• Corrosion Science and Technology
• /
• v.3 no.5
• /
• pp.198-208
• /
• 2004

Although there has been no general agreement on the mechanism of primary water stress corrosion cracking (PWSCC) as one of major degradation modes of Ni-base alloys in pressurized water reactors (PWR's), common postulation derived from previous studies is that the damage to the alloy substrate can be related to mass transport characteristics and/or repair properties of overlaid oxide film. Recently, it was shown that the oxide film structure and PWSCC initiation time as well as crack growth rate were systematically varied as a function of dissolved hydrogen concentration in high temperature water, supporting the postulation. In order to understand how the oxide film composition can vary with water chemistry, this study was conducted to characterize oxide films on Alloy 600 by an in-situ Raman spectroscopy. Based on both experimental and thermodynamic prediction results, Ni/NiO thermodynamic equilibrium condition was defined as a function of electrochemical potential and temperature. The results agree well with Attanasio et al.'s data by contact electrical resistance measurements. The anomalously high PWSCC growth rate consistently observed in the vicinity of Ni/NiO equilibrium is then attributed to weak thermodynamic stability of NiO. Redox-induced phase transition between Ni metal and NiO may undermine the integrity of NiO and enhance presumably the percolation of oxidizing environment through the oxide film, especially along grain boundaries. The redox-induced grain boundary oxide degradation mechanism has been postulated and will be tested by using the in-situ Raman facility.

• Journal of the Korean Geotechnical Society
• /
• v.15 no.4
• /
• pp.185-205
• /
• 1999

Hydraulic fracturing tests were performed in two inclined boreholes for the design of underground oil storages in Korea. Extensions of their application limits were expected through a precise comparison between the interpretation techniques for the vertical and the inclined boreholes. Especially, it was verified that the magnitude of in-situ stress can be varied even in the same rock mass with a variety of geographic/geotechnical characteristics. It was also demonstrated that its orientation can be changed even in the same borehole with the existence of explicit discontinuities.

• Journal of the Korean Ceramic Society
• /
• v.33 no.2
• /
• pp.203-213
• /
• 1996

In this study the subcritical crack growth behavior in an Al2O3-SiCw composite has been investigated using in situ fracture technique of applied moment double cantilever beam (AMDCB) specimens indside an SEM. This technique allows the detailed observation of whisker and grain bridging in the crack wake region. The experimental results indicated that the KI-a curve was deviated from the conventional powder law form and that the existed a region where the rate of microcrack growth was decreased with increasing the externally applied stress intensity factor. This behavior could be explained by arising crack growth resistance i.e. R-curve behavior which was associated with crack shielding due to whisker and grain bridging. The R-curve was also analyzed from the KI-a curve data in order to quantify the bridging effect in the Al2O3-SiCw composite.

• Proceedings of the Korean Magnestics Society Conference
• /
• 1997.11a
• /
• pp.106-107
• /
• 1997

• Proceedings of the Korean Radioactive Waste Society Conference
• /
• 2018.05a
• /
• pp.117-118
• /
• 2018

• Proceedings of the Korean Geotechical Society Conference
• /
• 2008.03a
• /
• pp.1-6
• /
• 2008

When a saturated clay is sampled in an undisturbed manner from a bore hole, the sample extends vertically and shrinks horizontally under undrained conditions due to stress release. The conventional consolidation test specimen is trimmed from the expanded sample so that its diameter is equal to the inner diameter of the consolidation test ring, this test procedure does not reproduce the actual consolidation behavior. The measurement of sample extension was conducted by means of overcoring method found that the extension strains were 1 to 2%. To simulate the in-situ consolidation behavior, the consolidation test method that uses a specimen with a slightly smaller diameter than the inside diameter of consolidometer so that the specimen expands laterally to the inside of the ring.

• Tunnel and Underground Space
• /
• v.5 no.2
• /
• pp.95-103
• /
• 1995

In this paper the stress redistribution around tunnel face was analyzed by using a three-dimensional finite element model. The effects of in-situ stress levels, excavation sequences, stiffness difference between the hard ground and the weak zone on the stress redistributions were considered. Displacement and stress changes at tunnel crown, side wall, and invert were investigated throughout the sequential excavation. To show ground response, percentage of the displacement and stress variations are used as a function of normalized distance that is between the face and monitoring section. Preceding displacements and stress variations were presented to be adopted in the two-dimensional tunnel analysis.

• Tunnel and Underground Space
• /
• v.18 no.5
• /
• pp.343-354
• /
• 2008

A new method is suggested herein to measure the virgin earth stresses by means of a borehole. This novel concept is basically a combination of borehole stress relieving and borehole fracturing techniques. The destressing of the borehole is achieved by means of inducing thermal tensile stresses at the borehole periphery by using a cryogenic fluid such as Liquid Nitrogen($LN_2$). The borehole wall eventually develops fractures when the induced thermal stresses exceed the existing compressive stresses at the borehole periphery in addition to the tensile strength of the rock. The above concept is theoretically analyzed for its potential applicability to interpret in situ stress levels from the tensile fracture stresses and the corresponding borehole wall temperatures. Coupled thermo-mechanical numerical simulations are also conducted using FLAC3D, with thermal option, to check the validity of the proposed techniques. From the preliminary theoretical and numerical analysis, the method suggested for the measurement of in situ stresses appears to be capable of accurate estimation of the virgin stresses by monitoring tensile crack formation at a borehole wall and recording the wall temperatures at the time of crack initiation.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.30 no.9
• /
• pp.546-550
• /
• 2017

Ferroelectric properties are governed by domain structures and domain wall motions, so it is of significance to understand domain evolution processes under mechanical stress. In the present study, in situ piezoresponse force microscopy (PFM) observation under compressive stress was carried out for a near-morphotropic PZT. Both $180^{\circ}$ and $non-180^{\circ}$ domain structures were observed from PFM images, and their habit planes were identified using electron backscatter diffraction in conjunction with PFM data. By externally applied mechanical stress, needle-like $non-180^{\circ}$ domain patterns were broadened via domain wall motions. This was interpreted via phenomenological approach such that the total energy minimization can be achieved by domain wall motion rather than domain nucleation mainly due to the local gradient energy. Meanwhile, no motion was observed from curvy $180^{\circ}$ domain walls under the mechanical stress, validating that $180^{\circ}$ domain walls are not directly influenced by mechanical stress.

• Journal of the Korean Ceramic Society
• /
• v.31 no.12
• /
• pp.1449-1458
• /
• 1994

A new analytical model which can discribe the relationship between the bridging stress and the crack opening displacement was proposed to investigate the microstructural effect on the R-curve behavior in a polycrystalline alumina. The crack opening displacement according to the distance behind the stationary crack tip was measured using in-situ fracture technique in an SEM, and then used for a fitting procedure to obtain the distribution of bridging stress. The current model and an empirical power law relation were introduced into the fitting procedure. The results indicated that the bridging stress function and R-curve computed by the current model were consistent with those computed by the power law relation. The microstructural factor, e.g., the distribution of grain size, was also found to be closely related to the bridging stress. Thus, this model explained well the interaction effect between the distribution of bridging stress and the local-fracture-controlling microstructure, providing important information for the systematic interpretation of microfracture mechanism including R-curve behavior of a monolithic alumina.