• Title/Summary/Keyword: Indentation Test

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Mechanical Characterization of Elastomeric Polymer Through Micro Instrumented Indentation Technique (마이크로 압입시험기법의 응용을 통한 탄성체 고분자 소재의 역학적 특성화 및 계면 접합에너지 평가기법 연구)

  • Lee, Gyu-Jei;Kang, Seung-Kyun;Kang, In-Geun;Kwon, Dong-Il
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.31 no.9
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    • pp.951-959
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    • 2007
  • In this study, the Johnson-Kendall-Roberts(JKR) theory was combined with the instrumented indentation technique (IIT) to evaluate work of adhesion and modulus of elastomeric polymer. Indentation test was used to obtain the load-displacement data for contacts between Tungsten Carbide indenter and elastomeric polymer. And the JKR contact model, contrived to take viscoelastic effects of polymer into account, was applied to compensate the contact area and the elastic modulus which Hertzian contact model would underestimate and overestimate, respectively. Besides, we could obtain the thermodynamic work of adhesion by considering the surface energy in this contact model. In order to define the relation between JKR contact area and applied load without optical measuring of contact area, we used the relation between applied load and contact stiffness by examining the correlation between JKR contact area and stiffness through dimensional analysis with 14 kinds of elastomeric polymer. From this work, it could be demonstrated that the interfacial work of adhesion and elastic modulus of compliant polymer can be obtained from a simple instrumented indentation testing without area measurement, and provided as the main algorithm of compliant polymer characterization.

Advanced Indentation Studies on the Effects of Hydrogen Attack on Tensile Property Degradation of Heat-Resistant Steel Heat-Affected Zones

  • Choi, Yeol;Jang, Jae-il;Lee, Yun-Hee;Kwon, Dongil;Kim, Jeong-Tae
    • Corrosion Science and Technology
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    • v.2 no.6
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    • pp.266-271
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    • 2003
  • Safety diagnosis of various structural components and facilities is indispensable for preventing catastrophic failure of material by time-dependent and environment accelerating degradation. Also, this diagnosis of operating components should be done periodically for safe maintenance and economical repair. However, conventional standard methods for mechanical properties have the problems of bulky specimen, destructive procedure and complex procedure of specimen sampling. So, a non-destructive and simple mechanical testing method using small specimen is needed. Therefore, an advanced indentation technique was developed as a potential method for non-destructive testing of in-field structures. This technique measures indentation load-depth curve during indentation and analyzes the mechanical properties related to deformation such as yield strength, tensile strength and work-hardening index. In this paper, we characterized the tensile properties including yield and tensile strengths of the V-modified Cr-Mo steels in petro-chemical and thermo-electrical plants. And also, the effects of hydrogen-assisted degradation of the V-modified Cr-Mo steels were analyzed in terms of work-hardening index and yield ratio.

A Conical Indentation Technique Based on FEA Solutions for Property Evaluation (유한요소해에 기초한 원뿔형 압입 물성평가법)

  • Hyun, Hong-Chul;Kim, Min-Soo;Lee, Jin-Haeng;Lee, Hyung-Yil
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.33 no.9
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    • pp.859-869
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    • 2009
  • The sharp indenters such as Berkovich and conical indenters have a geometrical self-similarity in theory, but different materials have the same load-depth curve in case of single indentation. In this study, we analyze the load-depth curves of conical indenter with angles of indenter via finite element method. From FE analyses of dual-conical indentation test, we investigate the relationships between indentation parameters and load-deflection curves. With numerical regressions of obtained data, we finally propose indentation formulae for material properties evaluation. The proposed approach provides stress-strain curve and the values of elastic modulus, yield strength and strain-hardening exponent with an average error of less than 2%. It is also discussed that the method is valid for any elastically deforming indenters made of tungsten carbide and diamond for instance. The proposed indentation approach provides a substantial enhancement in accuracy compared with the prior methods.

Evaluation of Indentation Fracture Toughens in Brittle Materials Based on FEA Solutions (유한요소해에 기초한 취성재료의 압입파괴인성평가)

  • Hyun, Hong Chul;Lee, Jin Heang;Felix, Rickhey;Lee, Hyungyil
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.37 no.12
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    • pp.1503-1512
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    • 2013
  • In this study, we proposed an indentation evaluation method for fracture toughness using cohesive finite element simulations. First, we examined the effect of material properties (yield strain, Poisson's ratio, and elastic modulus) on crack size during Vickers indentation and then generated a regression formula that explains the relations among fracture toughness, indentation load, and crack size. We also proposed another indentation formula for fracture toughness evaluation using the contact size a and E/H (H: hardness). Finally, we examined the relation between the crack size and the indenter shapes. Based on this, we can generate from the formula obtained using the Vickers indenter a formula for an indenter of different shapes. Using the proposed method, fracture toughness is directly estimated from indentation data.

Stacking Sequence Effects on Indentation Damage Behaviors of Fiber Metal Laminate (섬유의 적층 각도에 따른 섬유 금속 적층판의 압입 손상 거동)

  • Han, Gyeong-Seop;Nam, Hyeon-Uk;Jeong, Seong-Uk
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.5
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    • pp.960-968
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    • 2002
  • In this research, the effects of fiber stacking sequence on damage behaviors of FML(Fiber Metal Laminates) subject to indentation loading. SOP (Singly Oriented Ply) FML and angle ply FML were fabricated to study fiber orientation effects and angle ply effects. FML were fabricated by using 1050 aluminum laminate and carbon/epoxy prepreg. To increase adhesive bonding strength, Al laminate was etched using FPL methods. The static indentation test were conducted by using UTM under the 2side clamped conditions. During the tests, load and displacement curve and crack initiation and propagation behaviors were investigated. As fiber orientation angle increases, the crack initiation load of SOP FML increases because the stiffness induced by fiber orientation is increased. The penetration load of SOP FML is influenced by the deformation tendency and boundary conditions. However, the macro-crack of angle ply FML was initiated by fiber breakage of lower ply because angle plies in Angle ply FML prevents the crack growth and consolidation. The Angle ply FML has a critical cross-angle which prevent crack growth and consolidation. Damage behavior of Angle ply FML is changed around the critical cross-angle.

Application of Continuous Indentation Technique for Reliability Evaluation in Power Plant Facilities (발전설비 주요배관 신뢰도 확보를 위한 연속압입시험 적용)

  • Park, Sang-Ki;Ahn, Yeon-Shik;Jung, Gye-Jo;Cho, Yong-Sang;Choi, Yeol
    • Journal of the Korean Society for Nondestructive Testing
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    • v.24 no.2
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    • pp.158-162
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    • 2004
  • Reliability of welded structures in power plant facilities is very important, and their reliability evaluation requires exact materials properties. But, the conventional PQR (Procedure Qualification Record) can hardly reflect the real material properties in the field because the test is only done on specimens with simulated welding. Therefore, a continuous indentation technique is proposed in this study for simple and non-destructive testing of in-field structures. This test measures the indentation load-depth curve during indentation and analyzes the mechanical properties such as the yield strength, tensile strength and work hardening index. This technique has been applied to evaluate the tensile properties of the weldment in the main steam pipe and hot reheater pipe in power plants under construction and in operation.

Spherical Indentation Testing to Evaluate Mechanical Properties in 1Cr-1Mo-0.25V Steel (구형압입시험에 의한 1Cr-1Mo-O.25V강의 기계적 물성 평가)

  • Lee, Jong-Min;Lee, Seung-Seok;Lee, Ouk-Sub;Nam, Young-Hyun
    • Journal of the Korean Society for Nondestructive Testing
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    • v.22 no.5
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    • pp.516-522
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    • 2002
  • For the experimental study of rotor steel, seven kind of specimens with different degradation levels were prepared by isothermal heat treatment at $630^{\circ}C$. Spherical indentation technique was developed to evaluate the flow properties of metallic materials in carbon steel, stainless steel, and alloys, etc. Through the spherical indentation test, differently degraded 1Cr-1Mo-0.25V steel's mechanical properties were observed and compared with conventional standard test data. The flow properties of 1Cr-1Mo-0.25V steel's were estimated by analyzing the indentation load-depth curve. To characterize the flow property, we used material yield slope and constraint factor index rather than strain-hardening exponent because the variation of strain-hardening exponent was very little and the data showed irregularly. And the constraint factor's effect was small when the material yield slope was taken into account.

Assessment of Yield Characteristics of Gas Pipeline Materials by Observing Surface-Local Deformation (미소 표면변형 관찰을 통한 가스배관 부재의 항복특성 평가)

  • Lee, Yun-Hee;Baek, Un-Bong;Cheong, In-Hyeon;Nahm, Seung-Hoon;Lee, Sang-Houck
    • Journal of the Korean Institute of Gas
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    • v.12 no.2
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    • pp.92-98
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    • 2008
  • A combination of the instrumented indentation and 3D morphology measurement has been tried in order to perform a real-time property measurement of degraded materials in gas pipelines; three-dimensional indent morphologies were recorded using a reflective laser scanner after a series of insturmented indentations on three metallic specimens. Dimensions of the permanent deformation zone and contact boundary were analyzed from the cross-sectional profile over an remnant indent and used for estimating yield strength and hardness, respectively. Estimated yield strength was comparable with that from uniaxial tensile test and actual hardness implying material pile-up effects was lower than the calculated value from indentation curve by $20{\sim}30%$. It means that this 3D image analysis can explain the material pile-up effects on the contact properties. Additionally, a combined system of indentation and laser sensor was newly designed by modifying a shape of the indentation loading fixture.

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Laminate composites behavior under quasi-static and high velocity perforation

  • Yeganeh, E. Mehrabani;Liaghat, G.H.;Pol, M.H.
    • Steel and Composite Structures
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    • v.22 no.4
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    • pp.777-796
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    • 2016
  • In this paper, the behavior of woven E-glass fabric composite laminate was experimentally investigated under quasi-static indentation and high velocity impact by flat-ended, hemispherical, conical (cone angle of $37^{\circ}$ and $90^{\circ}$) and ogival (CRH of 1.5 and 2.5) cylindrical perforators. Moreover, the results are compared in order to explore the possibility of extending quasi-static indentation test results to high velocity impact test results in different characteristics such as perforation mechanisms, performance of perforators, energy absorption, friction force, etc. The effects of perforator nose shape, nose length and nose-shank connection shapes were investigated. The results showed that the quasi-static indentation test has a great ability to predict the high velocity impact behavior of the composite laminates especially in several characteristics such as perforation mechanisms, perforator performance. In both experiments, the highest performance occurs for 2.5 CRH projectile and the lowest is related to blunt projectiles. The results show that sharp perforators indicate lower values of dynamic enhancement factor and the flat-ended perforator represents the maximum dynamic enhancement factor among other perforators. Moreover, damage propagation far more occurred in high velocity impact tests then quasi-static tests. The highest damage area is mostly observed in ballistic limit of each projectile which projectile deviation strongly increases this area.

A Study on the Method of Residual Stress Relaxation during Wire Drawing and Evaluation of Residual Stress Using Nano Indentation Test (신선 시 선재의 잔류응력 완화 방법에 관한 연구 및 나노 압입 시험을 이용한 잔류응력 평가)

  • Ko Dae-Cheol;Hwang Won-Ho;Lee Sang-Kon;Kim Byung-Min
    • Journal of the Korean Society for Precision Engineering
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    • v.23 no.5 s.182
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    • pp.162-169
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    • 2006
  • Steel cord which is used as reinforcement in car tires is produced by wet-drawing process. Recently the quality improvement of the steel cord product is demanded by the tire market. After cold drawing process, produced residual stresses have a harmful effect on the durability of the wire and become the cause which decreases the quality of the product. Therefore, to improve the quality of the steel cord product, the research regarding the method of residual stress relaxation is necessary. To evaluate the quality of the cold drawn wire, it is very important to measure the residual stress, because the residual stress decides a variety of the quality level which is demanded in the cold drawn wire. The aim of this study is to propose residual stress relaxation method in the drawn wire using FE-analysis. The validity of the analysis results was verified by Nano indentation test.