• 대한치과보철학회지
• /
• 제35권1호
• /
• pp.221-243
• /
• 1997

The objective of this study was to characterize the mechanical properties of $Y_{2}O_{3}$-containing glass infiltrated ceramic core material, which was made by pressureless powder packing method. A pure alumina powder with a grain size of about $4{\mu}m$ was packed without pressure is silicon mold to form a bar shaped sample, and applied PVA solution as a binder. Samples were sinterd at $1350^{\circ}C$ for 1 hour. After cooling, $Y_{2}O_{3}$-containing glass($SiO_{2},\;Y_{2}O_{3},\;B_{2}O_{3},\;Al_{2}O_{3}$, ect) was infiltrated to the sinterd samples at $1300^{\circ}C$ for 2 hours and cooled. Six different proportions $Y_{2}O_{3}$ of were used to know the effect of the mismatch of the thermal expansion coefficient between alumina powder and glass. The samples were ground to $3{\times}3{\times}30$ mm size and polished with $1{\mu}m$ diamond paste. Flexural strength, fracture toughness, hardness and other physical properties were obtained, and the fractured surface was examined with SEM and EPMA. Ten samples of each group were tested and compared with In-Ceram(tm) core materials of same size made in dental laboratory. The results were as follows : 1. The flexural strengths of group 1 and 3 were significantly not different with that of In-Ceram, but other experimental groups were lower than In-Ceram. 2. The shrinkage rate of samples was 0.42% after first firing, and 0.45% after glass infiltration. Total shrinkage rate was 0.87%. 3. After first firing, porosity rate of experimental groups was 50%, compared with 22.25% of In-Ceram. After glass infiltration, porosity rate of experimental groups was 2%, and 1% in In-Ceram. 4. There was no statistical difference in hardness between two materials tested, but in fracture toughness, group 2 and 3 were higher than In-Ceram. 5. The thermal expansion coefficients of experimental groups were varied to $4.51-5.35{\times}10^{-6}/^{\circ}C$ according to glass composition, also the flexural strengths of samples were varied. 6. In a view of SEM, many microparticles about $0.5{\mu}m$ diameter and $4{\mu}m$ diameter were observed in In-Ceram. But in experimental group, the size of most particles was about $4{\mu}m$, and a little microparticles was observed. The results obtained in this study showed that the mismatch of the thermal expansion coefficients between alumina powder and infiltrated glass affect the flexural strength of alumin/glass composite. The $Y_{2}O_{3}$-containing glass infiltrated ceramic core made by powder packing method will takes less time and cost with sufficient flexural strength similar to all ceramic crown made with slip casting technique.

• 구강회복응용과학지
• /
• 제16권2호
• /
• pp.105-112
• /
• 2000

본 연구는 치아형성시 shoulder 폭경이 변연 적합도에 미치는 영향을 평가하기 위해 시행하였다. 지대치의 치경부쪽의 shoulder 폭경을 0.6 mm, 0.9 mm, 1.2 mm로 나누어 각각 9개씩, 총 27개의 모형을 제작하여 통법에 따라 In-Ceram 전부 도재관을 제작한 후 시멘트 접착하고 근심, 원심, 협, 설측 중앙 부위를 200배 확대하여 변연 적합도의 측정한 후 각 군과, 측정부위에 따른 변연 적합도 비교해 본 결과 다음과 같은 결론을 얻었다. 1. shoulder 폭경이 0.6 mm인 경우 $81.28{\mu}m$, 0.9 mm인 경우는 $70.78{\mu}m$, 1.2mm 인 경우는 $67.75{\mu}m$의 변연간극을 보였다. 2. shoulder 폭경이 0.6 mm인 경우가 0.9 mm, 1.2 mm인 경우보다 변연간극이 유의한 차이를 크게 나탔났으며(p<0.05), 0.9 mm인 경우와 1.2 mm인 경우는 유의한 차이가 없었다(p>0.05). 3. In-Ceram 시편의 변연부에서 근심측, 원심측, 순측, 설측의 측정위치에 따른 변연적합도의 비교시 유의한 차이가 없었다(p>0.05).

• 대한치과기공학회지
• /
• 제36권4호
• /
• pp.247-253
• /
• 2014

Purpose: The aim of this study was to evaluate the effect of colored zirconia with different coloring liquids. Methods: Total 30 specimens were prepared. Specimens were classified into 6 groups: IPS e.max Ceram(P), Uncolored zirconia(C), VITA In-Ceram$^{(R)}$2000 YZ LL1(L), Zirkonzahn coloring liquid(Z), Wieland coloring liquid(W), and Kuwotech coloring liquid(K). Four different types of zirconia coloring liquid, VITA In-Ceram$^{(R)}$ 2000 YZ LL1(VITA Zahnfabrik, Germany), Zirkonzahn coloring liquid(Zirkonzahn, Italy), Wieland coloring liquid(Wieland, Germany), Kuwotech coloring liquid(Kuwotech, Korea) were used to fabricate colored zirconia by using infiltrating method and then completely sintered. The color of the all specimens was measured using the spectrophotometer(CM-2600d, Konica Minolta, Japan) and expressed in terms of the 3-coordinated values(CIE $L^*a^*b^*$). Color differences were calculated using the equation $${\Delta}E^*=[({\Delta}L^*)^2+({\Delta}a^*)^2+({\Delta}b^*)^2]^{1/2}$$. Results: $L^*a^*b^*$ values of the colored zirconia were affected by the coloring liquids. The uncolored zirconia(C) group showed the highest $L^*$ value and zirkonzahn coloring liquid(Z) group showed the lowest $L^*$ value. Zirkonzahn coloring liquid(Z) showed the highest $a^*$ value and VITA In-Ceram 2000 YZ LL1(L) group showed the highest $b^*$ value. Generally, the color difference(${\Delta}E^*$) in all groups showed higher than 3.7 except between IPS e.max Ceram(P) and wieland coloring liquid(W) group. Conclusion: Within the limitations of this study, various coloring liquids influenced the $L^*$, $a^*$, and $b^*$ values of colored zirconia. IPS e.max Ceram(P) and wieland coloring liquid(W) group did not show clinically perceiving color difference.

• 대한소아치과학회지
• /
• 제35권2호
• /
• pp.259-267
• /
• 2008

구치부 인접면 와동에서 유동성 복합레진 이장재의 두께가 치은측 변연의 미세누출에 미치는 영향을 평가하기 위하여 발거된 소구치 및 대구치의 근, 원심면에 box 형태의 와동(협설폭경 3mm, 근원심폭경 2mm, 상아법랑경계 상방 1mm에 치은 변연) 120개를 형성한 뒤, 무작위로 30개씩 선정하여 다음과 같은 4개의 군으로 분류하였다. group I- Tetric ceram 충전군(대조군) group II- 0.5mm 두께의 Tetric flow + Tetric ceram group III- 1.5mm 두께의 Tetric flow + Tetric ceram group IV- 2.5mm 두께의 Tetric flow + Tetric ceram 색소침투법으로 치은측 변연부 미세누출을 측정하여 다음과 같은 결론을 얻었다. 1. group II는 group I에 비해 낮은 미세누출을 보였다(p<0.05). 2. group III, IV과 group I 사이에는 통계적으로 유의한 미세누출의 차이가 없었다(p>0.05). 3. group II는 group III, IV에 비해 낮은 미세누출을 보였다(p<0.05). 4. 모든 group에서 정도의 차이는 있으나 치경부에서 미세누출을 보였다. 이상의 결과로, 혼합형 복합레진으로의 구치부 인접면 와동 수복시 0.5mm 두께의 유동성 레진으로의 와동저 이장은 치은측 변연의 봉쇄능을 향상시켜 변연부 미세누출을 감소시킬 수 있는 방법으로 사료된다.

• 대한치과기공학회지
• /
• 제29권2호
• /
• pp.119-128
• /
• 2007

Although there are many different ways that restorations can be made, it can be said that the biocompatibility of abutment and crown is very important in this experiment. When placed in the actual oral cavity, the differences were obvious. Compared to In-ceram Aluminium, the structure that is obtained after firing reveals a particularly homogeneous distribution of the crystal and glass phase. The In-ceram aluminium system had many problems, such as having weak tensile strength, and having low bonding strength due to the shrinking that occurs after firing. Because of the opaque finish of the metal frame, the two may look similar from the outside, but it is evident that there are differences between using a metal frame and In-ceram. VITA VM9 has been designed as a special ceramic featuring a fine structure or stabilized Zro2 substructures, and so the VITA VM9 excels in its light refraction and reflection behavior, which is similar to natural teeth. It also has outstanding chemical balance, which presents advantages such as considerably reduced accumulation of plaque on the ceramic surface.? This ultimately results in easier care and cleaning for the patient.

• 대한치과보철학회지
• /
• 제42권1호
• /
• pp.49-57
• /
• 2004

Statement of problem : The increased awareness of esthetics in dentistry has brought the esthetic consideration in prosthetic restorations . Dental ceramics offer better esthetics for use of prosthetic restorations. Unfortunately, dental ceramic materials are not always the most suitable candidate materials since their inherently brittle nature. In recent years, basic research in ceramic science has led to the recognition or several approaches to strengthen and to enhance esthetics of ceramics. Several all ceramic systems use ceramic core and porcelain build up structures . Ceramic cores influence to strength of all ceramic crowns . So the strength of ceramic cores is important to all ceramic crowns. Purpose : The purpose of this study is to estimate the flexural strength of ceramic cores in some all ceramic systems. Material and method : A biaxial flexure test was conducted on three groups(Cergo, Empress 2, In-Ceram). Each group consisted of 30 discs of nearly identical dimension with a 0.5mm, 1.0mm, 1.5mm thickness and 12mm in diameter. The fracture load was recorded by Instron. Analysis of valiance(ANOVA) and Tukey's tests were performed using SAS statistical software. Results : 1.5mm thickness of specimens were significantly stronger than 0.5mm and 1.0mm thickness of specimens in Cergo and In-Ceram. But each sepecimen group of Empress 2 was no significantly strength by thickness. In order of In-Ceram, Empress 2 and Cergo has significantly stronger strength in the same thickness. Conclusion : In-Ceram is the strongest ceramic material in 3 materials. All the materials can be used according to the required characters.

• 대한치과보철학회지
• /
• 제33권4호
• /
• pp.611-633
• /
• 1995

The pupose of this study was to compare the fracture strength of five kinds of all-ceramic crowns(Vintage, Dicor Empress-staining, Empress-layering, In-Ceram) luted with glass ionomer cerment and composite resin cement and to evaluate the effect of cements on the fracture stregth of all ceramic crowns. Five groups of twelve uniform sized all-ceramic crown specimens were fabricated. Six specimens of each group were cemented with glass ionomer cement(Fuji G.I. Cement) and the remaining six specimens of each group were etched, silane-treated, and cemented with composite resin cement(Bistite resin cement). The crowns were stored in water$(37^{\circ}C)$ for 1 day prior to loading in an Instron, using a steel ball(diameter 4mm) at a crosshead speed of 0.5mm/min. The crowns were angled $30^{\circ}$, so the steel ball contacted with the crowns 2mm lingual from the mid-incisal edge. The results obtained were summarized as follows ; 1. With G.I. cement, mean fracture load(Kg) Were : Intage : $18.33{\pm}1.47$ ; Empress-staining : $23.92{\pm}6.67$ ; Dicor : $24.0{\pm}5.81$ ; Empress-layering : $26.92{\pm}2.80$ ; In-Ceram : $51.58{\pm}6.87$ ; ANOVA revealed a significant difference existed(p<0.05) between the group A(Vintage, Dicor, Empress-staining, Empress-layering) and group B(In-Ceram). 2. With Resin cement, mean fracture load(Kg) were : Intage : $22.75{\pm}4.97$ ; Dicor : $42.75{\pm}7.07$ ; Empress-staining : $44.08{\pm}7.99$ ; Empresslayering : $50.42{\pm}5.43$ ; In-Ceram : $52.58{\pm}6.51$ ; ANOVA revealed a significatnt difference existed(p<0.05) between the group A(Vintage) and B(Dicor, Empress-staining Empress-alyering, In-Ceram). 3. Resin cement significantly increased the fracture strength of the all-ceramic crowns for Dicor(156%), Empress-staining(185%), Empress-alyering(187%)(p<0.05); but did not increase the fracture strength of Vintage(128%) and In-Ceram(101%)(p>0.05). 4. Majority of the all-ceramic crowns show a wedge fracture extending through proximal surfaces to an apex, usually apical third(with G.I. cement) or middle third(with Resin cement) of the facial surface.

• 대한치과기공학회지
• /
• 제23권2호
• /
• pp.189-202
• /
• 2002

A study on reflective spectrum between In-Ceram alumina plate(IAP) and IPS empress 2 plate were carried out in order to determine the difference of reflective spectrum rates between materials and between thicknesses of materials(0.8mm, 1.0mm, 1.2mm) by visible wave. The rates are measured by spectrophotometer(Top scan model TC-1800). And an analysis of ANOVA and paired sample t-test were carried out. The results are summarized as follows. 1. The reflective rates of IAP and IPS increased slowly as visible wave spectrum increased. 2. The difference of reflective rates of IAP between 0.8mm and 1.0mm is significant but a little(less than 1%). The differences of reflective rates of IAP between 0.8mm and l.2mm and between 1.0mm and l.2mm are significant(8%, 10% ). 3. The differences of reflective rates of IPS between 0.8mm and 1.0mm and between 0.8mm and 1.2mm and between 1.0mm and 1.2mm are significant(0.06 %, 0.01 %, 2 %). 4. The differences of reflective rates of 0.8mm, 1.0mm between IAP and IPS are significant but a little(less than 0.9%, 0.5%). The difference of reflective rates of l.2mm between IAP and IPS is significant and larger than the other thicknesses relatively(7 %).

• 대한치과보철학회지
• /
• 제36권6호
• /
• pp.888-899
• /
• 1998

In-Ceram system is one of contemporary esthetic all ceramic restorations and has relatively high flexural strength. The purpose of this study was to evaluate the marginal fidelity according to type of resin cement and measuring position, and to evaluate fracture strength according to type of resin cement. In this study, twenty seven In-Ceram crowns were fabricated on the metal master die of prepared maxillary right central incisor and devided into three groups. All specimens were cemented with Panavia 21 (group PV), Super-bond (group SB) and Lute-it (group LI) on the metal master die. After cementation, specimens were measured marginal gap between the margin of the In-Ceram crown and the finishing line of metal master die by using a stereomicroscope (SZ-ST, Olympus, Japan). Marginal gaps were recorded at the labial, lingual, mesial and distal measuring points on the metal master die. For the mesurement of fracture strength, lingual surfaces of cemented specimens were loaded at a distance of 1mm from incisal edge by using the Autograph S-2000 (Shimadzu, Japan). The results of marginal fidelity and fracture strength were statistically analyzed with the SPSS version 8.0 programs. The results of this study were as follows: 1. In comparison of marginal fidelity according to the measuring points, there was no significant difference. 2. The marginal fidelity according to the type of resin cement was decreased in order of group $LI\;(63.75{\mu}m),\;SB\;(77.78{\mu}m),\;PV\;(86.53{\mu}m)$, and there was significant difference between group LI and PV (p<0.05). 3. The fracture strength according to the type of resin cement was showed descending order of group $LI\;(60.00kg/cm^2),\;SB\;(56.80kg/cm^2),\;PV\;(56.11kg/m^2)$, but there was no significant difference.

• 대한치과보철학회지
• /
• 제33권4호
• /
• pp.693-704
• /
• 1995

This study was performed to evaluate effective surface conditioning method of In-Ceram core to improve bonding with resin cement. The surface of each sample was avraded with glass bead for 20 seconds and then subjected to one of the following conditions : no modification, sandblasting with $50{\mu}m$ slumimum oxide powders for 20 seconds, etching with 20% hydrofluoric acid for 5, 10, and 15 minutes(half of the etched samples were coated with silane), and sandblasting with $250{\mu}m$ aluminum oxide powders and silica coating whith Silicoater MD system(Kulzer, Germany). The surface morphology changes were examined with scanning electronic microscope(SEM. and the shear bond strength of In-Ceram core samples to resin cement(Panavis 21, Kurayay, Japan) were measured. It was concluded that : 1. By SEM observation, 20% HF acid etching did not create clear microretentive structure and surface roughness diminished with increace in etching time. Sandblasting was more effective than 20% hydrofluoric acid etching in producing microretentive structure. 2. The bond strengths of all In-Ceram core samples surface conditioned were increased that that of control group. 3. Silica coating showed higher bond strength than etching with 20% hydrofluoric acid. 4. The use of silane coating was more effective in improving bond strength than lengthening etching time.