• Macromolecular Research
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• v.12 no.6
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• pp.545-552
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• 2004

The long-term stability of sulfonic acid-containing polyimides has been investigated. The hydrolytic degradation of homopolyimide and the block copolyimide comprising $27\;mol\%$ of 2,2'-bis(trifluoromethyl)benzidine and $9\;mol\%$ of m-phenylenediamine (BTFMB27mPl0[7/(3+1)]), was quantified through viscosity measurements and FT-IR spectroscopic analyses. The viscosity decrease with respect to time and the degradation rate were similar. The degrees of degradation with respect to time under ambient conditions and at elevated temperature in water were monitored by FT-IR spectroscopy. A new absorption peak was observed at $1786\;cm^{-1},$ which we corresponds to the presence of anhydride end groups formed by hydrolytic scission of the imide rings.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.19 no.10
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• pp.930-934
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• 2006

This paper reports a change of carbon nanotubes(CNTs) properties by post-treatment process after growth of CNTs. CNTs were treated by thermal method and solution method, and then investigated in detail using field emission scanning electron microscopy(FE-SEM), high resolution transmission scanning electron microscopy(HR-TEM), RAMAN spectroscopy, and Fourier Transform Infrared Spectrometer (FT-IR). FT-IR spectra showed that the amount of hydroxyl generated on surface of CNTs were changed with post-treatment condition. FE-SEM and TEM images were shown CNTs diameter and density variations were dependent with their treatment conditions. RAMAN spectroscopy was shown that carbon nanotubes structure vary with treatment conditions.

• Journal of the Korean Ceramic Society
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• v.25 no.1
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• pp.27-34
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• 1988

In order to investigate the reason of changes in the physical properties of glasses near the region for which R(Ga/Na)=1, spectroscopic studies using FT-IR and Raman spectroscopy have been carried out on Na2O.2SiO2 glass with addition of Ga2O3 from 0 to 35 mole %, i.e., from R=0 to 1.61. The main purpose of this work is to investigate the coordination number of Ga3+ in glass with variation of glass composition and to determine the existence of tricluster in the Ga-rich region for which R>1.0 in Na2O-Ga2O3-SiO2 system.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 1998.10a
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• pp.306-312
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• 1998

This paper describes syntheses of thickener for di-urea grease using constant velocity joint. The thickeners of di-urea grease were synthesized by reaction of diisocyanate with various alkylamines, hexylamine, octylamine, stearylamine and cyclohexylamine at high temperatxire. The synthesized thickener were analyzed by FT-IR spectroscopy and two kinds of Mass spectroscopy (EI & FAB). Dropping point and Consistency of synthesized di-urea grease were determined.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.13 no.1
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• pp.41-45
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• 2003

Infrared spectroscopy is a powerful tool for gem identification and research. Therefore, this study was focused to a method of the identification of amethyst, citrine, rock quartz and jadeite by the FT-IR. The FT-IR measurement was very effective in judgement of amethyst, citrine and rock quartz whether they are natural and synthetic. And FT-IR was very useful for the distinguishment of the natural jadeite (A-Jade) from wax/polymer-impregnated jadeite (B-Jade). Such technique will be helpful to identify new challenges present by treatments and synthetics.

• 연구논문집
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• s.30
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• pp.43-56
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• 2000

N-IR spectroscopy technology is very useful. And, the technology has wide application range. In the range, we know that single beam type silica analyzer has some handicap. So we were studied Splitted beam type silica analyzer. This dissertation have been discuss about system structure, system fundamentals and performance test. At the test, we were study in the spectral interference of NH3. We know that existing system had some problem. It is structural frailties of single beam type. Therefore we were study for Splitted beam type structure. And we obtain a good result. We have $\pm$5% accuracy and 0.5 ppb level measuring range. But, we have a question. It is ppt level measuring technology by the laser beam spectroscopy.

• Publications of The Korean Astronomical Society
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• v.32 no.1
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• pp.135-139
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• 2017

We have performed systematic studies of the properties of dust in various environments of nearby galaxies with AKARI. The unique capabilities of AKARI, such as near-infrared (near-IR) spectroscopy combined with all-sky coverage in the mid- and far-IR, enable us to study processing of dust, particularly carbonaceous grains includings polycyclic aromatic hydrocarbons (PAHs), for unbiased samples of nearby galaxies. In this paper, we first review our recent results on individual galaxies, highlighting the uniqueness of AKARI data for studies of nearby galaxies. Then we present results of our systematic studies on nearby starburst and early-type galaxies. From the former study based on the near-IR spectroscopy and mid-IR all-sky survey data, we find that the properties of PAHs change systematically from IR galaxies to ultraluminous IR galaxies, depending on the IR luminosity of a galaxy or galaxy population. From the latter study based on the mid- and far-IR all-sky survey data, we find that there is a global correlation between the amounts of dust and old stars in early-type galaxies, giving an observational constraint on the origin of the dust.

• Korean Journal of Metals and Materials
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• v.46 no.11
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• pp.755-761
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• 2008

We fabricated thermally evaporated 10 nm-Ni/1 nm-Ir/(poly)Si films to investigate the energy saving property of silicides formed by rapid thermal annealing (RTA) at the temperature range of $300{\sim}1200^{\circ}C$ for 40 seconds. Moreover, we fabricated 100 nm-thick ITO/(poly)Si films with an rf-sputter as references. A transmission electron microscope (TEM) and an X-ray diffractometer were used to determine cross-sectional microstructure and phase changes. A UV-VIS-NIR and FT-IR (Fourier transform infrared spectroscopy) were employed for near-IR and middle-IR absorbance. Through TEM analysis, we confirmed 20~65 nm-thick silicide layers formed on the single and polycrystalline silicon substrates. Ir-inserted nickel silicide on single crystalline substrate showed almost the same absorbance in near IR region as well as ITO, but Ir-inserted nickel silicide on polycrystalline substrate, which had the uniform absorbance in specific region, showed better absorbance in near IR region than ITO. The Ir-inserted nickel silicide on polycrystalline substrate particularly showed better absorbance in middle IR region than ITO. The results imply that nano-thick Ir-inserted nickel silicides may have excellent absorbing capacity in near-IR and middle-IR region.

• Journal of the Korean Chemical Society
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• v.39 no.7
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• pp.559-563
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• 1995

The three metabolites, Germacrene alcohol(1), Aaptamine(2) and Hexacyclic terpene(3) were isolated from Marine Sponge Luffariella sp., collected in October 1992, Manado Bay, Sulawesi in Indonesia showed in vitro activity against KB cancer cell line, and structure assignment for 1 was corrected by comparison of their spectral data with the literature $values^1$. Their structure were elucidated by $^1H$, $^13C$ NMR, $^1H$ $^13C$(1 bond) Heteronuclear Multiple Quantum Coherence Spectroscopy$(HMQC)^2$, $^1H$ $^13C$(2 and 3 bond) Heteronuclear Multiple Bond Correlation Spectroscopy$(HMBC)^3$, Electron Impact Mass Spectroscopy(EI ms), Ultra-violet Spectroscopy(UV) and Infrared Spectroscopy(IR).

• Plant Journal
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• v.16 no.3
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• pp.47-52
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• 2020

This study investigated the methodologies to enhance the corrosion resistance and the ways to measure for subsea equipment made of aluminum. The methodologies for the anticorrosion were cathodic protection, conversion coating, anodizing and organic coating. The simply analyzed ways to measure the corrosion resistance were Scanning Electron Microscope (SEM), Electrochemical Impedance Spectroscopy (EIS), Glow discharge optical emission spectrum spectroscopy (GD-OES), Fourier Transform Infrared Spectroscopy (FT-IR), Transmission Electron Microscopy (TEM), X-ray Photoelectron Spectroscopy (XPS), Scanning Vibrating Electrode Technique (SVET), contact angle and interfacial tension. The most widely used tools for increasing the corrosion resistance were the anodizing and the organic coating. Many ways were evenly used to measure corrosion. The methods more frequently utilized were SEM for the surface investigation and the contact angle to evaluate the corrosion resistance.