• Title/Summary/Keyword: Infrared stress analysis

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Preparation and Characterization of Small Sized PZT Powders: A Sol-Gel Modified Approach

  • Choi, Kyu-Man;Lee, Hae-Chun
    • The Journal of Korea Institute of Information, Electronics, and Communication Technology
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    • v.1 no.2
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    • pp.27-32
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    • 2008
  • A current research basically diverted towards an increase in the operational output with the minimization of the materials used, which ultimately scaled down the dimensions of ceramic electronic components. In this direction the nano-technology pave the revolutionary changes in particular the electronic industries. The applications of nano-sized particles or nano-sized materials are hence, playing a significant role for various purposes. The PZT(lead, zirconium, titanium) based ceramics which, are reported to be ferroelectric materials have their important applications in the areas of surface acoustic waves (SAW), filters, infrared detectors, actuators, ferroelectric random access memory, speakers, electronic switches etc. Moreover, these PZT materials possess the large electro mechanical coupling factor, large spontaneous polarization, low dielectric loss and low internal stress etc. Hence, keeping in view the unique properties of PZT piezoelectric ceramics we also tried to synthesize indigenously the small sized PZT ceramic powder in the laboratory by using the modified sol-gel approach. In this paper, propyl alcohol based sol-gel method was used for preparation of PZT piezoelectric ceramic. The powder obtained by this sol-gel process was calcined and sintering to reach a pyrochlore-free crystal phase. The characterization of synthesized material was carried out by the XRD analysis and the surface morphology was determined by high resolution scanning electron microscopy.

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Synthesis and Properties of Bio-Thermoplastic Polyurethanes with Different Isocyanate Contents

  • Li, Xiang Xu;Sohn, Mi Hyun;Cho, Ur Ryong
    • Elastomers and Composites
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    • v.54 no.3
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    • pp.225-231
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    • 2019
  • Bio-based polyester polyol was synthesized via esterification between azelaic acid and isosorbide. After esterification, bio-based polyurethanes were synthesized using polyester polyol, 1,3-propanediol as the chain extender, and 4,4'-diphenylmethane diisocyanate, in mixing ratios of 1:1:1.5, 1:1:1.8, 1:1:2, and 1:1:2.3. The bio TPU (Thermoplastic Polyurethane) samples were characterized by using FT-IR (Fourier Transform Infrared Spectroscopy), TGA (Thermal Gravimetric Analysis), DSC (Differential Scanning Calorimetry), and GPC (Gel Permeation Chromatography). The mechanical properties (tensile stress and hardness) were obtained by using UTM, a Shore A tester, and a Taber abrasion tester. The viscoelastic properties were tested by an Rubber Processing Analyzer in dynamic strain sweep and dynamic frequency test modes. The chemical resistance was tested with methanol by using the swelling test method. Based on these results, the bio TPU synthesized with the ratio of 1:1:2.3, referred to as TPU 4, showed the highest thermal decomposition temperature, the largest molecular weight, and most compact matrix structure due to the highest ratio of the hard segment in the molecular structure. It also presented the highest tensile strength, the largest elongation, and the best viscoelastic properties among the different bio TPUs synthesized herein.

Scanning acoustic microscopy for material evaluation

  • Hyunung Yu
    • Applied Microscopy
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    • v.50
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    • pp.25.1-25.11
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    • 2020
  • Scanning acoustic microscopy (SAM) or Acoustic Micro Imaging (AMI) is a powerful, non-destructive technique that can detect hidden defects in elastic and biological samples as well as non-transparent hard materials. By monitoring the internal features of a sample in three-dimensional integration, this technique can efficiently find physical defects such as cracks, voids, and delamination with high sensitivity. In recent years, advanced techniques such as ultrasound impedance microscopy, ultrasound speed microscopy, and scanning acoustic gigahertz microscopy have been developed for applications in industries and in the medical field to provide additional information on the internal stress, viscoelastic, and anisotropic, or nonlinear properties. X-ray, magnetic resonance, and infrared techniques are the other competitive and widely used methods. However, they have their own advantages and limitations owing to their inherent properties such as different light sources and sensors. This paper provides an overview of the principle of SAM and presents a few results to demonstrate the applications of modern acoustic imaging technology. A variety of inspection modes, such as vertical, horizontal, and diagonal cross-sections have been presented by employing the focus pathway and image reconstruction algorithm. Images have been reconstructed from the reflected echoes resulting from the change in the acoustic impedance at the interface of the material layers or defects. The results described in this paper indicate that the novel acoustic technology can expand the scope of SAM as a versatile diagnostic tool requiring less time and having a high efficiency.

Short-term Variation of the Mixed Layer in the Korea Strait in Autumn (가을철 대한해협 표면혼합층의 단기변화)

  • Jang, Chan-Joo;Kim, Kuh;Shim, Tae-Bo
    • 한국해양학회지
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    • v.30 no.5
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    • pp.512-521
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    • 1995
  • To investigate a short-term (from 2 hours to 24 hours) variability of a mixed layer, oceanographical data (water temperature, salinity, current) and meteorological data (wind, air temperature, solar radiation) were collected at a site in the Korea Strait at the interval of one hour for 48 hours from October 12 to 14, 1993. The average rates of temporal variations of the mixed layer depth (MLD) and temperature of the mixed layer (MLT), which are very weakly correlated with the wind stress and buoyancy flux at the sea surface, are about 5.2 m/hour and 0.2$^{\circ}C$/hour, respectively. The mixed layer is relatively shallow when both MLT and MLS (salinity of the mixed layer) are low, while MLD is relatively deep when they are high. MLT shows a sudden decrease or increase. Analysis of satellite infrared images and XBT data shows that sudden increase of MLT is caused by advection of warm water. These results suggest that the short-term variation of the mixed layer in the Korea Strait in autumn, in which surface current is relatively strong and different water masses exist, is mainly determined by advection rather than air0sea interaction such as wind stress or buoyancy flux.

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Development of Prefabricated Slab Panel for Asphalt Concrete Track (아스팔트 콘크리트 궤도용 사전제작형 슬래브 패널 개발)

  • Baek, In-Hyuk;Lee, Seong-Hyeok;Shin, Eung-Soo
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.23 no.3
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    • pp.75-82
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    • 2019
  • Slab panels are very important to develop asphalt concrete (AC) track for minimizing the roadbed stress due to the train load and reducing the plastic deformation of infrared-sensitive AC. In this study, the slab panel for AC track was developed through the shape design and the indoor performance test and its structural integrity has been investigated through the finite element analysis under the flexural tensile stress and the design moment according to various static load combination by KRL-2012 standard train load model and KR-C code. In order to verify the suitability of the slab panel for AC track, static bending strength test and dynamic bending strength test were performed according to EN 13230-2. Results show that the slab panel for AC track satisfies all the performance standards required by European standards such as crack loads and crack extension.

The Deterioration Properties and Actual Conditions of Insulation Cover used at 22.9 kV Transformer Bushing (22.9 kV용 변압기 부싱 절연 커버의 실태 조사 및 열화 특성)

  • Choi, Chung-Seog;Kim, Hyang-Kon;Han, Woon-Ki;Lee, Ki-Yeon
    • Fire Science and Engineering
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    • v.20 no.3 s.63
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    • pp.35-41
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    • 2006
  • In this study, we presented the problems in the insulation cover of 22.9kV transformer bushing through investigating actual conditions. After thermal stress applied to the insulation cover, deterioration patterns, thermogravimetric and infrared characteristics were analyzed, and the results were applied to the cause analysis of accidents and judgement of safety. The insulation covers are used to protect exposed terminals of transformer, but they had improper size and length. Therefore, they could not show efficient insulation function. In case that thermal stress of $150^{\circ}C$ was applied to the insulation covers, plastic insulation covers(A, B, D, E) damaged severely, whereas rubber insulation cover(C) showed normal shapes. In the result of thermogravimetric analysis, the thermal gravity of plastic covers(A) decreased about 33.3% at $307.8^{\circ}C\;to\;405.9^{\circ}C$. and he thermal gravity of rubber covers (C) decreased about 53.7% at $258.8^{\circ}C\;to\;32.9^{\circ}C$. In the result of FT-IR analysis, plastic covers showed peaks characteristic of $CH_2,\;CH_3$, C=O and C=C bonds, whereas rubber covers showed peaks characteristic of OH, $CH_2,\;CH_3$, C=O, C=N and C=C bonds.

Convergence Technique Study through Simulation Thermal Analysis due to the Shape of Electric Heater (전기 히터의 형상에 따른 시뮬레이션 열 해석 연구를 통한 융합 기술 연구)

  • Lee, Jung-Ho;Cho, Jae-Ung
    • Journal of the Korea Convergence Society
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    • v.6 no.6
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    • pp.241-246
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    • 2015
  • In cold winter season, the apparatuses of heating and heater which warm up the interior of a room are necessary element and the used amount of these apparatuses from the year 2000 has been increased abruptly. But, the fire accident and the danger of fire are also increased. Therefore, 3D modelling is done by referring three kinds of the electric heaters as the heaters of ceramic, carbon and near infrared ray sold in the city for the design of more safe heating apparatuses in this study. The thermal analyses with these models are carried out and the durabilities due to the thermal deformation and stress are studied. By the background of the study results derived in this study ultimately, the durabilities of electric heater models due to each shape can be anticipated and contributed to the development of new heating apparatus with more safe resistance to fire. And it is possible to be grafted onto the convergence technique at design and show the esthetic sense.

Visual Analysis for Detection and Quantification of Pseudomonas cichorii Disease Severity in Tomato Plants

  • Rajendran, Dhinesh Kumar;Park, Eunsoo;Nagendran, Rajalingam;Hung, Nguyen Bao;Cho, Byoung-Kwan;Kim, Kyung-Hwan;Lee, Yong Hoon
    • The Plant Pathology Journal
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    • v.32 no.4
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    • pp.300-310
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    • 2016
  • Pathogen infection in plants induces complex responses ranging from gene expression to metabolic processes in infected plants. In spite of many studies on biotic stress-related changes in host plants, little is known about the metabolic and phenotypic responses of the host plants to Pseudomonas cichorii infection based on image-based analysis. To investigate alterations in tomato plants according to disease severity, we inoculated plants with different cell densities of P. cichorii using dipping and syringe infiltration methods. High-dose inocula (${\geq}10^6cfu/ml$) induced evident necrotic lesions within one day that corresponded to bacterial growth in the infected tissues. Among the chlorophyll fluorescence parameters analyzed, changes in quantum yield of PSII (${\Phi}PSII$) and non-photochemical quenching (NPQ) preceded the appearance of visible symptoms, but maximum quantum efficiency of PSII ($F_v/F_m$) was altered well after symptom development. Visible/near infrared and chlorophyll fluorescence hyperspectral images detected changes before symptom appearance at low-density inoculation. The results of this study indicate that the P. cichorii infection severity can be detected by chlorophyll fluorescence assay and hyperspectral images prior to the onset of visible symptoms, indicating the feasibility of early detection of diseases. However, to detect disease development by hyperspectral imaging, more detailed protocols and analyses are necessary. Taken together, change in chlorophyll fluorescence is a good parameter for early detection of P. cichorii infection in tomato plants. In addition, image-based visualization of infection severity before visual damage appearance will contribute to effective management of plant diseases.

The Comparison between Hot-Water Extracts and Microwave Extracts of Scutellaria radix for Antioxidant and Neuroprotective Effects (가열 추출법과 마이크로웨이브 추출법을 이용한 황금 물 추출물의 뇌세포 보호 및 항산화 효과 비교 연구)

  • Lee, Dong-Sung;Ko, Wonmin;Kim, Kyoung-Su;Kim, Dong-Cheol;Yoon, Chi-Su;Cho, Kwangho;Cui, Xiang;Oh, Hyuncheol;Kim, Youn-Chul
    • Korean Journal of Pharmacognosy
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    • v.45 no.1
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    • pp.55-61
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    • 2014
  • Microwaves are non-ionizing electromagnetic waves of frequency between 300MHz to 300GHz and positioned between the X-ray and infrared rays in the electromagnetic spectrum. In recent years, the use of microwave for extraction of ingredient from plant material has shown remarkable research interest and potential. Scutellaria radix has been used as a traditional medicine for a variety of diseases. It has been reported to exert beneficial health effects, such as anti-bacterial, antiviral, anti-inflammatory, and free-radical scavenging. Oxidative stress or the accumulation of reactive oxygen species (ROS) leads neuronal cellular death and dysfunction, and it contributes to neuronal degenerative disease such as Alzheimer's disease, Parkinson's disease and stroke. In this study, we aimed to compare the neuroprotective and antioxidant effect of Scutellaria radix extracted by different methods using hot-water extraction (SBE-DW) or microwave extraction (SBE-DW-MW). As a result, we first examined HPLC analysis of hot-water and microwave extracts of Scutellaria radix. The hot-water and microwave extracts of Scutellaria radix showed the discernible difference patterns of HPLC analysis. Microwave-water extracts of Scutellaria radix increased DPPH radical scavenging activity more than hot-water extraction. Microwave-water extracts of Scutellaria radix also showed neuroprotective effects and ROS inhibition against glutamate-induced oxidative stress in mouse hippocampal HT22 cells, but hot-water extraction not showed. In addition, the phosphorylation of MAPKs induced by glutamate insult was prevented by microwave-water extracts of Scutellaria radix. Thus, these results suggested that microwave extraction can be utilized for improving the extraction efficiency and biological activity of Scutellaria radix.

The Variation of Structure and Physical Properties of XLPE during Thermal Aging Process (가교 폴리에틸렌의 열노화에 따른 구조와 물성의 변화)

  • 이미영;김철환;구철수;김복렬;이영관
    • Polymer(Korea)
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    • v.27 no.3
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    • pp.249-254
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    • 2003
  • The variation of chemical structure and physical properties of crosslinked polyethylene (XLPE) during thermal aging process was investigated. The formation of carbonyl functional group resulting from thermal oxidation reaction of XLPE was monitored using X-ray photoelectron spectroscopy and near infrared (NIR) spectroscopy. It was observed that the intensity of carbonyl peak observed at 1715 nm linearly increased with aging time in NIR spectroscopy. The linear relationship between NIR peak absorbance and aging time confirmed that NIR spectroscopy might be used as a proper tool for monitoring the aging process of polymeric materials. Also the formation of crosslinks during the aging process was monitored using thermal mechanical analysis, stress-strain test, and Shore hardness test. The change in the physical properties, such as the increase in the glass transition temperature from 110 to 132$^{\circ}C$, the decrease in the strain from 265 to 110%, as well as the increase in the shore D hardness from 32 to 50, was observed during the aging process.