• Journal of the Computational Structural Engineering Institute of Korea
• /
• v.32 no.5
• /
• pp.273-278
• /
• 2019

In this study, a new simple method for the estimation of hyperelastic material properties by indentation tests is proposed. Among hyperelastic material models, the Yeoh model with three material properties ($C_{10}$, $C_{20}$, $C_{30}$) is adopted to describe the strain energy density in terms of strain invariants. Finite element simulations of the spherical indentation of hyperelastic materials of the Yeoh model with different material properties are performed to establish a database of indentation force-displacement curves. The indentation force-displacement curves are fitted by cubic polynomials, which are approximated as a product of third-order polynomials of ($C_{10}$, $C_{20}$, $C_{30}$). A regression analysis is conducted to determine the coefficients of the equations for the indentation force-displacement curve approximations. A regression equation is used to estimate the hyperelastic material properties. The present method is verified by comparing the estimated material properties with true values.

• Journal of the Computational Structural Engineering Institute of Korea
• /
• v.23 no.4
• /
• pp.353-360
• /
• 2010

In this paper, an efficient algorithm is established in order to estimate the plastic properties of power-law hardening bulk specimen materials with one simple spherical indentation impression test. This work is based on a new formulation of representative strain and, therefore, compare to the preceding approaches the fitting parameters are significantly reduced. Moreover, the new definition of representative strain endowed more physical meaning to the representative strain. In order to verify the reliability of the reverse analysis, we have studied a broad set of materials whose property ranges cover essentially all engineering metals and alloys. Based on the indentation force-displacement P-${\delta}$ curves obtained from numerical simulations, the characteristics of the indentation response and material elastoplastic properties are bridged via explicit functions. Next, through the procedure of reverse analysis the yield stress and power-law hardening exponent of bulk specimen materials can be determined. Finally, good agreement between the result from reverse analysis and initial input data from experiment can be observed.

• Proceedings of the Korean Society of Precision Engineering Conference
• /
• 2006.05a
• /
• pp.527-528
• /
• 2006

In the proposed research plan, the effects of anisotropic and time-dependent mechanical properties on nanoindentation measurements of osteonic lamellae in a human cortical bone are investigated. The most popular method(Oliver-Pharr method) in nanoindentation data analysis is based on the assumption of elastic isotropy. Since cortical bone has exhibited anisotropy, it is necessary to consider the effects of anisotropy on nanoindentation measurement for cortical bone. By comparison with the contact area obtained from monitoring the contact profile in FEA simulations, the Oliver-Pharr method was found to underpredict or overpredict the contact area due to effects of anisotropy. The mount of error depended on the indentation orientation. The indentation modulus results and were also similar to moduli calculated from mathematical model. The Oliver-Pharr method has been shown to be useful for providing first order approximations in analysis of anisotropic mechanical properties of cortical bone, although the indentation modulus is influenced by anisotropy.

• Journal of Welding and Joining
• /
• v.31 no.5
• /
• pp.41-46
• /
• 2013

Different microstructures in the weld zone of a metal structure such as a fusion zone or heat affected zone are formed as compared to the parent material. Thus, the mechanical properties in the weld zone are different from those in the parent material. As the basic data for reliably understanding the structural characteristics of a welded PCHE specimen to be made of Alloy 617, the mechanical properties in the weld zone and parent material for a Alloy 617 plate are measured using an instrumented indentation technique in this study.

• Journal of Welding and Joining
• /
• v.31 no.2
• /
• pp.37-42
• /
• 2013

Different microstructures in the weld zone of a metal structure such as a fusion zone or heat affected zone are formed as compared to the parent material. Thus, the mechanical properties in the weld zone are different from those in the parent material. As the basic data for reliably understanding the structural characteristics of welded PCHE prototype made of SUS316L, the mechanical properties in the weld zone and parent material for a SUS316L plate are measured using an the instrumented indentation technique in this study.

• Journal of Powder Materials
• /
• v.5 no.1
• /
• pp.22-27
• /
• 1998

The effect of the $\alpha$/$\beta$ phase fraction on the mechanical properties in silicon nitrides was investigated in part 1. In part II, we describe the role of microstructure on the mechanical properties and contact damage of silicon nitrides with coarse/equiaxed and coarse/elongated microstructures. Grain sizes and shapes were controlled by starting powder. Hertzian indentation using spherical indenter was also used to investigate contact damage behavior. Cone cracks from the spherical indentation were suppressed when the silicon nitride contains coarse and elongated grains. Coarse and elongated grains played an important role of cone crack suppression. The size of quasi-plastic zone does not depend on grain size or shape but depends on the fraction of $\alpha$/$\beta$ phase. A quasi-plastic zone was consisting of microcracks by shear stress during indentation.

• Journal of Welding and Joining
• /
• v.30 no.3
• /
• pp.51-56
• /
• 2012

Different microstructures in the weld zone of a metal structure including a fusion zone and heat affected zone are formed as compared to the base material. Thus, the mechanical properties in the weld zone are different from those in the base material. As the basic data for reliably understanding the structural characteristics of welded nuclear material, the mechanical properties in the weld zone and base material for a Zircaloy-4 strap and Hastelloy${(R)}$-X alloy strap are measured using an instrumented indentation technique (IIT) in this study.

• Proceedings of the KSME Conference
• /
• 2007.05a
• /
• pp.1367-1372
• /
• 2007

Over the past decade, many computational researches have been performed to investigate quantitative relationships between load-displacement and material properties. But piling-up which causes errors to estimate mechanical material properties remains the most significant unresolved issue in nano-indentation test. This study has estimated quantitative aspects of the effects of material properties, especially work hardening exponent, on piling up/sinking in response of various materials. Using FE Analysis, piling up/sinking in response when material is indented by sharp indenter is investigated to evaluate the effects of material properties. From the FE analysis result, quantitative relationships between piling up/sinking in height and material properties is assessed using dimensional analysis which is used to define scaling variables and universal functions. And nano-indentaion test is performed to verify this relation on various materials. From the result of comparison with prediction from dimensional function and experiment, the work hardening exponent was found to have greater influence on the piling up/sinking in height during the nano-indentation than other material properties, such as elastic modulus and yield stress.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.39 no.11
• /
• pp.1079-1089
• /
• 2015

In this paper, we propose a method to evaluate the material properties of high-yield strength materials exceeding 10GPa from spherical indentation. Using a regression equation considering four indentation variables, we map the load displacement relation into a stress-strain relation. To calculate the properties of high-strength materials, we then write a program that produces material properties using the loading / unloading data from the indentation test. The errors in material properties computed by the program are within 0.3, 0.8, and 6.4 for the elastic modulus, yield strength, and hardening coefficient, respectively.

• Advances in nano research
• /
• v.15 no.4
• /
• pp.315-328
• /
• 2023

The main goal of the present study was to assess the effects of eggshell powder (ESP) and halloysite nanotubes (HNTs) on the mechanical properties of abaca fiber (AF)-reinforced natural composites. For this purpose, a limited number of indentation tests were first performed on the AF/polypropylene (PP) composites for different HNT and ESP loadings (0 wt.% ~ 6 wt.%), load amplitudes (150, 200, and 250 N), and two types of indenters (Vickers or conical). The Young's modulus, hardness and plasticity index of each specimen were calculated using the indentation test results and Oliver-Pharr method. The accuracy of the experimental results was confirmed by comparing the values of the Young's modulus obtained from the indentation test with the results of the conventional tensile test. Then, a feed-forward shallow artificial neural network (ANN) with high efficiency was trained based on the obtained experimental data. The trained ANN could properly predict the variations of the mentioned mechanical properties of AF/PP composites incorporated with different HNT and ESP loadings. Furthermore, the trained ANN demonstrated that HNTs increase the elastic modulus and hardness of the composite, while the incorporation of ESP reduces these properties. For instance, the Young's modulus of composites incorporated with 3 wt.% of ESP decreased by 30.7% compared with the pure composite, while increasing the weight fraction of ESP up to 6% decreased the Young's modulus by 34.8%. Moreover, the trained ANN indicated that HNTs have a more significant effect on reducing the plasticity index than ESP.