• 한국전기전자재료학회논문지
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• 제25권8호
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• pp.593-601
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• 2012

Ordered mesoporous oxide films have been focused because of their low density, high interior specific surface area, and high thermal insulation. Specially, the ordered mesoporous oxide films prepared by self-assembly has many advantages due to easy process and high reproducibility. In this work, ordered mesoporous $SiO_2$, $Al_2O_3$, and $TiO_2$ films were synthesized by control of composition and processing parameter. Also, their structural, thermal, and mechanical properties were characterized variously. In conclusion, ordered mesoporous oxides will be one of core materials in new technology due to their excellent and unique properties.

• 청정기술
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• 제11권3호
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• pp.153-164
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• 2005

This study found a reliable evaluation for four kinds of pb-Free plating solutions and it's layers, through pure Sn, SnAg, SnBi and SnCu. These four kind of solutions are widely used to pb-Free plating. Hull-cell, Harring-blum, coverage, throwing power, current efficiency, stability, life-time, composition, hardness, roughness, abrasion, scratch, solderability, corrosion, contact angle, morphology, SIR(Surface insulation resistance) and Whisker test were experimented. Also, Using ICP, XRF, FE-SEM, EDS, temperature/humidity chamber, solderability tester, hardness tester, roughness tester, abrasion tester, salt spray tester, contact angle tester, SIR tester, and microscope. In this paper could be shown the systematic and various analysis for reliability about four kinds of pb-Free plating solutions, processes and it's deposit surface.

• 한국소음진동공학회:학술대회논문집
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• 한국소음진동공학회 2002년도 춘계학술대회논문집
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• pp.190-195
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• 2002

The intermittent high vibration has been occurred one or two times a day for a 500MW large steam turbine during 5 months. This abnormal vibration was caused by the rubbing between the rotor and the carbide accumulated on the seal tooth of oil deflector. It was found that the accumulated carbide was insulation material installed on the HIP casing from the examination of the chemical composition. Also, this paper presents the mechanism of the intermittent high vibration and the proper method to eliminate this vibration problem. This result would be good practice to find the solution of similar high vibration in the steam turbines for power plant as well as industrial rotating machineries.

• 한국표면공학회지
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• 제35권2호
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• pp.113-121
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• 2002

We have investigated insulating properties of $SiO_2$ interlayer for the thin film strain gauge, which were prepared by RF magnetron sputtering method in various deposition conditions, such as Ar pressure, gas flow rates and sputtering gases. SEM, AFM and FT-IR techniques were used to analyze its structures and composition. As the Ar pressure and the flow rate increased, the insulating interlayer showed low insulating resistance due to its porous structure and defects. Oxygen deficiency in $SiO_2$ was decreased as fabricated by hydrogen reactive sputtering. We could enhance the surface mobility of sputtered adatoms by using Ar/$H_2$ sputtering gas and obtain a good surface roughness and insulating property. The optimum insulating resistance of 9.22 G$\Omega$ was obtained in Ar/30% $H_2$ mixed gas, flow rate 10sccm, and 1mTorr.

• 한국전기전자재료학회논문지
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• 제13권2호
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• pp.177-182
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• 2000

Composite insulation system of liquid nitrogen and solid spacer is widely applied in high temperature superconduction power machine. This study has three step procedure. As follow, first step is composition of parallel deposited electrode and vertically deposited electrode along the direction of immersion in liquid nitrogen(LN2). Second step is investigation into surface flashover voltage of solid spacer under partially immersed in LN2, and last step is comparison the result of this research with that of fully immersed in LN2 and at cryogenic temperature gaseous nitrogen(GN2). This result presented that surface flashover voltage along solid spacer half immersed in LN2 was almost the same as that of fully immersed spacer when the thickness of spacer(t) was t<10mm. In the case of t> 10mm, however, spacer flashover voltage was equal to that obtained in GN2 at cryogenic temperature. And the immersed direction functions as role of deciding the difference of surface flashover voltage.

• 한국소음진동공학회논문집
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• 제12권11호
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• pp.897-903
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• 2002

The periodic high vibration has been occurred one or two times a day for a 500 MW large steam turbine during 5 months. This abnormal vibration was caused by the rubbing between the rotor and the carbide accumulated on the seal tooth of oil deflector. It was found that the accumulated carbide was insulation material installed on the HIP casing from the examination of the chemical composition. Also, this paper presents the mechanism of the periodic high vibration and the proper method to eliminate this vibration problem. This result would be good practice to find the solution of similar high vibration in the steam turbines for power plant as well as industrial rotating machineries.

• Asian-Australasian Journal of Animal Sciences
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• 제27권7호
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• pp.1050-1056
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• 2014

This study investigated the main factors influencing digester temperature and methods to reduce heat losses during the cold season in the subtropics. Four composite digesters (two insulated and two uninsulated) were buried underground to measure their internal temperature ($^{\circ}C$) at a depth of 140 cm and 180 cm, biogas production and methane ($CH_4$) concentration in biogas from August to February. In parallel the temperature of the air (100 cm above ground), in the slurry mixing tank and in the soil (10, 100, 140, and 180 cm depth) was measured by thermocouple. The influent amount was measured daily and the influent chemical composition was measured monthly during the whole experimental period. Seasonal variations in air temperature significantly affected the temperature in the soil, mixing tank and digester. Consequently, biogas production, which is temperature dependent, was influenced by the season. The main factors determining the internal temperature in the digesters were insulation with Styrofoam, air temperature and temperature of slurry in the mixing tank. Biogas production is low due to the cold climate conditions in winter in Northern Vietnam, but the study proved that storing slurry in the mixing tank until its temperature peak at around 14:00 h will increase the temperature in the digester and thus increase potential biogas production. Algorithms are provided linking digester temperature to the temperature of slurry in the mixing tank.

• 한국재료학회:학술대회논문집
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• 한국재료학회 2010년도 춘계학술발표대회
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• pp.48.2-48.2
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• 2010

The effect of additives as rare-earth in dielectric materials has been studied to meet the development trend in electronics on the miniaturization with increasing the capacitance of MLCCs (multi-layered ceramic capacitors). It was reported that the addition of rare-earth oxides in dielectrics would contribute to enhance dielectric properties and high temperature stability. Especially, dysprosium and thulium are well known to the representative elements functioned as selective substitution in barium titanate with perovskite structure. The effects of these additives on microstructure and electric properties were studied. The 0.8 mol% Dy doped $BaTiO_3$ and the 1.0 mol% Tm doped $BaTiO_3$ had the highest electric properties as optimized composition, respectively. According to the increase of rare-earth contents, the growth of abnormal grains was suppressed and pyrochlore phase was formed in more than solubility limits. Furthermore, the effect of two rare-earth elements co-doped $BaTiO_3$ on the dielectric properties and insulation resistance was investigated with different concentration. The dielectric specimens with $BaTiO_3-Dy_2O_3-Tm2O_3$ system were prepared by design of experiment for improving the electric properties and sintered at $1320^{\circ}C$ for 2h in a reducing atmosphere. The dielectric properties were evaluated from -55 to $125^{\circ}C$ (at $1KHz{\pm}10%$ and $1.0{\pm}0.2V$) and the insulation resistance was examined at 16V for 2 min. The morphology and crystallinity of the specimens were determined by microstructural and phase analysis.

• 한국신뢰성학회지:신뢰성응용연구
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• 제15권3호
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• pp.197-206
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• 2015

Failure analysis of pre-insulated pipe (SPPS 380, 400A) transporting high temperature water ($95{\sim}110^{\circ}C$) for a plant was carried out. The damaged area (${\Phi}5mm$) of pre-insulated pipe was found only on welds. The chemical composition of damaged pipe meets specification of carbon steel pipes for pressure service (KS D 3562). As results of microstructure analysis, crack propagated from outer to inside after pitting corrosion occurred on the outside surface. The non-metallic inclusion existed on the end of crack. And the non-metallic inclusion continuously and linearly formed along with the bond line of welds. Based on SEM-EDS analysis, the nonmetallic inclusions have higher Manganese (Mn) and Oxygen (O) content but sulfur (S) was not detected. As results of water quality analysis, hydrogen ion concentration and minerals like Fe, Mg, Si were in low level. But the content of dissolved oxygen (11.2 ppm) was slightly higher than that of standard. It seems that the cause of damaged pipe is grooving corrosion due to MnO inclusion formed on bond line and corrosion took place nearby welds.

• 자원리싸이클링
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• 제17권4호
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• pp.30-36
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• 2008

본 연구에서는 하수슬러지 소각재를 원료로 사용한 다공성 경량재료의 제조 및 물성측정 실험을 수행하였다. 경량충진재로써 perlite와 silica sphere의 2종류 경량물질을 각각 사용하였으며, 무기바인더로써 벤토나이트를 첨가하여 $1,000^{\circ}C$에서 소성하는 방법으로 경량재료를 제조하였다. 제조한 시편은 밀도, 압축강도, 열전도도 및 흡음율을 측정하여 원료 조성 및 제조 조건에 따른 각각의 물성변화를 조사하였다. 실험결과 perlite를 경량충진재로 사용한 시편의 밀도는 $1.23{\sim}1.37g/cm^3$, 압축강도는 $242.3{\sim}370.5kg/cm^2$로 나타났으며, silica sphere를 사용한 경우는 perlite에 비해 밀도가 낮고 압축강도가 $100kg/cm^2$ 이하인 것으로 나타났다. 또한, 경량재료의 열전도도는 원료 조성에 따라 $0.3{\sim}0.5W/m^{\circ}K$의 수치를 보여 일반 콘크리트보다 단열효과가 매우 우수한 것으로 나타났다.