• Title/Summary/Keyword: Impregnation method

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C3H8 Gas Sensitivity of Pd, Pt-$SnO_2$ Gas Sensor with Varying Impregnation Method (함침 방법의 차이에 따른 Pd, Pt-$SnO_2$의 프로판 가스 감응성 변화)

  • 이종흔;박순자
    • Journal of the Korean Ceramic Society
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    • v.27 no.5
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    • pp.638-644
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    • 1990
  • The C3H8 gas sensitivities of SnO2, Pd-SnO2, Pt-SnO2 gas sensor are looked over with the impregnation method of PdCl2, H2PtCl6 solution on SnO2. The Cl- ion due to incomplete decomposition of PdCl2 at 80$0^{\circ}C$ for 30 min decrease the C3H8 gas sensitivity of SnO2, and the sensitivity is increased by the impreganation of H2PtCl6 solution on SnO2 because of its lower decomposition temperature compared with PdCl2. The C3H8 gas sensitivities of Pd-SnO2, Pt-SnO2 impregnated slightly after 1st sintering are larger than that of pure SnO2 sensor because very small amount of Cl- ion exist in sample due to smaller amount of impregnaiton.

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Study on the Hybridization of Polymer-macromers for the Dimensional Stabilization of Woody Materials (치수안정화를 위한 목질재료의 고분자 하이브리드화에 관한 연구)

  • Lim, Kie-Pyo;Cho, Chong-Su;Kim, Ik-Joo;Na, Eun-Sun
    • Journal of the Korean Wood Science and Technology
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    • v.23 no.4
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    • pp.1-9
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    • 1995
  • This study was carried out to experiment the dimensional stabilization of woods of red pine (Pinus densiflora S. et Z.) and sugi(Cryptomeria japonica D. Don) by vacuum impregnation of polyehtylene glycols(PEG) with mo. wt. 200, 400, 600, 1000; polypropylene glycols (PPG) with mo. wt. 425,725 ; PEG-acryloylates, and PPG-acryloylates synthesized, and then by water soaking. The results obtained are as follows: 1. The density of sapwood and heartwood was different from each other in both species. 2. The PEG and PEG-macromers with lower molecular weight by impregnation has increased the density of wood specimens more higher, thereby caused their higher volume expansion, and those with higher molecular weight than 600 has tended to down their density increment. 3. Before and after water soaking, the density decrease of specimen impregnated was high in woods impregnated with simple PEG and PPG, while lower in specimens impregnated with PEG-macromers and PPG-macromers. 4. So PEG-macromer was expected to hold the original dimension of decayed wood for antiques, but it was necessary to develop another penetration method as well as aqueous solvent.

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Effects of the Methods of Polyethylene Glycol Impregnation and Drying on the Volumetric Shrinkage of Wood (Polyethylene Glycol 주입방법과 건조방법이 목재 부피수축률에 미치는 효과)

  • Lee, Won-Hee;Kang, Chun-Won;Hong, Seung-Hyun;Kang, Ho-Yang
    • Journal of the Korea Furniture Society
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    • v.27 no.1
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    • pp.43-48
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    • 2016
  • PEG (Polyethylene glycol) impregnation in wood reduces the occurrence of checking during kiln drying. The volumetric shrinkages of wood PEG impregnated by pressure (PEG-P) or soaking (PEG-S) methods, and oven-dried by vent (VD) or air-tight (AD) methods were measured and compared with the controls. The average oven-dry weight of PEG impregnated specimens was larger than that of the controls by 3.6 g, but was not influenced by the drying methods. The average of the total volumetric shrinkage of PEG-P-VD specimens was the least (2.3%), while that of CON-S-AD specimens was the largest (28.9%). Within a drying method the total volumetric shrinkage of the control was the largest followed by PEG-S and PEG-P specimens, which implied that residual PEG in wood restrained its shrinkage during drying.

Combustion Characteristics of Spruce Wood by Pressure Impregnation with Waterglass and Carbon Dioxide (물유리와 이산화탄소로 가압함침한 가문비 나무의 연소특성)

  • Park, Hyung-Ju;Lee, Se-Myeoung
    • Fire Science and Engineering
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    • v.26 no.4
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    • pp.18-23
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    • 2012
  • After produce the extracted wood to silicic acid gel, sodium carbonate and silicon dioxide with application of the making method for carbon dioxide, ignition time, ignition temperature, mass loss rate and critical heat flux are measured according to external radiation source (20, 25, 35 and 50 $kW/m^2$). From the results, pressure impregnation wood to use with water glass and carbon dioxide has fire retardant performance at heat flux (less than 20 $kW/m^2$) of Pre-Flashover fires. If we find out the excellent maxing ratio through continuously study, it might be decided to be able to be utilized as fire-retardant wood.

A Study on Characteristics of Concrete Impregnated with the Inorganic Surface Penetration Agents (무기계 표면침투제 용액으로 함침한 콘크리트의 특성 연구)

  • Bae, Ju-Seong;Kim, Hyeok-Jung;Park, Gook-Jun;Han, Jong-Won
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.14 no.1
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    • pp.71-77
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    • 2010
  • The concrete structure's durability and integrity is reduced owing to various deterioration phenomena. Therefore, it is important to prevent the deterioration phenomena. This study inquired into the various experimental results of specimens with different dilution concentration and impregnation time by the each solution to present the economic and efficient using method of the inorganic surface penetration agents. As a results, the reasonable dilution concentration and impregnation time of colloidal silica solutions are 15% and 5 minute and for the sodium alumina silicate solutions are 17% and 10 second.

Essential oil impregnation into graphene sponges with electric desorption control

  • Mendez, Jose Antonio Cabello;Bueno, Jose de Jesus Perez;Valencia, Jorge Ivan Mendoza;Soto, Jonathan Soto;Lopez, Maria Luisa Mendoza;Guerrero, Mizraim Uriel Flores
    • Advances in nano research
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    • v.12 no.6
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    • pp.629-638
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    • 2022
  • This work shows the impregnation of scents using a graphene sponge (GS). This was functionalized by the modified Hummers method, pursuing to add different functional groups. It is proposed to achieve the release and seek to control it through electrical potential applied to the graphene sponge with essential oils. The graphene sponge was functionalized and steeped with two kinds of oil. The electrochemical study demonstrates the variation in the electrochemical behaviour of the functionalized graphene sponge without and impregnated with oil. The release of the oil and its aromatic scents was carried out by applying an electrical potential of 30 V, with a release rate of 1.86 mg/min. The heating of the sample that causes the release of oil, associated with the electrical resistance of the system, reaches temperatures of about 150℃. The essential oils, graphene sponge, surfactant, graphene sponge with essential oils, graphene sponge recuperated after applying electric potential, graphene sponge recovered by temperature and dipropylene glycol (DPG) were characterized using Fourier transformed infrared spectroscopy (FTIR), digital microscopy, and x-ray photoelectron spectroscopy (XPS).

Preparation of Porous Mullite-Corundum Ceramics Via Organic Foam Impregnation

  • Zhou, Xianzhi;Zhu, Shaofeng;Wang, Yuxi;Zhang, Tong
    • Korean Journal of Materials Research
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    • v.32 no.2
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    • pp.85-93
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    • 2022
  • Porous mullite-corundum ceramics were prepared using organic foam impregnation method with alumina and silica as raw materials. The influence of alkaline treatment and surfactant modification on polyurethane foam were studied. Effects of sintering process and material composition on porous mullite-corundum ceramics were investigated. The results show that the hang-pulp quantity of polyurethane foam increases with alkaline treatment. After treatment with 3 wt% SDS solution, the hang-pulp quantity of polyurethane foam further improved. Open porosity of sample decreased with elevation of sintering temperature and holding time, and compressive strength of sample showed a trend opposite to the change of porosity. The open porosity of the sample was enhanced by the increase of m(Al2O3/SiO2); the compressive strength decreased with increase of m(Al2O3/SiO2). However, when m(Al2O3/SiO2) was 2.5, the compressive strength of the sample reached 6.23 MPa, and the open porosity of the sample was 80.7 %.

Pt Electrocatalysts Composited on Electro-Spun Pt Nanowires for Direct Methanol Fuel Cells

  • An, Geon-Hyoung;Ahn, Hyo-Jin
    • Korean Journal of Materials Research
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    • v.22 no.8
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    • pp.421-425
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    • 2012
  • Two types of Pt nanoparticle electrocatalysts were composited on Pt nanowires by a combination of an electrospinning method and an impregnation method with NaBH4 as a reducing agent. The structural properties and electrocatalytic activities for methanol electro-oxidation in direct methanol fuel cells were investigated by means of scanning electron microscopy (SEM), high-resolution transmission electron microscopy (HRTEM), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and cyclic voltammetry. In particular, SEM, HRTEM, XRD, and XPS results indicate that the metallic Pt nanoparticles with polycrystalline property are uniformly decorated on the electro-spun Pt nanowires. In order to investigate the catalytic activity of the Pt nanoparticles decorated on the electro-spun Pt nanowires, two types of 20 wt% Pt nanoparticles and 40 wt% Pt nanoparticles decorated on the electro-spun Pt nanowires were fabricated. In addition, for comparison, single Pt nanowires were fabricated via an electrospinning method without an impregnation method. As a result, the cyclic voltammetry and chronoamperometry results demonstrate that the electrode containing 40 wt% Pt nanoparticles exhibits the best catalytic activity for methanol electro-oxidation and the highest electrochemical stability among the single Pt nanowires, the 20 wt% Pt nanoparticles decorated with Pt nanowires, and the 40 wt% Pt nanoparticles decorated with Pt nanowires studied for use in direct methanol fuel cells.

Effect of Textile Pattern on Mechanical and Impregnation Properties of Glass Fiber/Thermoplastic Composite (유리 섬유/열가소성 복합 재료의 기계적 및 함침 특성에 대한 직물 패턴의 영향)

  • Kim, Neul-Sae-Rom;Lee, Eun-Soo;Jang, Yeong-Jin;Kwon, Dong-Jun;Yang, Seong Baek;Yeom, Jung-Hyun
    • Composites Research
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    • v.31 no.6
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    • pp.317-322
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    • 2018
  • In various industry, the composite is tried to be applied to products and thermoplastic based composite is in the spotlight because this composite can be recycled. The use of continuous fiber thermoplastic (CFT) method increased gradually than long fiber thermoplastic (LFT). In this study, tensile, flexural, and impact test of different array types of glass fiber (GF)/thermoplastic composites were performed to compare with GF array. Impregnation property between GF mat and thermoplastic was determined using computed tomography (CT). At CFT method, thermoplastic film is not wet into GF roving and many voids are appeared into composite. This phenomenon affects to decrease mechanical properties. Plain pattern GF mat was the best mechanical and impregnation properties that distance between two roving was set closely to $100{\mu}m$.