• 제목/요약/키워드: In-process Electrolytic

검색결과 295건 처리시간 0.033초

Cyclitol 유도체 합성에 관한 연구 (제3보)-myo-Inositol의 전해 산화- (Synthesis of Cyclitol Derivatives (Ⅲ). Electrolytic Oxidation of myo-Inositol)

  • 손주환;남종우;김유옥
    • 대한화학회지
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    • 제15권3호
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    • pp.127-132
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    • 1971
  • To obtain the various kinds of inosose stereomers, the process of electrochemical oxidation is more effective than chemical oxidation of myo-inositol. So that myo-inositol aqueous solution was electrolyzed by platinum and lead peroxide anode to confirming the occurrence of electrochemical oxidation. The result is that myo-inosose-2 is producing with high yield comparatively by electrolytic oxidation of myo-inositol. Also we studied about the relation between the electrolytic current efficiency and electrolytic temperature and anodic current density. The current efficiency is rising with lowering of electrolytic temperature identically in both anode such as platinum and lead peroxide and also rising with increasing of anodic current density in platinum anode, but inversely in lead peroxide.

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최적 연속 전해드레싱에 의한 연삭기구의 규명에 관한 연구 (A study on the analysis of grinding mechanism by using optimum in-process electrolytic dressing)

  • 이은상;김정두
    • 대한기계학회논문집A
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    • 제21권8호
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    • pp.1298-1310
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    • 1997
  • In recent years, grinding techniques for precision machining of brittle materials used in electric, optical and magnetic parts have been improved by using superabrasive wheel and precision grinding machine. The completion of optimum dressing of superabrasive wheel makes possible the effective precision grinding of brittle materials. However, the present dressing system cannot have control of optimum dressing of the superabrasive wheel. In this study, a new system and the grinding mechanism of optimum in-process electrolytic dressing were proposed. This system can carry out optimum in-process dressing of superabrasive wheel, and give very effective control according to unstable current and gap increase. Therefore, the optimum in-process electrolytic dressing is a good method to obtain the efficiency and mirror-like grinding of brittle materials.

플라즈마 전해 산화처리된 Ti-6Al-4V합금의 표면특성에 미치는 울라스토나이트 코팅효과 (Effects of Wollastonite Coating on Surface Characteristics of Plasma Electrolytic Oxidized Ti-6Al-4V Alloy)

  • 고재은;이종국;최한철
    • Corrosion Science and Technology
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    • 제22권4호
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    • pp.257-264
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    • 2023
  • Ti-6Al-4V alloys are mainly used as dental materials due to their excellent biocompatibility, corrosion resistance, and chemical stability. However, they have a low bioactivity with bioinertness in the body. Therefore, they could not directly bond with human bone. To improve their applications, their bone bonding ability and bone formation capacity should be improved. Thus, the objective of this study was to improve the bioinert surface of titanium alloy substrate to show bioactive characteristics by performing surface modification using wollastonite powder. Commercial bioactive wollastonite powder was successfully deposited onto Ti-6Al-4V alloy using a room temperature spray process. It was found that wollastonite-coated layer showed homogeneous microstructure and uniform thickness. Corrosion resistance of Ti-6Al-4V alloy was also improved by plasma electrolytic oxidation treatment. Its wettability and bioactivity were also greatly increased by wollastonite coating. Results of this study indicate that both plasma electrolytic oxidation treatment and wollastonite coating by room temperature spray process could be used to improve surface bioactivity of Ti-6Al-4V alloy substrate.

충전복극전해조에 의한 총 인 제거 (Removal of Total Phosphate by Bipolar Packed Bed Electrolytic Cell)

  • 김은희;박승조
    • 공업화학
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    • 제19권4호
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    • pp.366-369
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    • 2008
  • 입자상 알루미늄 충전복극조의 성능을 파악할 목적으로 실험은 회분식과 연속식으로 진행하였다. 입자상 알루미늄 충전복극조를 이용하여 T-P 농도 10 mg/L인 인산염 함유 용액을 6 V에서 3 h 회분식으로 전해처리 한 결과 T-P의 제거율은 88% 이었다. 입자상 알루미늄 충전복극조를 이용하여 T-P 농도 10 mg/L인 인산염 함유 용액을 6 V에서 HRT를 3 h으로 하여 연속식으로 전해처리 한 결과 T-P의 농도는 2 mg/L이었다. HRT 3 h으로 고정하여 전해처리 할 경우 120 h 처리 후 파과점을 관찰할 수 있었다.

전해인프로세스드레싱에 의한 경면연삭기술개발 (Mirror grinding with Electrolytic In-process Dressing Method)

  • 이응숙;제태진;강재훈
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 1995년도 추계학술대회 논문집
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    • pp.57-60
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    • 1995
  • Recently, ELID (electrolytic in-process dressing) grinding technique is developed. It is possible to make a efficient precision machining of hard materials such as ceramic hard metals, and quenched steels. This paper deals with some typical applications of ELID-grinding for cylindrcal machining. The significant advantages, performance and characteristics on mirror surface grinding for external surface are described.

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ELID 연삭에서 가공 상태 감시 시스템 개발 (Development of process monitoring system in ELID grinding)

  • 서영호;김화영;안중환
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2000년도 춘계학술대회 논문집
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    • pp.599-602
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    • 2000
  • A new dressing technique with utilizes electrolytic phenomenon for realizing effective mirror surface grindings with metal bonded super-abrasive wheels is called “Electrolytic In-process Dressing Grinding”. This technique enabled metal bonded micro-grain wheels, such as micro-grain cast iron fiber bonded wheels, to be used for mirror surface finish processes effectively. But this technique requires a lot of knowledge and experience to perform. And the condition of dressing is variable according to the time. Therefore adaptation of Monitoring and Control technique is needed.

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세라믹스의 ELID연삭가공 ((Electrolytic in-Process Dressing)-Grinding of Ceramics)

  • 오오모리 히토리;카타히라 카즈토시
    • 세라미스트
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    • 제9권6호
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    • pp.37-41
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    • 2006
  • A novel grinding technology, known as ELID (Electrolytic In-Process Dressing), which incorporates 'inprocess dressing' of metal- bonded diamond grinding wheels, provides continuous protruding abrasives effectively applied to ceramic grinding. This article describes the ELID-grinding method and introduces its application examples on ceramics

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Corrosion behaviors of plasma electrolytic oxidation (PEO) treated high-silicon aluminum alloys

  • Park, Deok-Yong;Chang, Chong-Hyun;Oh, Yong-Jun;Myung, Nosang V.;Yoo, Bongyoung
    • 한국표면공학회지
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    • 제55권3호
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    • pp.143-155
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    • 2022
  • Ceramic oxide layers successfully were formed on the surface of cast Al alloys with high Si contents using plasma electrolytic oxidation (PEO) process in electrolytes containing Na2SiO3, NaOH, and additives. The microstructure of the oxide layers was systematically analyzed using scanning electron microscopy (SEM), cross-sectional transmission electron microscopy (TEM), X-ray diffraction patterns (XRD), and energy X-ray dispersive spectroscopy (EDS). XRD analysis indicated that the PEO untreated high-silicon Al alloys (i.e., 17.1 and 11.7 wt.% Si) consist of Al, Si and Al2Cu phases whereas Al2Cu phase selectively disappeared after PEO treatment. PEO process yielded an amorphous oxide layer with few second phases including γ-Al2O3 and Fe-rich phases. The corrosion behaviors of high-silicon Al alloys treated by PEO process were investigated using electrochemical impedance spectroscopy (EIS) and other electrochemical techniques (i.e., open circuit potential and polarization curve). Electroanalytical studies indicated that high-silicon Al alloys treated by PEO process have greater corrosion resistance than high-silicon alloys untreated by PEO process.

미세 펄스전원을 이용한 스테인레스강 300 계열의 전기화학연마 (Study on Electrochemical Polishing for Stainless Steel 300 Series using Micro Pulse Current)

  • 이동활;박정우;문영훈
    • 소성∙가공
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    • 제12권4호
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    • pp.388-393
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    • 2003
  • Electrolytic polishing is the anodic dissolution process in the transpassive state. It removes non-metallic inclusions and improves mechanical and corrosion resistance of stainless steel. Electrolytic polishing is normally used to remove a very thin layer of material from the surface of a metal object. An electrolyte of phosphoric acid 50% in vol., sulfuric acid 20% in vol. and distilled water 30% in vol. has been used in this study. In the low current density region, there can be found plateau region and material removal process and leveling process occur successively. In this study, an electrochemical polishing process using pulse current is adopted as a new electrochemical polishing process. In electrochemical machining processes, it has been found that pulse electrochemical processes provide an attractive alternative to the electrochemical processes using continuous current. Hence, this study will discuss the electrochemical polishing processes in low current density region and pulse electrochemical polishing.