• Resources Recycling
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• v.30 no.1
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• pp.53-59
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• 2021

Waste vinyl generated from household waste has been used as a solid refuse fuel (SRF) due to the presence of impurities such as soil, metal, and glass; however, the amount of SRF used has been decreasing owing to recent environmental problems, thereby necessitating the need for recycling. In this study, the mixed recycled raw material produced from household waste vinyl and polyethylene (PE) single recycled raw material produced from agricultural waste vinyl were examined. Raw material analysis revealed that waste vinyl was mainly composed of polyethylene, and approximately 2% of ash remained in the mixed recycled raw material, whereas no ash was found in the PE single recycled raw material. In addition, the analysis of tensile strength according to the mixing ratio of the two recycled raw materials revealed that the highest tensile strength was approximately 16 MPa under the heat treatment temperature of 200 ℃, compression pressure of 30 MPa, and a mixing ratio of 3:7 (mixed:PE single). In addition, the highest bending strength was approximately 39 MPa under the heat treatment temperature of 200 ℃, compression pressure of 30 MPa, and a mixing ratio of 3:7 (mixed:PE single). Therefore, the possibility of recycling waste vinyl was suggested by investigating the change in strength characteristics according to the mixing ratio of the recycled raw materials.

• Journal of the Korean Applied Science and Technology
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• v.35 no.4
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• pp.1307-1319
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• 2018

As interests in the air pollution increases, many kinds of researches are underway on the reduction of air pollutants. The removal of nitrogen oxides from the emission gas of diesel vehicles using urea solution has shown a great effect. The quality of urea solution is strictly defined by domestic law, but the increase of impurities in urea solution reduces the effect of reducing nitrogen oxides. Therefore, in this study, the change of physical properties of urea solution was analyzed after heating the urea solution for a certain temperature and time. Also, the changes of physical properties of urea solution were analyzed according to kinds of storage container and temperature for storing the urea solution. After heating the urea solution for a certain period of time, the biuret content in urea solution increased and the content of urea decreased. As the urea content decreased, both density and refractive index decreased. In the storage stability test carried out at a constant temperature with iron and PET containers, no change in physical properties was observed.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.20 no.8
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• pp.649-656
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• 2019

Flux cored arc welding (FCAW), which is used widely in many fields, such as shipyards, bridge structures, construction machinery, and plant industry, is an alternative to shielded metal arc welding (SMAW). FCAW is used largely in the welding of carbon and alloy steel because it can be welded in all poses and obtain excellent quality in the field under a range of working conditions. In this study, the mechanical properties of welded parts were analyzed after different welding of SS400 and SM490A using FCAW. The following conclusions were drawn. The tensile test results satisfied the KS standard tensile strength in the range of 400~510 N/mm2 in all welding positions. The bending test confirmed that most of the specimens did not show surface breakage or other defects during bending and exhibited sufficient toughness, even after plastic deformation. The hardness test results were lower than the standard value of 350 Hv of KS B 0893. Similar to the hardness test, were greater than the KS reference value. The macro test revealed no internal flaws, non-metallic inclusions, bubbles or impurities on the entire cross section of the weld, and there were no concerns regarding lamination.

• Journal of the Korea Institute of Building Construction
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• v.19 no.2
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• pp.113-121
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• 2019

Single walled carbon nanotube (SWCNT) has been used as a material for reinforcing various advanced materials because it has superior mechanical properties. However, pure SWCNT that does not have any functional group has a hydrophobic character, and exists as bundles due to the strong Van der Waals attraction between each SWCNT. Due to these reasons, it is very difficult to disperse SWCNTs in the water. In this work, in order to use SWCNT for production of cementitious composites, SWCNT was first dispersed in water to make an aqueous solution. Sodium deoxycholate (DOC) and Sodium dodecyl sulfate (SDS) were chosen as surfactants, and the dosage of DOC and SDS were 2wt% and 1wt%, respectively. Sonication and ultracentrifugation were applied to separate each SWCNT and impurities. Using such processed SWCNT solutions, cement paste was prepared and its shear stress vs. strain rate relationship was studied. The yield stress and plastic viscosity of cement paste were obtained using Bingham model. According to the results in this work, cement pastes made with DOC and SDS showed similar rheological behavior to that of air entrained cement paste. While cement paste made with DOC 2 wt.% SWCNT solution showed similar rheological behavior to that of plain cement paste, cement paste made with SDS 1 wt.% SWCNT solution showed different rheological behavior showing much less yield stress than plain cement paste.

• Korean Chemical Engineering Research
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• v.59 no.4
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• pp.542-547
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• 2021

Glass lined impellers are corrosion resistant to most chemicals, including strong acids, and also have a smooth, non-stick surface, easy to clean and free from impurities in the process. Glass lined home base impeller is a multi-purpose impeller designed to stir a wide viscosity range of liquids from low viscosity fluids to high viscosity fluids, among others, cell culture, yeast culture, and beer fermentation pots, especially used for air-water system breathable stirring. The glass lining for HB impellers, which are simple in structure and competitive in performance, is essential to have upper and lower division in order to make the joint area between the impeller and shaft as small as possible. The upper and lower division of the impeller hardly affects the mixing performance, but the aeration performance. In this study, in order to optimize the shape of the Glass Lining HB impeller, a study was conducted on the effect of the angle between the upper and lower impellers, the clearance between the impellers, and the number of baffles on the aeration power. The optimal shape and baffle plate conditions for the Glass lined HB impeller were derived through the study results that the angle and the clearance between the upper and lower impellers decreased the ration of the power consumption with aeration P_g and that without aeration P₀, P_g/P₀.

• Applied Chemistry for Engineering
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• v.22 no.1
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• pp.67-71
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• 2011

The cathodic active material of $Li/SO_2Cl_2$ battery is $SO_2Cl_2$, which is the solvent of an electrolyte. It is referred to as a catholyte, a compound word of cathode and electrolyte. As the battery discharges, the catholyte burns out. And thus, the characteristics of the $SO_2Cl_2$ in the battery determine the capacity. In addition, the transition minimum voltage (TMV) and the voltage delay deviation of $Li/SO_2Cl_2$ battery are due to the passivation film formed by the reaction between an electrolyte and Li. Impurities in the electrolyte, such as moisture or heavy metal ions, will accelerate the growth of the passivation film. Therefore, a technology must be established to purify an electrolyte and to ensure the effectiveness of the purification method. In this research, $LiAlCl_4/SO_2Cl_2$ was manufactured using $AlCl_3$ and LiCl. Its concentration, the amount of moisture, and the metal amount were evaluated using an ionic conductivity meter, a colorimeter, and FT-IR.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.22 no.2
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• pp.378-385
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• 2021

The production of plum jangachi requires the cleaning of plums, immersion in saltwater, separation of seed and pulp, removal of impurities, and addition of sugar. In most farms, the separation of plum seed and pulp is carried out manually, requiring considerable labor, which is why plum jangachi is expensive. To solve this problem, this study designed and manufactured automatic, semi-automatic plum seed and pulp separators. During the design process, the characteristics were compared, and the machine power was determined through on-site test after manufacture. As a result, automatic machines used plums 180° arrayed and six reverse-edged blades, semi-automated plums 180° arrayed, and six blades, each with a 68% and 57% pulp recovery rate and a machine power of 80 kg/h and 62 kg/h respectively. Overall, the mechanization of plum processed food will reduce labor and increase the market value of plums compared to the previous method.

• Korean Journal of Clinical Laboratory Science
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• v.53 no.1
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• pp.1-10
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• 2021

Radiopharmaceuticals are drugs that contain radioisotopes and are used in the diagnosis, treatment, or investigation of diseases. Radiopharmaceuticals must be manufactured in compliance with good manufacturing practice regulations and subjected to quality control before they are administered to patients to ensure the safety of the drug. Radiopharmaceuticals for administration to humans need to be sterile and pyrogen-free. Hence, sterility tests and membrane filter integrity tests are carried out to confirm the asepticity of the finished drug product, and a bacterial endotoxin test conducted to assess contamination, if any, by pyrogens. The physical appearance and the absence of foreign insoluble substances should be confirmed by a visual inspection. The chemical purity, residual solvents, and pH should be evaluated because residual by-products and impurities in the finished product can be harmful to patients. The half-life, radiochemical purity, radionuclidic purity, and strength need to be assessed by analyzing the radiation emitted from radiopharmaceuticals to verify that the radioisotope contents are properly labeled on pharmaceuticals. Radiopharmaceuticals always carry the risk of radiation exposure. Therefore, the time taken for quality control tests should be minimized and care should be taken to prevent radiation exposure during handling. This review discusses the quality control procedures and acceptance criteria for a diagnostic radiopharmaceutical.

• Analytical Science and Technology
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• v.33 no.6
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• pp.262-273
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• 2020

A fluorine content analysis method for krill oils, which is a representative oil formulation in foods, was developed in compliance with the Korea Food and Drug Ministry's "Guidelines for Validation of Testing Methods Related to Food". Using this method for krill oils, the presence of impurities was evaluated via combustion-ion chromatography (C-IC). A review of published technical data on fluorine in krill oils showed that while the traditional wet potentiometric method was typically used, it was not reliable. Moreover, there was no food testing/analysis laboratory in Korea to perform a fluorine test analysis on such an oil matrix. Therefore, we identified halogen (fluorine) tests, developed to national and international standards, and developed a test method suitable for krill oils by selecting a C-IC method that is sufficiently applicable to the oil matrix. Based on the characteristics of the oil matrix, the optimal test method was established through various experiments by reviewing the concerns related to loss and interference in the preparation and introduction of samples. The fluorine content test was carried out on 11 krill oil products that were purchased online. Most products (with the exception of only one) were found to contain less than the reporting limit obtained by the test method. Furthermore, after additional testing, a high fluorine content of approximately 2,000 ~ 3,000 mg/kg was detected on the krill surface, although the concentration varied depending on the area of the krill. A comparison with samples from two ISO/IEC 17025 testing laboratories confirmed that there was no significant difference in the statistical analysis results obtained by ANOVA among the three laboratories. A testing guide for fluorine content analysis was completed.

• Korean Journal of Mineralogy and Petrology
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• v.35 no.2
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• pp.141-151
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• 2022

The 16 natural zeolites collected from Mongolia (6 types), the United States (1 type), and Korea (9 types) were characterized by XRD, XRF, TGA, DTA, and CEC analysis. All 16 samples are composite minerals. Two or more mineral phases co-exist and consist primarily of minerals such as clinoptilolite, heulandite, mordenite, and chabazite. In certain samples, minerals like illite and quartz were present as impurities. The XRF analysis showed that the 16 natural zeolites contain SiO₂, Al₂O₃, K₂O, CaO, Na₂O, MgO, and Fe₂O₃ oxides. The cation exchange capacity of the U-1 sample was 223.3 meg/100 g, which is higher than the rest of the samples. M-6 sample in Mongolian natural zeolite and K-1 sample in Korean natural zeolite showed the highest cation exchange capacity at 166.6 meg/100 g. As a result of thermal differential and thermos gravimetric analysis, all 16 samples showed excellent thermal stability up to 600℃.