• Title/Summary/Keyword: Hybrid Bonding

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CHANGES OF MARGINAL ADAPTATION TO THE CAVITY FLOOR OF LIGHT-CURED GLASS IONOMER CEMENT BASE AFTER APPLICATION OF A COMPOSITE RESTORATION (복합레진 적용에 따른 광중합형 글라스아이오노머 시멘트의 변연 적합도의 변화)

  • Lee, Gye-Young;Lee, Kwang-Won;Park, Soo-Joung
    • Restorative Dentistry and Endodontics
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    • v.24 no.1
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    • pp.136-146
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    • 1999
  • The purpose of this study was to estimate the changes of marginal adaptation to the cavity floor of light-cured glass ionomer cement base after application of a composite restoration. Eighty non-carious extracted human molars were used in the present study. Circular cavities were prepared on the center of the exposed dentin surface to 0.5mm, 1.0mm, 1.5mm, 2.0mm in depth and the prepared cavities were pretreated with Dentin conditioner and filled with Fuji II LC(GC Int. Co., Japan). They randomly assigned into 3 groups according to the difference in application of a composite restoration; Group 1(control group): only glass ionomer base, Group 2: The application of a composite restoration surrounded by dentin with class I cavity over glass ionomer base after conventional dentin bonding to the exposed dentin and glass ionomer base, Group 3: The application of composite restoration not-surrounded by dentin over glass ionomer base after conventional dentin bonding to the exposed dentin and glass ionomer base. To examine the interface between cavity floor and light-cured glass ionomer cement base, each groups were sectioned vertically through the center of restorations with diamond saw and the gap size(${\mu}m$) of interface measured by SEM. The results were analyzed by using One Way ANOVA. The results were as follows: 1. Good adaptation between glass ionomer cement base and cavity floor was showed in specimens with 0.5mm, 1.0mm depth base of control group. But in specimens with 1.5mm, 2.0mm depth base of control group, the gap was measured about $15{\mu}m$, $40{\mu}m$ respectively. 2. Gap size in group 2 was significantly higher than that in control group(P<0.05). 3. Gap size in group 3 was significantly higher than that in control group and group 2(P<0.05). 4. It was possible to observe the good adaptation between glass ionomer cement base and dentin which was intermediated with 4-10${\mu}m$ hybrid layer in specimens with 0.5mm, 1.0mm depth base of control group. Cohesive fracture within cement base was observed in all specimens which had the gap between glass ionomer cement base & dentin. 5. It was possible to observe the gap formation between cement base and bonding agent and between composite resin and dentin in all specimens of group 2.

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A SCANNING ELECTRON MICROSCOPIC STUDY OF BONDING ASPECTS TO THE SCLEROTIC DENTIN (경화된 상아질의 접합 양상에 관한 주사전자현미경적 연구)

  • Lee, Rin;Lee, Hyeong-Il;Lee, Kwang-Won;Son, Ho-Hyun
    • Restorative Dentistry and Endodontics
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    • v.22 no.1
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    • pp.228-243
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    • 1997
  • The changes of microstructures, morphology of sclerotic dentin and bonding aspects generated by an adhesive resin was investigated. Incisors and premolars showing natural cervical abrasions were collected and conditioned with 10 % phosphoric acid or 10 % maleic acid. The sclerotic dentin specimens were then rinsed and blot-dried and applied with dentin adhesive (All Bond 2) to the conditioned dentin surface. To examine the morphologic change of the sclerotic dentin specimen after etching and bonding procedure, the treated specimens were examined by SEM. To analyze the chemical composition of sclerotic dentin and crystals occluding dentinal tubules, the sclerotic dentin specimen was powdered and examined with X-ray Diffractometer. To investigate the Ca/P weight percent ratio within the dentinal tubules, the sclerotic dentin specimen was fractured perpendicularly to the long axis of the tooth from the center of cervical abrasion lesion and then examined with EDX(Energy Dispersive X-ray) microanalyzer. The results were as follows : 1. The increased width of peritubular dentin and the depositions of the irregular amorphous materials within the dentinal tubules were showed in the sclerotic dentin specimens. 2. After the treatment of sclerotic dentin specimen with 10 % phosphoric acid or 10 % maleic acid, the lateral side of tubules rather than cross-sectional tubule openings was showed exclusively at the incisal and gingival incline of the specimens. 3. After the treatment of sclerotic dentin specimen with 10 % phosphoric acid or 10 % maleic acid, the hybrid layer was not formed evidently and the resin tag was not formed or shortly penetrated into the tubules with the thinner diameter. 4. According to the results of XRD analysis of the sclerotic dentin specimen, Hydroxyapatite and Octacalcium phosphate were predominent, however, Whitlockite crystals were rare. 5. The mean Ca/P weight percent ratio analysed from 5 fractured sclerotic dentin specimens was $2.322{\pm}0.170$ at the intertubular dentin, $1.826{\pm}0.051$ within the dentinal tubule.

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mPW1PW91 Calculated Structures and IR Spectra of the Conformational Stereoisomers of C-Cyanophenyl Pyrogallol[4]arene

  • Ahn, Sangdoo;Park, Tae Jung;Choe, Jong-In
    • Bulletin of the Korean Chemical Society
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    • v.35 no.5
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    • pp.1323-1328
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    • 2014
  • Molecular structures of the various conformational stereoisomers of 2,8,14,20-cyanophenyl pyrogallol[4]arenes 1 were optimized using the mPW1PW91 (hybrid Hartree-Fock density functional) calculation method. The total electronic and Gibbs free energies and the normal vibrational frequencies of the different structures from three major conformations (CHAIR, TABLE, and 1,2-Alternate) of the four stereoisomers [1(rccc), 1(rcct), 1(rctt), and 1(rtct)] were analyzed. The mPW1PW91/6-31G(d,p) calculations suggested that $1(rcct)_{1,2-A}$, 1(rctt)CHAIR, and $1(rtct)_{CHAIR}$ were the more stable conformations of the respective stereoisomers. Hydrogen bonding is the primary factor for the relative stabilities of the various conformational isomers, and maximizing the ${\pi}-{\pi}$ interaction between the cyanophenyl rings is the secondary factor. The calculated IR spectra of the more stable conformers [$1(rctt)_{CHAIR}$, $1(rcct)_{1,2-A}$, $1(rtct)_{CHAIR}$] were compared with the experimental IR spectrum of $1(rtct)_{CHAIR}$.

Vibration Control of a Smart Cantilevered Beam Using Electro-Rheological Fluids and Piezoelectric Films Actuators (전기유동유체와 압전필름 액튜에이터를 이용한 스마트 외팔보의 진동제어)

  • Park, Y.K.;Park, S.B.
    • Journal of the Korean Society for Precision Engineering
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    • v.14 no.1
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    • pp.119-125
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    • 1997
  • This paper deals with an experimental investigation on an active vibration control of ahybrid smart structure(HSS) via an electro-rheological fluid actuator(ERFA) and a piezoelectric film actuator(PFA). Firstly, an HSS is constructed by inserting a silicone oil-based electro-rheological fluid into a hollow can- tilevered beam and perfectly bonding piezoelectric films ofn the upper and lower surfaces of the beam as an actuator and a sensor, respectively. The control scheme of the ERFA tuning stiffness and damping charac- teristics of the HSS with imposed electric fields is formulated as a function of excitation frequencies on the basis of field-dependent respnses. On the other hand, as for the control scheme of the PFA permitting control voltages to generate axial forces or bending moments for suppressing deflections of the HSS, a neuro sliding mode controller(NSC) is employed. Furthermore, an experimental implementation activating the ERFA and the PFA independently is established to carry out an active vibration control in both the transient and forced vibrations. The experimental results exhibit a superior ability of the gtbrid actuation system to tailor elastodynamic response characteristics of the HSS rather than a single class of actuator system alone.

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Flexural performance of wooden beams strengthened by composite plate

  • Tahar, Hassaine Daouadji;Abderezak, Rabahi;Rabia, Benferhat
    • Structural Monitoring and Maintenance
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    • v.7 no.3
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    • pp.233-259
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    • 2020
  • Using bonded fiber-reinforced polymer laminates for strengthening wooden structural members has been shown to be an effective and economical method. In this research, properties of suitable composite materials (sika wrap), adhesives and two ways of strengthening beams exposed to bending moment are presented. Passive or slack reinforcement is one way of strengthening. The most effective way of such a strengthening was to place reinforcement laminates in the stretched part of the wooden beam (lower part in our case), in order to investigate the effectiveness of externally bonding FRP to their soffits. The model is based on equilibrium and deformations compatibility requirements in and all parts of the strengthened beam, i.e., the wooden beam, the sika wrap composite plate and the adhesive layer. The theoretical predictions are compared with other existing solutions. This research is helpful for the understanding on mechanical behaviour of the interface and design of the composite-wooden hybrid structures. The results showed that the use of the new strengthening system enhances the performance of the wooden beam when compared with the traditional strengthening system.

A Study on 1024-QAM RF Transmission System using Channel Bonding Technologies for 8K-UHD Services (방송망 채널결합형 8K-UHDTV 1024-QAM RF 전송시스템 개발에 관한 연구)

  • Kim, Sung-Hoon;Choi, Jinsoo;Kim, Jinwoong
    • Proceedings of the Korean Society of Broadcast Engineers Conference
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    • 2011.07a
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    • pp.320-321
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    • 2011
  • 본 논문은 디지털 케이블전송망인 HFC(Hybrid Fiber and Coaxial)망 기반하에서 6MHz 다수의 방송채널결합 기술을 이용하여, 대용량 3D 및 8K-UHD 콘텐츠 전송을 위한 방송망 채널결합형 200Mbps 급 1024-QAM 송수신시스템 개발에 대하여 기술한다. H.264 비디오 부호화기를 사용하여 8K-UHDTV 및 3D/UHD 융합형 서비스를 시청자에게 제공하기 위해서는 약 120~160Mbps 의 대용량 데이터 전송률이 확보되어야 한다. 이와같이 대용량 3D/8K-UHDTV 콘텐츠를 전송하기 위해서는 상대적으로 채널환경이 우수한 HFC 디지털 케이블망을 이용한 대용량 실감미디어 콘텐츠 전송기법에 대한 연구가 주목 받고 있다. 본 논문에서는 FPGA 를 이용하여 HFC 망 기반에서 기존 OpenCalbe/DOCSIS 3.0 256-QAM 대비 약 30% 전송효율이 개선된 3D/8K-UHDTV 대용량 실감미디어 콘텐츠 전송을 위한 방송망 채널결합형 1024-QAM 송수신기 구현 및 개발에 관한 내용을 기술한다.

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Study on the Characteristic due to the Various Polarity based on the Carbon Contents in Organic Thin Film (유기물 박막에서 탄소 함량에 따라서 달라지는 분극의 변화에 따른 특성 변화에 대한 연구)

  • Oh, Teresa
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.14 no.9
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    • pp.2065-2070
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    • 2010
  • The diluted PMMA treated $SiO_2$ films as an passivation materials for semiconductor devices was researched by using the FTIR spectra. The diluted PMMA solution with various ratios changed the surface of $SiO_2$ film as the hydrophilic, hydrophobic or hybrid type properties. The sample 7 with little carbon content showed dramatically the chemical variation by the FTIR spectra analysis. Beacuse the little carbon with electrons decreased the polarity and surface energy on the $SiO_2$ film, and then became a stable bonding structure and decreased the leakage current. The FTIR spectra can define the detail variation due to the chemical reaction on the organic thin film, and help to research the characteristic of the organic materials.

A Study of Optical Characteristics Correlated with Low Dielectric Constant of SiOCH Thin Films Through Ellipsometry (Ellipsometry를 이용한 저 유전상수를 갖는 SiOCH박막의 광학특성 연구)

  • Park, Yong-Heon
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.23 no.3
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    • pp.228-233
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    • 2010
  • We studied the optical characteristics correlated with low dielectric constants of low-k SiOCH thin films through ellipsometry. The low-k SiOCH thin films were prepared by CCP-PECVD method using BTMSM(Bis-trimethylsilylmethane) precursors deposited on p-Si wafer. The Si-O-CHx, Si-O-Si, Si-CHx, CHx and Si-H bonding groups were specified by FTIR spectroscopic spectra, and the groups coupled with the nano-porous structural organic/inorganic hybrid-type of SiOCH thin films which has extremely low dielectric constant close to 2.0. The structural groups includes highly dense pore as well as ions in SiOCH thin films affecting to complex refraction characteristics of single layer on the p-Si wafer. The structural complexity originate the complex refractive constants of the films, and resulted the elliptical polarization of the incident linearly polarized light source of Xe-light source in the range from 190 nm to 2100 nm. Phase difference and amplitude ratio between s wave and p wave propagating through SiOCH thin film was studied. After annealing, the amplitude of p wave was reduced more than s wave, and phase difference between p and s wave was also reduced.

A Fundamental Study on Polymer/Metal Additive Method using a UV Laser for Consumer-oriented 3D Helmet Products (소비자 지향 3차원 헬멧제품 제작을 위한 UV레이저 기반의 폴리머/금속적층에 대한 기초연구)

  • Kang, Bo-Seok;Ahn, Dong-Gyu;Shin, Bo-Sung;Shin, Jong-Kuk
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.15 no.6
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    • pp.89-94
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    • 2016
  • Consumer orientation requires that companies understand consumer needs and produce products that meet their expectations. This study proposes a new additive method that creates a polymer/metal bonding layer and thus can lighten the weight of helmets to develop a consumer-oriented 3D printing helmet. The composite solution is experimentally prepared with copper formate and a photopolymer resin. Stereolithography apparatus and photothermal reactions are introduced to fabricate an adhesive hybrid layer of copper metal and polymer. A UV pulse laser with a 355 nm wavelength was installed to simplify this process. Resistance, adhesion, and accuracy were investigated to evaluate the properties of the layer produced.

Experimental Method for Evaluating Debonding Strength of FRPs Used for Retrofitting Concrete Structures (콘크리트 휨부재 보강용 FRP의 부착성능 평가를 위한 실험방법 연구)

  • Utui, Nadia;Kim, Hee-Sun
    • Journal of the Korean Society for Advanced Composite Structures
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    • v.2 no.3
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    • pp.36-41
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    • 2011
  • This study proposes a experimental method to evaluate bonding strength of FRPs used for retrofitting concrete structures. Specimens are designed so that debonding failure of FRPs can be induced from reinforced concrete beams retrofitted with two layers of carbon and glass FRPs. And three-point loading tests are performed to see if debonding failure with proper debonding strength is observed from the specimens. The test results show that the tested beams are failed due to debonding of FRPs, therefore, the proposed test method is capable of evaluating debonding strength of FRPs using relatively small normal strength concrete beams.