• Title/Summary/Keyword: Indentation Technique

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The Measurement Errors of Elastic Modulus and Hardness due to the Different Indentation Speed (압입속도의 변화에 따른 탄성계수와 경도의 오차 연구)

  • Lee, Kyu-Young;Lee, Chan-Bin;Kim, Soo-In;Lee, Chang-Woo
    • Journal of the Korean Vacuum Society
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    • v.19 no.5
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    • pp.360-364
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    • 2010
  • Most research groups used two analysis methods (spectroscopy and nanotribology) to measure the mechanical properties of nano-materials: NMR (Nuclear Magnetic Resonance), IR (Infrared Spectroscopy), Raman Spectroscopy as the spectroscopy method and AFM (Atomic Force MicroScope), EFM (Electrostatic Force Microscope), KFM (Kelvin Force Microscope), Nanoindenter as the nanotribological one. Among these, the nano-indentation technique particularly has been recognized as a powerful method to measure the elastic modulus and the hardness. However, this technique are prone to considerable measurement errors with pressure conditions during measurement. In this paper, we measured the change of elastic modulus and hardness of an Al single crystal with the change of load, hold, and unload time, respectively. We found that elastic modulus and hardness significantly depend on load, hold, and unload time, etc. As the indent time was shortened, the elastic modulus value decreased while the hardness value increased. In addition, we found that elastic modulus value was more sensitive to indent load, hold, and unload time than the hardness value. We speculate that measurement errors of the elastic modulus and the hardness originate from the residual stress during indenting test. From our results, the elastic modulus was more susceptible to the residual stress than the hardness. Thus, we find that the residual stress should be controlled for the minimum measurement errors during the indenting test.

The effect of ultrasonic nano crystal surface modification for mitigation of the residual stress after weld inlay on the alloy 82/182 dissimilar metal welds of reactor vessel in/outlet nozzles (원자로 입출구 노즐 Alloy 82/182 이종금속 용접부 Weld Inlay 적용 후 초음파나노표면개질이 잔류응력 완화에 미치는 영향)

  • Cho, Hong Seok;Park, Ik Keun;Jung, Kwang Woon
    • Journal of Welding and Joining
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    • v.33 no.2
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    • pp.40-46
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    • 2015
  • This study was performed to investigate the effect of ultrasonic nano crystal surface modification (UNSM) on residual stress mitigation after Weld Inlay repair for butt dissimilar metal weld with Alloy 82/182 in reactor vessel In/Outlet nozzle. As-welded and Weld Inlay specimens were made in accordance with design standard of ASME Code Case N-766, and two planes of their weld specimens were peened by the optimum UNSM process condition. Peening characteristics for weld specimens after UNSM treatment were evaluated by surface roughness and Vickers hardness test. And, residual stress for weld specimens developed from before and after UNSM treatment was measured and evaluated by instrumented indentation technique. Consequently, it was revealed that the mitigation of residual stress in weld metal after Weld Inlay repair of reactor vessel In/Outlet nozzle could be possible through UNSM treatment.

A Program Similarity Evaluation Algorithm (프로그램 유사도 평가 알고리즘)

  • Kim Young-Chul;Hwang Seog-Chan;Choi Jaeyoung
    • Journal of Internet Computing and Services
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    • v.6 no.1
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    • pp.51-64
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    • 2005
  • In this paper, we introduce a system for evaluating similarity of C program source code using method which compares syntax-trees each others. This method supposes two characteristic features as against other systems. It is not sensitive for program style such as indentation, white space, and comments, and changing order of control structure like sentences, code block, procedures, and so on. Another is that it can detect a syntax-error cause of using paring technique, We introduce algorithms for similarity evaluation method and grouping method that reduces the number of comparison, In the examination section, we show a test result of program similarity evaluation and its reduced iteration by grouping algorithm.

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The Effects of Grain Size on the Degradation Phenomena of PZT Ceramics (입자의 크기가 PZT 세라믹스의 열화현상에 미치는 영향)

  • 정우환;김진호;조상희
    • Journal of the Korean Ceramic Society
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    • v.29 no.1
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    • pp.65-73
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    • 1992
  • The effect of grain size on the time-dependent piezoelectrice degradation of a poled PZT of MPB composition Pb0.988Sr0.012 (Zr0.52Ti0.48)O3 with 2.4 mol% of Nb2O5 was studied, and the degradation mechanism was discussed. Changes in the internal bias field and the internal stress both responsible for the time-dependent degradation of poled PZT were examined by the polarization reveral technique, XRD and Vickers indentation, respectively. The piezoelectric degradation increased with increasing time and grain size, and the internal bias field due to space charge diffusion decreased with increasing grain size of poled PZT. The internal bias field, however, was almost insensitive to the degradation time regardless of the grain size. On the other hand, both the x-ray diffraction peak intensity ratio of (002) to (200) and the fracture behavior including the crack propagation support that the ferroelectric domain rearrangement of larger grain size showed rapid relaxation of the internal stress compared with smaller one, which is thought the origin of the larger piezoelectric degradation in the former. In conclusion, the contribution of space charge diffusion on the piezoelectric degradation of PZT is strongly dependent on both the grain size and the composition. Thus, the relaxation of internal stress due to the ferroelectric domain rearrangement as well as the amount and time-dependence of the internal bias field due to space charge diffusion should be considered simultaneously in the degradation mechanism of PZT.

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Fabrication of RFID Micro-pattern using Ultrasonic Vibration (초음파 진동을 이용한 RFID 미세패턴 성형)

  • Oh, Myung-Seok;Lee, Bong-Gu;Park, Myung-Kyu
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.26 no.3
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    • pp.344-349
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    • 2017
  • In this study, we developed a process technology to fabricate RFID tag antennas using a one-sheet inlay micro-pattern forming process by press-molding RFID tag antennas on insulation sheet layers, such as polymer films, using ultrasonic longitudinal vibration. In addition, a fine pattern applicable for RFID tag antennas was manufactured using a $25{\mu}m$ thick thin-plate square wire; this is in contrast to the method that uses a conventional round wire. The developed ultrasonic indentation process can be used to fabricate fine pattern of the RFID antenna using one piece of equipment. The simplified manufacturing process technology has a shorter manufacturing time and is more economical. The developed RFID tag antenna forming technique involves pressing the $25{\mu}m$ square wire directly on the thin sheet insulation sheet of maximum thickness $200{\mu}m$, using a 60 kHz ultrasonic tool horn.

발전 설비의 가동 중 신뢰성 평가를 위한 연속압입시험법의 활용

  • Song, Won-Seok;Gang, Seung-Gyun;Kim, Yeong-Cheon;Kwon, Dong-Il
    • Proceedings of the Korean Reliability Society Conference
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    • 2011.06a
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    • pp.125-130
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    • 2011
  • 발전 설비는 기대 수명동안의 안정성을 확보하기 위하여 해당 규격에 부합하도록 설계하여 건설된다. 하지만 가동 중 다양한 복합 환경에 노출됨에 따라 구조물을 이루고 있는 재료의 열화 현상이 가속화되어 예기치 못한 파손이 발생할 수 있다. 기계적 물성은 재료의 기계적 거동을 나타내는 주요 척도가 되며 이는 신뢰성 및 안전과 직결된다. 하지만 기존의 역학물성을 측정하는 대부분의 시험법들은 특정 크기의 시편을 요구하고 파괴적인 시험법이기 때문에 가동 중 시설물에 적용하기가 불가능하였다. 이러한 한계점을 극복하고자 비파괴적이고 정량적인 시험이 가능한 연속압입시험법이 최근 각광받는 시험법으로서 많은 연구자들에 의해 연구되고 있다. 이 시험법은 시험 대상물의 형상에 제약을 받지 않으며 시험 절차가 매우 간단하다는 장점을 가진다. 또한 대상의 국소 부위에 시험할 수 있어 취약 부위 판별이 가능하다. 본 연구에서는 대표응력-대표변형률 기법을 통하여 인장물성을 평가하고, 압입 하중 차이를 이용하여 소재에 존재하는 잔류응력을 평가하는 기법을 소개한다. 또한, 연속압입시험을 이용하여 실제 발전소 파이프의 취약부위로 알려진 용접부에 대하여 인장물성 및 잔류응력을 측정함으로써 실제 산업체의 신뢰성 평가가 적용할 수 있음을 확인하였다.

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Real-Time Haptic Rendering of Slowly Deformable Bodies Based on Two Dimensional Visual Information for Telemanipulation (원격조작을 위한 2차원 영상정보에 기반한 저속 변형체의 실시간 햅틱 렌더링)

  • Kim, Jung-Sik;Kim, Young-Jin;Kim, Jung
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.31 no.8
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    • pp.855-861
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    • 2007
  • Haptic rendering is a process providing force feedback during interactions between a user and a virtual object. This paper presents a real-time haptic rendering technique for deformable objects based on visual information of intervention between a tool and a real object in a remote place. A user can feel the artificial reaction force through a haptic device in real-time when a slave system exerts manipulation tasks on a deformable object. The models of the deformable object and the manipulator are created from the captured image obtained with a CCD camera and the recognition of objects is achieved using image processing techniques. The force at a rate of 1 kHz for stable haptic interaction is deduced using extrapolation of forces at a low update rate. The rendering algorithm developed was tested and validated on a test platform consisting of a one-dimensional indentation device and an off-the shelf force feedback device. This software system can be used in a cellular manipulation system providing artificial force feedback to enhance a success rate of operations.

Crush Strength Analysis of a Spacer Grid for PWR Nuclear Fuel Considering Mechanical Properties in Weld Zone (용접부 기계적 물성치를 고려한 경수로 핵연료 지지격자의 충격해석)

  • Song, Kee-Nam;Lee, Sang-Hoon
    • Transactions of the Korean Society of Pressure Vessels and Piping
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    • v.8 no.2
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    • pp.7-13
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    • 2012
  • A spacer grid which is one of the most important structural components in a pressurized water reactor fuel is an interconnected array of slotted grid straps, welded at the intersections to form an egg-crate structure. The spacer grid is required to not only protect fuel rods stably but also have sufficient lateral crush strength for the sake of enabling shut-down of the nuclear reactor during abnormal operating environments. Then, the lateral crush strength of the spacer grid is closely related with welding quality of the spacer grid. Previous research on the crush strength analysis of the spacer grid had been performed using only parent material properties. In this study, to investigate the effect on the crush strength of the spacer grid when used mechanical properties in weld zone instead of parent material properties, crush strength analysis considering mechanical properties in weld zone obtained from the instrumented indentation technique was performed and compared the results with the previous research.

Nanoindentation on the Layered Ag/Cu for Investigating Slip of Misfit Dislocation (나노인덴테이션 해석을 통한 Ag/Cu층에서 발생하는 Misfit 전위의 slip 특성에 대한 연구)

  • Trandinh, Long;Ryu, Yong-Moon;Cheon, Seong-Sik
    • Composites Research
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    • v.24 no.3
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    • pp.17-24
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    • 2011
  • The EAM simulation of nanoindentation was performed to investigate misfit dislocation slip in the Ag/Cu. The film layer, whose thickness in the range of 2-5nm, was indented by a spherical indenter with the N$\'{o}$se-Hoover thermostat condition. The simulation shows that the indentation position relative to misfit dislocation (MFD) has the effect on the dislocation, glide up or cross slip, for Ag film layer thickness less than 4 nm. Elastic energy variation during MFDs slip was revealed to be a key factor for the softening of Ag/Cu. The critical film layer thickness was evaluated for each case of Ag/Cu according to the spline extrapolation technique.

Effects of Tungsten Addition on Tensile Properties of a Refractory Nb-l8Si-l0Ti-l0Mo-χW (χ=0, 5, 10 and 15 mot.%) In-situ Composites at 1670 K

  • 김진학;Tatsuo Tabaru;Hisatoshi Hirai
    • Transactions of Materials Processing
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    • v.8 no.3
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    • pp.233-233
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    • 1999
  • To investigate the effect of tungsten addition on mechanical properties, we prepared refractory (62χ)Nb-18Si-l00Mo-l0Ti-χW (χ=0, 5, 10 and 15 mol.%) in-situ composites by the conventional arc-casting technique, and then explored the microstructure, hardness and elastic modulus at ambient temperature and tensile properties at 1670 K. The microstructure consists of relatively fine (Nb, Mo, W, Ti)/sub 5/Si₃, silicide and a Nb solid solution matrix, and the fine eutectic microstructure becomes predominant at a Si content of around 18 mol.%. The hardness of (Nb, Mo, W, Ti(/sub 5/Si₃, silicide in a W-free sample is 1680 GPa, and goes up to 1980 GPa in a W 15 mol.% sample. The hardness, however, of Nb solid solution does not exhibit a remarkable difference when the nominal W content is increased. The elastic modulus shows a similar tendency to the hardness. The optimum tensile properties of the composites investigated are achieved at W 5 mol.% sample, which exhibits a relatively good ultimate strength of 230 MPa and an excellent balance of yield strength of 215 MPa, and an elongation of 3.7%. The SEM fractography generally indicates a ductile fracture in the W-free sample, and a cleavage rupture in W-impregnated ones.