• Title/Summary/Keyword: Hot-injection

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Hyperthermia Properties of Fe3O4 Nanoparticle Synthesized by Hot-injection Polyol Process (Hot-injection Polyol 공정에 의해 제조된 Fe3O4 나노입자의 Hyperthermia 특성)

  • Lee, Seong Noh;Kouh, Taejoon;Shim, In-Bo;Shim, Hyun Ju
    • Journal of the Korean Magnetics Society
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    • v.24 no.2
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    • pp.51-55
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    • 2014
  • The $Fe_3O_4$ nanoparticle was synthesized by the hot-injection method while varying the injection time of the precursor solution. The crystal structure was determined to be cubic inverse spinel with space group of Fd-3m based on X-ray diffraction (XRD) measurements and the morphology of the prepared $Fe_3O_4$ nanoparticle was studied with a high-resolution transmission electron microscope (HR-TEM). When the precursor solution was injected for 0.5 min, the size of the $Fe_3O_4$ nanoparticle was 7.63 nm, while the size of the obtained particle was 21.27 nm with the injection time of 60 min. The magnetic properties of the prepared $Fe_3O_4$ nanoparticle were investigated by both vibrating sample magnetometer (VSM) and $^{57}Co$ M$\ddot{o}$ssbauer spectroscopy at various temperatures. From the hyperthermia measurement, we observed that the temperature of the $Fe_3O_4$ nanoparticle powder reached around $120^{\circ}C$ under 250 Oe at 50 kHz, when the injection time of the precursor solution was 60 min.

Thermal Decomposition Synthesis of CoSb3 Nanoparticle by Hot Injection Method (열분해와 Hot Injection법을 이용한 CoSb3 나노분말합성)

  • Kim, Min-Suk;Ahn, Jong-Pil;Kim, Kyung-Ja;Park, Joo-Seok;Kim, Kyoung-Hun;Kim, Hyung-Sun
    • Journal of the Korean Ceramic Society
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    • v.50 no.6
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    • pp.476-479
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    • 2013
  • $CoSb_3$ with its high electrical conductivity, Seebeck coefficient and rather low thermal conductivity is quite a promising material for thermoelectric conversion applications. A potentially high figure of merit (ZT) can be achieved by a nanostructure evolution of thermoelectric materials. In this work, $CoSb_3$ nanoparticles were synthesized through a thermal decomposition method in cooperation with a hot injection technique. Nano-sized $CoSb_3$ particles were obtained through the thermal decomposition reaction between the pre-heated cobalt-oleate at $320^{\circ}C$ and the injected antimony oleate with room temperature. The results showed that the particle size was increased with increasing synthesis temperature and the crystallinity of particles was improved with temperature but the decomposition of $CoSb_3$ was observed at $320^{\circ}C$. The $CoSb_3$ particles synthesized at $300^{\circ}C$ showed a high purity and an homogeneous shape with average particle size of 26 nm.

THERMO-FLUID ANALYSIS ON THE HELIUM INJECTION COOLING OF GLASS FIBER FOR HIGH SPEED OPTICAL FIBER MANUFACTURING (광섬유 고속생산용 헬륨 주입식 유리섬유 냉각공정에 대한 열유동 해석)

  • Oh, I.S.;Kim, D.;Kwak, H.S.;Kim, K.
    • 한국전산유체공학회:학술대회논문집
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    • 2011.05a
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    • pp.92-95
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    • 2011
  • In manufacturing optical fibers, the process starts with the glass fiber drawing from the heated and softened silica preform in the furnace, and the freshly drawn glass fiber is still at high temperature when it leaves the glass fiber drawing furnace. It is necessary to cool down the glass fiber to the ambient temperature before it then enters the fiber coating applicator, since the hot glass fiber is known to cause several technical difficulties in achieving high quality fiber coating. As the fiber drawing speed keeps increasing, a current manufacturing of optical fibers requires a dedicated cooling unit with helium gas injection. A series of three-dimensional flow and heat transfer computations are carried out to investigate the effectiveness of fiber cooling in the fiber cooling unit. The glass fiber cooling unit is simplified into the long cylindrical enclosure at which the hot glass fiber passes through at high speed, and the helium is being supplied through several injection slots of rectangular shape along the cooling unit. This study presents and discusses the effects of helium injection rates on the glass fiber cooling rates.

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Study for a Secondary Air Affecting Fluid Flow in a Solid Waste Incinerator (쓰레기 소각로의 2차공기가 유동현상에 미치는 현상 연구)

  • Lee, Geum-Bae
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.20 no.9
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    • pp.2924-2932
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    • 1996
  • As the environmental pollution can be greatly reduced and the waste heat can be also recovered through a combustion of municipal solid waste, the incineration begins to be highlighted recently in our country. But it is very difficult to be operated with constant combustion conditions for a long time as the domestic waste is composed of various components, contains a large percentage of water, and has a low heating value. Therefore, the cold flow test and partial hot flow test were conducted in the incinerator by use of injection angles of a secondary air affecting fluid flow as the first action to maintain the optimum combustion conditions. A model to a scale of 1:10 was designed and manufactured through the similarity of model and prototype flows. Velocities and temperatures were measured through the experiment. From the results, fluid flows of secondary air obtained from partial hot flow test correspond almost well with those of main flow obtained from cold flow test. Consequently, injection angles of secondary air are proved to affect main flow decisively.

A Study on the Filling Imbalances between Multi-Cavity in Hot-Runner Mold (핫러너 금형에서 다수 캐비티 사이에 발생하는 충전불균형에 관한 연구)

  • Han Seong Ryeol;Kang Chul Min;Han Kyu Taek;Jeong Yeong Deug
    • Journal of the Korean Society for Precision Engineering
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    • v.22 no.9 s.174
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    • pp.173-178
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    • 2005
  • Recently plastic parts are molded for the purpose of mass production in multi-cavity system. Therefore, designer is usually designing mold that has geometrically balanced runner lay-out for filling balance at each cavity. Although, mold is manufactured with geometrically balanced runner lay-out, there are actually filling imbalances in the cavities. These filling imbalances phenomenon are caused by complicated interaction between melt and mold. In this study, based on previous studies for filling imbalances in cold-runner mold, filling imbalances in hot-runner mold were investigated by CAE and injection molding experiments. ABS and PMMA as amorphous polymer, PA as crystalline polymer were used to compare the filling imbalances. There were different results of CAE and experiment. The filling imbalances decreased as injection rate increased without regard to kind of resins and were lower than the one of cold-runner.

A Study on the Filling Imbalances between Multi-Cavity in Hot-Runner Mold (핫러너 금형에서 캐비티사이의 충전불균형 현상에 관한 연구)

  • Han S.R.;Jeong Y.D.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.06a
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    • pp.598-601
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    • 2005
  • Plastic parts are molded for the purpose of mass production in multi-cavity system. Therefore, designer is usually designing molds that has geometrically balanced runner lay-out for filling balance at each cavities. Although, mold is manufactured with geometrically balanced runner lay-out, there are actually filling imbalances in cavities. These filling imbalances phenomenon are caused by complicated interaction between melt and mold. In this study, based on previous studies for filling imbalances in cold-runner mold, filling imbalances in hot-runner mold were investigated by CAE and injection molding experiments. ABS, PMMA as amorphous polymer and PA, PP as crystalline polymer were used to compare the filling imbalances. The filling imbalances decreased as injection rate increased without regard to kind of resins and were lower than the one of cold-runner.

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Degradation Characteristics by Hot Carrier Injection of nchannel MOSFET with Gate- $n^{-}$S/D Overlapped Structure (게이트와 $n^{-}$소스/드레인 중첩구조를 갖는 n 채널 MOSFET의 핫캐리어 주입에의한 소화특성)

  • 이대우;이우일
    • Journal of the Korean Institute of Telematics and Electronics A
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    • v.30A no.2
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    • pp.36-45
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    • 1993
  • The n-channel MOSFETs with gate-$n^{-}$S/D overlapped structure have been fabricated by ITLDD(inverse-T gate lightly doped drain) technology. The gate length(L$_{mask}$) was 0.8$\mu$m. The degradation effects of hot carriers injected into the gate oxide were analyzed in terms of threshold voltage, transconductance and drain current variations. The degradation dependences on the gate voltage and drain voltage were characterized. The devices with higher n-concentration showed higher resistivity against the hot carrier injection. As the results of investigating the lifetime of the device, the lifetime showed longer than 10 years at V$_{d}$ = 5V for the overlapped devices with the implantation of an phosphorus dose of 5$\times$10$^{13}$ cm$^{-2}$ and an energy of 80 keV in the n$^{-}$resion.

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디젤오염토양복원을 위한 고온공기 주입/추출 공정의 토양 파일 공법에의 적용 연구

  • 박민호;박기호;홍승모;고석오
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2004.09a
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    • pp.63-67
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    • 2004
  • A field pilot study on remediation of diesel-contaminated soil by hot air injection/extraction process constructing soil piling system was conducted to evaluate the effects of hot air on the removal of diesel and each constituent. After the heating process of 2 months, the equilibrium temperature of soil reached to 10$0^{\circ}C$ and soil TPH concentration was reduced to about 72% against the initial concentration. Additional extraction process of 2 months induced the continuous extraction of residual diesel and the increment of microbial activity, which made soil TPH concentration reduced to 95%. In addition biological removal of non volatile constituents in diesel was verified indirectly and the removal pattern of each DRO(diesel range organic) as soil temperature was explained.

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Back bias effects in the programming using two-step pulse injection (2 단계 펄스 주입을 이용한 프로그램 방법에서 백바이어스 효과)

  • An, Ho-Myoung;Zhang, Yong-Jie;Kim, Hee-Dong;Seo, Yu-Jeong;Kim, Tae- Geun
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.258-258
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    • 2010
  • In this work, back bias effects in the program of the silicon-oxide-nitride-oxide-silicon (SONOS) cell using two-step pulse sequence, are investigated. Two-step pulse sequence is composed of the forward biases for collecting the electrons at the substrate terminal and back bias for injecting the hot electrons into the nitride layer. With an aid of the back bias for electron injection, we obtain a program time as short as 600 ns and an ultra low-voltage operation with a substrate voltage of -3 V.

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Surface Heating Method Using Hot Jet Impingement for Improving Transcription of Nano-Pattern (나노 패턴의 전사성 향상을 위한 고온 기체 분사를 이용한 금형 표면의 가열 기법)

  • Kim, K.H.;Yoo, Y.E.;Je, T.J.;Choi, D.S.;Kim, S.K.
    • Transactions of Materials Processing
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    • v.16 no.1 s.91
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    • pp.9-14
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    • 2007
  • In this paper, a mold temperature control method for injection molding is proposed. The inner surface of mold is locally heated by jet impingement to improve pattern transcription. Heating by hot jet is completed while the mold is open. An experimental system that realizes the proposed idea has been built, which includes mold, nozzle assembly and heater. Actual injection molding process including the proposed heating procedure has been conducted to verify the validity of the method. The process has been done for several conditions with different jet temperatures and duration of heating. The results from different conditions are compared.