• 산업기술연구
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• 제36권
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• pp.45-48
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• 2016

The purpose of this study is to evaluate and compare wettability and setting time of twelve polyvinylsiloxane impression pastes. For comparing the wettability, the contact angle of a water drop on the impression materials was measured. It is important for impression materials to have higher wettability when trying to make impressions of interproximal spaces and gingival crevices. The higher wettability the better the material will flow into these spaces and the more accurate the impression. An ideal impression material will have adequate working time but a fast intraoral setting time. The clinician needs time to inject material into the sulcus, place the impression material into the tray and position it in the mouth, but the material should set rapidly to reduce time in the patient's mouth. It is considered that the results obtained in this study will provide guideline information for the manufacturing of impression materials and for selecting appropriate impression materials.

• 대한치과보철학회지
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• 제38권2호
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• pp.191-199
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• 2000

Wettability of addition silicone impression material is very important property for making an accurate restoration. This study examined the impression quality in clinical condition and the wettability of impression and die material. Four commercially available addition silicone impression material (Express, Examix, Contrast, Perfect) and three die materials (Die-Keen, Vel-Mix, Fuji-Rock) were studied. A total of 50 putty/wash and heavy body/wash impressions of wet intact permanent molar teeth were examined for definition of the gingival sulcus reproduction and then classified in quality ranking. The percentage of the sulcus reproduction ability of each material was calculated from the sulcus depths of cross-sectioned epoxy resin casts from the impressions and clinically measured sulcus depths, The same impression materials were used to produce 3 groups of die stone casts form void entrapment die had been exposed to milk. Voids in the impression body and stone casts ere counted under a stereoscopic microscope. From the experiment, the following results were obtained : 1. Sulcus reproduction ability of additional silicone impression material were diminished in order of Express, Examix, Perfect, Contrast. The significant difference was found between Perfect and other material. Heavy body/wash combination was superior In putty/wash method n Perfect impression material. 2. In direct observation, Contrast showed least void in impression body but correlations ere not found between sulcus reproduction and void production. 3. In void entrapment laboratory test, wettability were diminished in order of Examix, Contrast, Express, Perfect. Clinical impression recording seems not to correlate with laboratory test. 4. The wettability of die material to impression material was not different in Express, Examix, Contrast. But, in Perfect, Die-Keen had superior wettability to others.

• 대한치과보철학회지
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• 제35권3호
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• pp.535-543
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• 1997

In order to compare the accuracy of impression technique using the addition silicone putty and improved heavy body material, impression were taken for the natural 6 maxillary anterior teeth, and for the metal mast model that has full arch shape with 4 cylindrical abutment teeth. Marginal gingiva was retracted by routine method using retraction cord, and two techniques were tried to compare the length of impression materials in the gingival sulcus. This was aimed to see the effect of viscosity and hydraulic pressure of impression materials for the subgingival impression. Impressions for the full arch-shaped metal master model were taken to compare the linear stability of the different impression materials and their related techniques. The conclusions were as belows : 1. The one-step impression technique showed longer extension of impression material in gingival sulcus than two-step impression technique. 2. High viscosity and hydraulic pressure of impression material were useful to take subgingival impression. 3. There was no statistically significant difference for the two-dimensional accuracy of impression technique, but two-step technique showed better trend than one-step technique.

• 대한치과의사협회지
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• 제41권1호통권404호
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• pp.35-41
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• 2003

Wettability of addition silicone impression material is very important property for making an accurate restoration. This study examined theimpression quality in clinical condition and the wettability of impression material. Three commercially available addition silicone impression material (Imprint; 3M, USA, Examix; GC, Japan, Perfect; Handae, Korea) were studied. A total of 90 putty/wash impressions of semi-dried premolars and wet molar teeth were examined for void production in impression body. The percentae of the sulcus reproduction ability of each material was calculated from the sulcus depths of cross-sectioned casts from the impressions with stereomicroscope. Three impression materials were used to produce die stone casts from vcid entrapment die. Voids in the stone casts were counted with the stereomicroscpe. From the experiment, the following results were obtained: 1. In direct observation, Imprint showed greatest numbers of void in impression body (P<.001).However, correlations were not found between sulcus reproduction and void production. 2. Sulcus reproduction ability of additional silicone impression material was diminished in order of Imprint, Examix, Perfect. The significant difference was found between Imprint and other material (P<.001). 3. In void entrapment laboratory test, void productions was diminished in order of Examix, Imprint, Perfect. All voids in casts were less in delayed poured cast than immediately poured cast. 4. Especially, the stone pouring time of Perfect impression material should be delayed.

• 대한치과보철학회지
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• 제33권3호
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• pp.569-583
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• 1995

Disinfection of dental impressions are necessary due to contamination with patient’s saliva and blood, which is a potential for cross-infection. The purpose of this study was to evaluate the effects of disinfection of four hydrophilic rubber impression materials with three disinfecting solutions, on the dimensional stability and surface hardness of improved stone casts. Three hydrophilic vinyl polysiloxane impression materials(Express, Reprosil, Exafine) and one polyether impression material(Impregum-F) were mixed according to the manufacturer’s directions and impressions were made on a ADA specification No. 19 stainless-steeldie. On removal of the impressions, each impression was immersed in one of the disinfectants(Banicide, Potadine, Clorox) for 10 minutes. After disinfection, type IV improved stone. casts were poured. On this cast, the linear dimension and surface hardness were measuredusing a Measurescope(Nikon, Japan) and a Barcol hardness tester(Barber, Colman Co U. S. A). The results were as follows : 1. The improved stone casts from disinfected Reprosil and Impregum-F impression material did not show dimensional changes(P>0.01). Those from disinfected Express and Exafine impression material showed dimensional changes(P<0.01). The amount of shrinkage was not clinically significant. 2. The improved stone casts from disinfected Express impression material did not exhibit changes in surface hardness(P>0.01), but those from disinfected Reprosil, Exafine, Imp regnum-F impression material showed changes in surface hardness(P<0.01). 3. The dimensinal stability and surface hardness of the improved stone casts were satisfactory using Banicide on Express, all disinfectants used in this study on Reprosil, Potadin and Clorox on Exafine, Banicide and Clorox on Impregum-F. According to these results, immersion disinfection of hydrophilic rubber impression mate rials did not adversely affect the resultant casts. Nevertheless compatibility tests of impression materials and disinfectants should be done when disinfecting impressions.

• The Journal of Advanced Prosthodontics
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• 제3권4호
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• pp.177-185
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• 2011

PURPOSE. The aim of this study was to evaluate the effect of dimensional stability of splinting material on the accuracy of master casts. MATERIALS AND METHODS. A stainless steel metal model with 6 implants embedded was used as a master model. Implant level impressions were made after square impression copings were splinted using 5 different techniques as follows. (1) Splinted with autopolymerizing resin and sectioned, reconnected to compensate polymerization shrinkage before the impression procedure. (2) Splinted with autopolymerizing resin just before impression procedure. (3) Primary impression made with impression plaster and secondary impression were made over with polyether impression material. (4) Splinted with impression plaster. (5) Splinted with VPS bite registration material. From master model, 5 impressions and 5 experimental casts, total 25 casts were made for each of 5 splinting methods. The distortion values of each splinting methods were measured using coordinate measuring machine, capable of recordings in the x-, y-, z- axes. A one-way analysis of variance (ANOVA) at a confidence level of 95% was used to evaluate the data and Tukey's studentized range test was used to determine significant differences between the groups. RESULTS. Group 1 showed best accuracy followed by Group 3 & 4. Group 2 and 5 showed relatively larger distortion value than other groups. No significant difference was found between group 3, 4, 5 in x-axis, group 2, 3, 4 in y-axis and group 1, 3, 4, 5 in z-axis (P<.0001). CONCLUSION. Both Splinting impression copings with autopolymerizing resin following compensation of polymerization shrinkage and splinting method with impression plaster can enhance the accuracy of master cast and impression plaster can be used simple and effective splinting material for implant impression procedure.

• 한국치위생학회지
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• 제8권2호
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• pp.53-66
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• 2008

There was to purpose of this study improves analyzing cause that prosthesis brings bite engaging that is inaccurate in patient's mouth, when supposed that all conducts that do in operatory and dental laboratory are perfect. Impression did check bite by alginate impression material and polymerization style silicon impression material that use usually in presence at a sickbed Irreversibility, hydrocolloid, alginate impression material washed in flowing water and poured anhydrite after wait about 8 minutes so that region that charge interest after impression check bite may become undoing. And hydrophile property addition polymerization style impression material poured anhydrite after blow 30 considering impression material dwell time and H2 gas occurrence time (5~15 minute) after have washed in flowing water. I got each 7 models, result that manufactures total 28 and measures by third dimension measuring instrument (Meteo, Korea) following sequence curing in tray holder and floor 1, By Alginate impression when is hardened in tray holder and when is hardened in the floor after do check bite, SPH 4, SPH5 all as there is synonymy appeared(P<0.05). By in case do not use average 0.1741 in case use tray holder in 0.0447 SPH5s in case do not use average 0.2838 pastas in case use tray holder in SPH4 0.0309, When did not use both SPH4 and SPH5 tray holder, when used tray holder, 1 appeared more greatly. 2. By amity sex addition polymerization style silicon impression when is hardened in tray holder after do check bite and when is hardened in the floor SPH 4, a11 of the SPH5s very big synonymy be(P>0.05). And in case use tray holder in 0.000657 pasta SPH5s in case do not use average 0.000129 pastas in case use tray holder in SPH4 average 0.000114 pastas, by in case do not use 0.000757, I appeared more greatly when used tray when did not use both SPH4 and SPH5 tray holder, but 1 appeared is not level to keep in mind(Table 8~9). 3 SPH4 was looked very big mindfulness in model that manufacture doing impression check bite by Alginate and model that do impression check bite by amity sex accessory penalty silicon without using tray holder(P< 0.001). I use tray holder and SPH4 did not appear synonymy in model that manufacture doing impression check bite by Alginate and model that do impression check bite by amity sex accessory penalty silicon(P>0.05). Study finding of above when see synthesis Alginate certainly tray holder use must and I could know that hardening method does not exert big influence on volume stability if remove impression sieve of excess because amity sex accessory penalty silicon passes over tray, Also, Alginate impression material previewed can get heading a conspiracy style that volume stability of accessory penalty silicon impression material degree is if use tray holder.

• Elastomers and Composites
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• 제36권2호
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• pp.102-110
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• 2001

Nonylphenoxy poly(ethylene) ethanol homologues, caster oil poly(ethylene) ethanol homo-logues 및 sodium perfluoroalkyl carboxylates의 세 가지 종류 계면활성제를 사용하여 고무인상재의 젖음성 향상 연구를 수행한 결과 불소 관능기가 도입된 sodium perfluoroalkyl carboxylates 계면활성제의 경우 다른 계면활성제를 사용한 경우에 비해 고무인상재의 초기 표면에너지 값은 유사했으나 평형상태에 이른 후의 표면에너지 값이 낮아 치아와의 젖음성이 가장 우수한 것으로 나타났다. 또한, 수소가스의 발생을 억제시키고 미세부 재현성을 높이기 위해 소포제를 사용한 결과 젖음성이 향상된 sodium perfluoroalkyl carboxylates를 포함한 조성에 소포제를 첨가할 경우 인열물성이 약 40% 이상 증가하였는데, 이는 소포제가 고무인상재 내부의 반응으로 생성되는 수소가스의 발생을 억제하기 때문이다. 따라서, 소포제는 고무인상재의 표면특성에는 크게 영향을 미치지 않으면서 인상재 내부에 발생되는 기포를 효과적으로 억제 혹은 제거하여 고무 인상재의 기계적물성을 향상시킴을 알 수 있었다.

• 구강회복응용과학지
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• 제21권1호
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• pp.83-93
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• 2005

This study was designed to investigate the fitness of adjustable dental impression trays. The size and shape of these trays were designed from the results of the dental arch size of Korean adults. Tray samples were made by CAD-CAM working. A hundred dental students(male:50, female:50) were selected for taking irreversible hydrocolloid impression using these trays. The author measured the width and length of impression material on the several measuring points. The results obtained were as follows : 1. Uniform impression material thickness was achieved by controlling the width of the tray using stops and beveled guides. 2. In the upper tray, the impression material thickness was measured to be rather great showing thickness of the labial vestibule 8.3 mm and the midpalatal part 8.6 mm. 3. In the lower tray, length of the impression material of the labial vestibule of first, second premolar contact point was 7.8 mm, and thickness of the lingual part of premolars(1.8 mm) and molars(1.9 mm) showed small values. 4. In the lower tray, the impression material thickness of the buccal shelf area(0.2 mm) and the retromolar pad area(0.6 mm) was measured to be too small.

• 대한치과보철학회지
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• 제44권4호
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• pp.477-487
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• 2006

Purpose : this study was to evaluate the fitness of adjustable dental impression trays on the Koreans : the trays used in the previous study by Kim et al. as part of the dental adjustable tray development project were improved and modified. Material and method: The patterns of tray were made through CAD-CAM process, and a simple silicone-base molds were made from them. The trial products were reproduced by pouring polyurethane into these molds. 30 male students(Wonkwang University, Dental College) and 30 female students (Wonkwang Health Science College, Department of Dental Hygiene) were selected and Reversible hydrocolloid impression materials were used for this study. The fitness of the trays was evaluated by measuring the width and length of impression materials of each measurement sites. Results and conclusion : 1. In adapting the trays inside the mouth, a uniform width of impression material(3 $\sim$ 6mm) was obtained in most sites due to the tooth stops and the inclined planes accommodating the width of the tray 2. The thickness of impression material in the central part of the palate was a mean 9.8mm, which turned out to be somewhat thick. 3. In the mandible. the thickness of the impression material in the lingual side inferior to the contact point of the 1st and 2nd molars was 2.7mm, and the thickness of the material in the lingual side of the rearmost margin was 2.5 mm. The thickness of the impression material of these areas was relatively thin.