• 제목/요약/키워드: Hot-pressing

검색결과 585건 처리시간 0.026초

Effect of Silicon Nitride Whisker Content on the Flexural Strength of Silicon Nitride-Boron Nitride-Silicon Carbide Multi-Layer Composites

  • Park, Dong-Soo;Cho, Byung-Wook
    • 한국세라믹학회지
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    • 제40권9호
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    • pp.832-836
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    • 2003
  • Multi-layer ceramic composites were prepared by tape casting followed by hot pressing using silicon nitride layer with silicon nitride whiskers, silicon nitride layer with silicon carbide particles and boron nitride-alumina layer. The whiskers were aligned during the casting. As the whisker content of the silicon nitride layer was increased up to 10 wt%, the flexural strength of the multi-layer composite was increased. However, further increase of the whisker content in the layer resulted in a rapid decrease of the strength of the composite. The results suggest that the strength of multi-layer ceramic composite showing non-catastrophic failure behavior can be significantly improved by incorporating the aligned whiskers in the layers.

SiC 휘스커 및 TiC 입자 강화 알루미나 복합재료의 기계적 성질과 미세조직 (Mechanical Properties and Microstructures of Alumina Composites Reinforced with SiC Whiskers and TiC Particles)

  • 이영규;김준규;조원승;최상욱
    • 한국세라믹학회지
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    • 제37권8호
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    • pp.792-798
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    • 2000
  • Alumina composites reinforced with SiC whiskers only or combinded with TiC particles were prepared by hot-pressing at 1850$^{\circ}C$ for 1h. The mechanical properties and microstructures of composites were investigated in this study. By of addition either 20 vol% SiC whiskers or 20 vol% TiC particles, the flexural strength fo alumina was increased from 360 MPa to 650 MPa or 730 MPa, respectively, and the KIC was also increased from 3.5 MPa$.$m1/2 to 5.5MPa$.$m1/2 or 4.4MPa$.$m1/2, respectively. In the case of composites with 20 vol% SiC whiskers and 2 vol% TiC particles. The flexural strength and KIC showed relatively high value of 800 MPa and 5.3MPa$.$m1/2, respectively. The improvement of mechanical properties was considered to be due to both the smaller average grain size and the crack deflection.

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Fabrication of SiC Fiber-SiC Matrix Composites by Reaction Sintering

  • Lim, Kwang-Young;Kim, Young-Wook;Park, Ji-Yeon
    • 한국세라믹학회지
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    • 제45권4호
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    • pp.204-207
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    • 2008
  • This paper presents a new process for producing SiC fiber-SiC matrix(SiC/SiC) composites by reaction sintering. The processing strategy for the fabrication of the SiC/SiC composites involves the following: (1) infiltration of the SiC fiber fabric using a slurry consisting of Si and C precursors, (2) stacking the slurry-infiltrated SiC fiber fabric at room temperature, (3) cross-linking the stacked composites, (4) pyrolysis of the stacked composites, and (5) hot-pressing of the pyrolyzed composites. It was possible to obtain dense SiC/SiC composites with relative densities of >96% and a typical flexural strength of ${\sim}400$ MPa.

Percolative Electrical Conductivity of Platy Alumina/Few-layer Graphene Multilayered Composites

  • Choi, Ki-Beom;Kim, Jong-Young;Lee, Sung-Min;Lee, Kyu-Hyoung;Yoon, Dae Ho
    • 한국세라믹학회지
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    • 제54권3호
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    • pp.257-260
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    • 2017
  • In this work, we present a facile one-pot synthesis of a multilayer-structured platy alumina/few-layer graphene nanocomposite by planetary milling and hot pressing. The sintered composites have electrical conductivity exhibiting percolation behavior (threshold ~ 0.75 vol.%), which is much lower than graphene oxide/ceramic composites (> 3.0 vol.%). The conductivity data are well-described by the percolation theory, and the fitted exponent values are estimated to be 1.65 and 0.93 for t and q, respectively. The t and q values show conduction mechanisms intermediate between 2D- and 3D, which originates from quantum tunneling between nearest neighbored graphenes.

투광성 PLZT의 HYSTERESIS와 광투과 효과에 과한 연구 (A study on properties optical transparency effect and Hysteresis of transparent PLZT)

  • 이호걸;김상연;송준태
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1993년도 하계학술대회 논문집 A
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    • pp.21-23
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    • 1993
  • In this study PLZT was selected which has the excellent quadratic electro-optic property and slim-loop. It was fabricated by the methods of vacuum hot-pressing and sintering. The electrode of color filter was evaporated using the interdigital type masks. Through XRD have we investigated the molecular structure composition formular. Hysteresis and transmission characteristics were measured, The transmission of RGB was envestigated. We are going to study the correlation of coercive field and the nontransmited field.

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Sintering of $Si_3N_4$ Powder Prepared by Self-Propagating High-Temperature Synthesis (SHS)

  • Bai, Ling;Zhao, Xing-Yu;Ge, Chang-Chun
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.268-269
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    • 2006
  • Preparation processing of sintered silicon nitride ceramics was emphatically investigated with Self-Propagating High-Temperature Synthesis (SHS) of silicon nitride prepared by ourselves as raw material. The results indicate that good sinter ability can be obtained with cheaply SHS of silicon nitride preparing silicon nitride materials. The cost of silicon nitride materials will be lowered.

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Factors Affecting Longitudinal Tensile Strength of SiC/Ti-Al-V Composites Manufactured by Plasma Spraying

  • Baik, Kyeong-Ho
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.514-515
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    • 2006
  • In this study, multi-ply SiC fiber reinforced Ti-6Al-4V composites have been manufactured by plasma spraying and subsequent vacuum hot pressing. Two different sizes of Ti-6Al-4V feedstock powders were used for plasma spraying to form matrix. A considerable amount of oxygen was incorporated into as-sprayed Ti matrix during plasma spraying, and consequently caused matrix embrittlement. The use of coarse-sized feedstock powder reduced oxygen contamination, but tended to increase fiber spacing irregularity and fiber strength degradation. Longitudinal tensile strength and ductility of the composites were mainly affected by the matrix oxygen content.

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산화처리된 구형 Fe 분말 성형제의 방전플라즈마 소결거동에 관한 연구 (Densification Behavior of the Oxidation-treated Spherical Fe-powder Compact during Spark-Plasma Sintering Process)

  • 권영순;김윤호;김지순;석명진;문진수;김환태
    • 한국분말재료학회지
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    • 제8권1호
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    • pp.61-69
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    • 2001
  • Spark-Plasma Sintering(SPS) is one of the new sintering methods which takes advantages both inconventional pressure sintering and electric current sintering. It is known that SPS is very effective for the densification of hard-to-sinter materials like refractory metals, intermetallic compounds, glass and ceramics without grain growth. However, a clear explanation for sintering mechanism and an experimental evidence for the formation of weak plasma during SPS are not given yet. In this study, fundamental study on sintering behavior and mechanism of SPS was investiged. For this study, various spherical Fe powders were prepared such as as-received, as-reduced, and as-oxidized and then sintered by SPS facility. In order to confirm the surface cleaning effect during SPS neck region and fracture surface of sintered body was observed and analyzed by SEM/EPMA. Densification behavior was analyzed from the data of deflection along the pressure axis. Some specimens were additionally produced by Hot Pressing and the results were compared with those of SPS.

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투광성 PLZT의 HYSTERESIS와 광투과 효과에 관한 연구 (A study on properties optical transparency effect and Hysteresis of transparent PLZT)

  • 이호걸;김상연;송준태
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1993년도 하계학술대회 논문집 B
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    • pp.555-557
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    • 1993
  • In this study PLZT was selected which has the excel lent quadratic electro-optic property and slim-loop. It was fabricated by the methods of vacuum hot-pressing and sintering. The electrode of color filter was evaporated using the interdigital type masks. Through XRD have we investigated the molecular structure composition formular. Hysteresis and transmission characteristics were measured. The transmission of RGB was envestigated. We are going to study the correlation of coercive field and the nontransmited field.

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알루미나 단섬유 및 유리섬유 보강 청동기지 복합재의 마모특성 연구 (Tribological Properties of the Aluminum Short fiber and glass fiber Reinforced Tin-Bronze Matrix Composites)

  • 황순홍;안병길;이범주;최웅수;허무영
    • 한국윤활학회:학술대회논문집
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    • 한국윤활학회 1996년도 제24회 춘계학술대회
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    • pp.13-19
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    • 1996
  • The tribological properties of the aluminum short fiber and glass fiber reinforced tin-bronze matrix composites manufactured by vacuum hot pressing was studied. The effect of the composition and the relative density on the wear properties was examined by a reciprocal type tribo-test machine. The results were discussed by the observation of the microstructure of sintered specimen and worn surface observation using SEM and EDS. Addition of the fibers led to the wear resistance since the metal matrix was reinforced by the fibers. The reinforcement of the fiber seemed to be stronger as the distribution of the fibers was more uniform. Graphite also reduce the wear loss. The pores in the sintered composites seemed to play an important role to improve the wear resistance since the pores provide the places where the solid lubricants locate.

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