta}$. Bias described as discrepancy among laboratories in group ${\alpha}$ was within ${\pm}0.001$ and expanded uncertainty (k = 2) was in the vicinity of 0.002. The bias and the uncertainty of Korea Institute of Ocean Science and Technology (KIOST), in group ${\alpha}$, were 0.000 and 0.002, respectively. The biases of group ${\beta}$ were greater than group ${\alpha}$ because of constraints related to instrument accuracy. Biases from 3 laboratories in group ${\beta}$ exceed the accuracy specification of the corresponding instruments. Considering that the uncertainty of Standard Seawater (SSW) is of the order 0.001 to 0.002, the inter-comparison results show that 16 laboratories among the 25 laboratories made high quality measurements, largely indistinguishable from one another.

Linear versus Non-linear Interference Cancellation

  • Buehrer, R.Michael;Nicoloso, Steven P.;Gollamudi, Sridhar
    • Journal of Communications and Networks
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    • v.1 no.2
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    • pp.118-133
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    • 1999
  • In this paper we compare linear and non-linear inter-ference cancellation for systems employing code division multi-ple access (CDMA) techniques. Specifically, we examine linear and non-linear parallel interference cancellation(also called multi-stage cancellation) in relationship to other multiuser detection al-gorithms. We show the explicit relationship between parallel inter-ference cancellation and the decorrelator (or direct matrix inver-sion). This comparison gives insight into the performance of paral-lel interference cancellation (PIC) and leads to vetter approaches. We also show that non-linear PIC approaches with explicit chan-nel setimation can provide performance improvement over linear PIC, especially when using soft non-linear symbol estimates. The application of interference cancellation to non-linear modulation techniques is also presented along with a discussion on minimum mean-squared error(MMSE) symbol estimation techniques. These are shown to further improve the performance of parallel cancella-tion.

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The generation of cloud drift winds and inter comparison with radiosonde data

  • Lee, Yong-Seob;Chung, Hyo-Sang;Ahn, Myeung-Hwan;Park, Eun-Jung
    • Proceedings of the KSRS Conference
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    • 1999.11a
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    • pp.135-139
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    • 1999
  • Wind velocity is one of the primary variables for describing atmospheric state from GMS-5. And its accurate depiction is essential for operational weather forecasting and for initialization of NWP(Numerical Weather Prediction) models. The aim of this research is to incorporate imagery from other available spectral channels and examine the error characteristics of winds derived from these images. Multi spectral imagery from GMS-5 was used for this purpose and applied to Korean region with together BoM(Bureau of Meteorology). The derivation of wind velocity estimates from low and high resolution visible, split window infrared, and water vapor images, resulted in improvements in the amount and quality of wind data available for forecasting.

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