• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2004년도 춘계학술대회 논문집
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• pp.148-151
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• 2004

Mechanical properties such as Young's modulus and hardness of thin film in coated steel are difficult to determine by nano-indentation from the conventional analysis using the load-displacement curve. Therefore, an analysis of the nano-indentation loading curve was used to determine the Young's modulus, hardness and strain hardening exponent. A new method is recently being developed for plasticity properties of materials from nano-indentation. Elastic modulus of the thin films shows relatively small influence whereas yield strength and strain hardening are found to have significant effect on measured data. The load-displacement behavior of material tested with a Berkovich indenter and nano-indentation continuous stiffness method is used to measure the modulus and hardness through thin films.

• 소성∙가공
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• 제13권8호
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• pp.731-737
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• 2004

Mechanical properties such as Young's modulus and hardness of thin film in coated steel are difficult to determine by nano-indentation from the conventional analysis using the load-displacement curve. Therefore, an analysis of the nano-indentation loading-unloading curve was used to determine the Young's modulus, hardness. A new method is recently being developed for elastic-plastic properties of materials from nano-indentation. Elastic modulus of the thin films shows relatively small influence whereas yield strength is found to have significant effect on measured data. The load-displacement curves of material tested with a Berkovich indenter and nano-indentation continuous stiffness method is used to measure the modulus and hardness through thin films, and then these are computed using the analysis procedure. The developed neural networks apply also to obtain reliable mechanical properties.

• 대한기계학회논문집A
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• 제38권9호
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• pp.943-951
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• 2014

마이크로/나노 압입시험에 사용되는 각뿔 혹은 원뿔형 압입자의 선단 형상은 제작한계 및 사용 중 마모 등으로 인해 필수적으로 곡면 형태를 띄게 된다. 많은 압입시험 관련 연구에서 각뿔형 압입자의 선단 형상은 편의상 구형으로 가정한 후, 얕은 압입에 대한 구형압입 이론식을 적용하고 있다. 이러한 가정에는 근본적으로 두 가지 문제점이 있는데, 첫 번째로 이론해의 정확성은 재료 물성치 및 압입자 형상에 따라 변화한다는 점이며, 두 번째로 각뿔형 압입자의 실제 선단 형상은 이상적인 구형이 아니라는 점이다. 본 연구에서는 유한요소해석에 기반하여 압입시험에 미치는 이 두 요소의 영향을 분석한다. 먼저 탄성 구형 압입시험에 대해 푸아송비와 하중-변위 곡선의 상관관계를 살펴보고, 이를 기반으로 수정된 구형 탄성 압입 관계식을 제시한다. 이어 가정된 Berkovich 선단 형상의 3차원 유한요소해석으로부터 압입깊이에 따른 하중-변위 곡선의 특성을 분석한다.

• 한국정밀공학회지
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• 제22권10호
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• pp.186-194
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• 2005

This study was designed to investigate the mechanical properties of the coating layer on electronic galvanized sheet steel as a part of the ongoing research on the coated steel. Those properties were determined using nano-indentation, the finite element method, and artificial neural networks. First and foremost, the load-displacement curve (the loading-unloading curve) of coatings was derived from a nano-indentation test by CSM (continuous stiffness measurement) and was used to measure the elastic modulus and hardness of the coating layer. The properties derived were applied in FE simulations of a nano-indentation test, and the analytical results were compared with the experimental result. A numerical model for FE simulations was established for the coating layer and the substrate separately. Finally, to determine the mechanical properties of the coating, such as the stress-strain curve, functional equations of loading and unloading curves were introduced and computed using the neural networks method. The results show errors within $5\%$ in comparison with the load-displacement measured by a nano-indentation test.

• 한국세라믹학회지
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• 제48권4호
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• pp.288-292
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• 2011

In this study, we investigated the mechanical behavior of carbon fiber reinforced silicon carbide composites by indentation stress. Relatively porous and dense fiber reinforced ceramic composites were fabricated by liquid silicon infiltration (LSI) process. Densification of fiber composite was controlled by hardening temperature of preform and consecutive LSI process. Load-displacement curves were obtained during indentation of WC sphere on the carbon fiber reinforced silicon carbide composites. The indentation damages at various loads were observed, and the elastic modulus were predicted from unloading curve of load-displacement curve.

• 한국정밀공학회지
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• 제20권12호
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• pp.64-72
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• 2003

This paper presents a small loading and positioning device using VCM (voice coil motor). The developed device consists of a VCM-based linear actuating system, a capacitance displacement sensor and a cantilever deflection sensing system. The trust force of the VCM proportional to applied current moves the column supported on two pairs of parallel leaf springs. The infinitesimal displacement of moved column is detected by capacitance displacement sensor with a resolution of 0.1nm and a repeatability of 1nm. Also, a micro cantilever with known stiffness (200N/m), which is mounted on the end of the column, is used as a force sensor to detect the load applied to a specimen. After the cantilever contacts with the specimen, the deflection of cantilever and the load applied to the specimen are measured by using an optical lever system which consists of a diode laser, a mirror and a PSD (position sensitive detector). In this paper, an experimental system was constructed and its actuator and sensing parts were tested and calibrated. Also, the constructed system was applied to the indentation experiment and the load-displacement curve of aluminum was obtained. Experimental results showed that the developed device can be applied for performing nano indentation.

• 한국세라믹학회지
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• 제40권7호
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• pp.667-671
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• 2003

테이프 캐스팅법을 이용하여 알루미나/지르콘(반응결합 뮬라이트/지르코니아 유도)을 내부층으로 하고 알루미나/지르코니아 혹은 뮬라이트/지르코니아를 외부층으로 하는 산화물 층상 복합체를 고온가압소결법으로 제조하였다. 나노압입시험법을 이용하여 층상 산화물 복합체의 기계적 성질(경도 및 탄성계수)을 측정하고, SEM을 통하여 복합체의 미세구조를 관찰하였다. 산화물 층상 복합체의 제조를 위한 가열·냉각시 유도된 구성 산화물간의 열팽창 계수의 차이로 인하여 생성된 잔류응력을 하중-변위곡선을 이용하여 확인할 수 있었다.

• 한국세라믹학회지
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• 제48권5호
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• pp.396-403
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• 2011

In this study, we investigated the mechanical behaviors of layered thermal barrier coatings by indentations. Various single and double-layered thermal barrier coatings were deposited by air plasma spray process using different type of commercialized YSZ (Yttria stabilized zirconia) starting powders. Indentation stress-strain curve, load-displacement curve and hardness of the single and the double-layered thermal barrier coatings were obtained experimentally and analyzed. The indentation damages at the same loads were compared, and thus, the results depend on the structure of each coating. The result indicates improvement in damage resistances from tailoring of layered structures in the component of gas turbine system is expected.

• 한국정밀공학회지
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• 제22권10호
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• pp.167-173
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• 2005

The Berkovich nano-indentation is an indentation test method analyzing mechanical properties of materials such as hardness and elastic modulus. The length scale of the penetration is measured in nanometers. Therefore, this method becomes widely useful for analyzing the mechanical property of thin film which can not be measured before. In this paper, comparing two results of the load-displacement curve obtained by the Berkovich nano-indentation and the 3-D finite element analysis, it was confirmed that the 3-D finite element analysis is useful. The phenomenon of pile-up and sink-in due to material properties was discussed by the finite element analysis.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2001년도 추계학술대회논문집A
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• pp.204-209
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• 2001

In this research, the effects of fiber stacking sequence on damage behaviors of FML(Fiber Metal Laminates) subject to indentation loading. SOP (Singly Oriented Ply) FML and angle ply FML were fabricated to study fiber orientation effects and angle ply effects. FML were fabricated by using 1050 aluminum laminate and carbon/epoxy prepreg. To increase adhesive bonding strength, Al laminate was etched using FPL methods. The static indentation test were conducted by using UTM(5ton, Shimadzu) under the 2side clamped conditions. During the tests, load and displacement curve and crack initiation and propagation behaviors were investigated. As fiber orientation angle increases, the crack initiation load of SOP FML increases because the stiffness induced by fiber orientation is increased. The penetration load of SOP FML is influenced by the deformation tendency and boundary conditions. However, the macro-crack of angle ply FML was initiated by fiber breakage of lower ply because angle plies in Angle ply FML prevents the crack growth and consolidation. The Angle ply FML has a critical cross-angle which prevent crack growth and consolidation. Damage behavior of Angle ply FML is changed around the critical cross-angle.