• 제목/요약/키워드: Hot pressing

검색결과 581건 처리시간 0.032초

Hot Pressing of the Silicon Nitride Based Ceramics and Their Mechanical Behavior

  • Park, D.S.;Lee, S.Y.;Kim, H.D.;Park, W.S.;D.S. Lim;B.D. Han
    • The Korean Journal of Ceramics
    • /
    • 제1권1호
    • /
    • pp.45-54
    • /
    • 1995
  • Four kinds of silicon nitride based ceramic materials have been hot pressed. Effect of the sintering additives on the phase transformation, microstructural development and mechanical properties was investigated. While sintering under the same condition a big difference among the microstructures of the specimens, they appeared alike if sintered to have a similiar $\alpha$-$\beta$ phase ratio. The specimen of the stoichiometric $\alpha$-$\beta$ sialon composition showed very limited amount of the intergranular glassy phase and a significant degree of the residual stress. It exhibited almost no strength degradation up to $1300^{\circ}C$, and the strength of the specimen degraded more as its composition deviated from the stoichiometry.

  • PDF

고온진공가압 티타늄 금속기 복합재료의 미시-기계적 특성에 관한 연구 (A Study on the Micro-mechanical Characteristics of Vacuum Hot Pressed Titanium Metal Matrix Composites)

  • 하태준;김태원
    • 한국복합재료학회:학술대회논문집
    • /
    • 한국복합재료학회 2003년도 추계학술발표대회 논문집
    • /
    • pp.207-210
    • /
    • 2003
  • Vacuum hot pressing has been used for the development of Ti-MMCs using foil-fiber-foil method, and subsequent micro-mechanical characteristics of the composites are evaluated by means of several experimental processes. As shown by the results, fiber strength degradation occurs during the consolidation, and particularly residual stresses results from the thermal expansion mismatch between fiber and matrix materials during cooling process are incorporated in the changes of mechanical properties of the composites. In industrial applications, the processing conditions avoiding micro-material failures are important together with the properties of finished products, and therefore should be included in the assesment of the material characterization.

  • PDF

Thermal conductivity of PLA-bamboo fiber composites

  • Takagi, Hitoshi;Kako, Shuhei;Kusano, Koji;Ousaka, Akiharu
    • Advanced Composite Materials
    • /
    • 제16권4호
    • /
    • pp.377-384
    • /
    • 2007
  • 'Green' composites were fabricated from poly lactic acid (PLA) and bamboo fibers by using a conventional hot pressing method. The insulating properties of the PLA-bamboo fiber 'green' composites were evaluated by determination of the thermal conductivity, which was measured using a hot-wire method. The thermal conductivity values were compared with theoretical estimations. It was demonstrated that thermal conductivity of PLA-bamboo fiber 'green' composites is smaller than that of conventional composites, such as glass fiber reinforced plastics (GFRPs) and carbon fiber reinforced plastics (CFRPs). The thermal conductivity of PLA-bamboo fiber 'green' composites was significantly influenced by their density, and was in fair agreement with theoretical predictions based on Russell's model. The PLA-bamboo fiber composites have low thermal conductivity comparable with that of woods.

TiNi/Al 6061 형상기억복합재료의 기계적특성에 관한 실험 및 해석적 평가 (The Evaluation of Mechanical Properties of TiNi/Al 6061 Shape Memory Composites by Using Experimental and Finite Element Analysis)

  • 박동성;박영철;이동화;이규창
    • 한국정밀공학회:학술대회논문집
    • /
    • 한국정밀공학회 2001년도 춘계학술대회 논문집
    • /
    • pp.687-691
    • /
    • 2001
  • Al alloy matrix composite with TiNi shape memory fiber as reinforcement has been fabricated by hot pressing to investigate mechanical properties. The stress-strain behavior of the composites was evaluated at temperatures between 363K and room temperature as a function of pre-strain by using experimental and finite element analysis, and both cases showed that the tensile stress at 363K was higher than that of the room temperature. Especially, the tensile stress of this composite increases with increasing the amount of pre-strain, and it also depends on the volume fraction of fiber and heat treatment. The smartness of the composite is given due to the shape memory effect of the TiNi fiber which generates compressive residual stress in the matrix material when heated after being pre-strained.

  • PDF

$Si_3{N_4}$휘스커 첨가량에 따른 코디에라이트 glass-ceramics 복합체의 미세구조 (A study on the microstructure of cordierite glass-ceramics composites containing $Si_3{N_4}$ whisker)

  • 한병성;최효상
    • E2M - 전기 전자와 첨단 소재
    • /
    • 제7권1호
    • /
    • pp.1-6
    • /
    • 1994
  • Cordierite based glass ceramics has become an electronic substrate material for electronic circuits and the use of whickers for improving strength and toughness is evident. Pure cordierite containing 15 vol.% silicon nitride were sintered by hot-prossing and it has above 99% density. Especially, it is assumed that toughening increasing at the more high sintering temperature relevants to the glass phase increasing, as showned in the roughness of the fracture surfaces. It was directionally dependent of whisker drirection during processing.

  • PDF

유리상 첨가한 안경렌즈 절삭용 재료 (Materials for Spectacle lens cutting with Glass phase)

  • 이영일
    • 한국안광학회지
    • /
    • 제6권1호
    • /
    • pp.145-148
    • /
    • 2001
  • 안경렌즈 절삭용 재료의 파괴인성과 경도를 향상시키기 위하여 glass상을 함유한 탄화규소계 복합재료를 개발하여 그 기계적 물성과 특성을 연구하고자 하였다. glass상을 갖는 탄화규소를 $1810^{\circ}C$에서 2시간, 25 MPa의 조건에서 일축 가압소결 공정으로 안경렌즈 절삭용 시편을 제조하였다. 파괴인성과 경도를 측정하여 전에 실험한 결과의 기계적 특성과 비교하였다. 본 연구에서 연구된 안경렌즈 절삭용 시편의 대표적인 경도와 파괴인성은 각각 12 GPa과 $5.1MPa{\cdot}m^{1/2}$ 이었다.

  • PDF

잔류 자성원소 검출에 의한 금속간화합물의 기계적 합금화 공정에서의 합금화 정도 해석 (Determination of the Degree of Alloying by Detection of Residual Ferromagnetic Elements for Intermetallic Alloys Processed by Mechanical Alloying)

  • 어순철
    • 한국재료학회지
    • /
    • 제13권9호
    • /
    • pp.561-566
    • /
    • 2003
  • Mechanical alloying(MA) process using elemental powders followed by hot pressing has been applied to some intermetallic alloy system containing ferromagnetic elements, such as NiAl and $FeSi_2$. A modified thermogravimetric analysis (TGA) technique was used to investigate the degree of alloying in milled powders and hot consolidated specimens as well as heat-treated bulk specimens. It is shown that the measurement of Curie temperatures in MA intermetallic powders and consolidated specimens containing ferromagnetic components, when determined as a function of milling and heat treatment parameters, can give some insight into the progress and mechanism of alloying.

Spark Plasma Sintering and Hot Pressing Sintering of Nanocrystalline WC-$10C_o$-0.8VC

  • Zhu, Li Hui;Shao, Guang Jie;Liu, Yi Xiong;Siddle, Dave
    • 한국분말야금학회:학술대회논문집
    • /
    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
    • /
    • pp.894-895
    • /
    • 2006
  • WC-$10C_o$-0.8VC nanocrystalline powders were sintered by spark plasma sintering (SPS) and hot press sintering (HPS), and the microstructure and properties were compared. Results show that dense WC-$10C_o$-0.8VC can be obtained by SPS in several minutes when the sintering temperature is $>1200^{\circ}C$. Sintered at a temperature of $1300^{\circ}C$ the sample prepared by SPS for 3 minutes has higher density, finer grains and better properties than that prepared by HPS for 60 minutes. SPS can be used to prepare nanocrystalline WC-$10C_o$-0.8VC with improved properties when suitable sintering parametesr are chosen.

  • PDF

완도납석으로부터 제조된$\beta$-Sialon의 기계적 성질 (Mechanical Properties of $\beta$-Sialon Prepared from Wando Pyrophyllite)

  • 이홍림;장병국
    • 한국세라믹학회지
    • /
    • 제23권4호
    • /
    • pp.17-22
    • /
    • 1986
  • $\beta$-Sialon powders were prepared by the reduction-nitridation reaction from the mixture of Wando-pyrophyllite and graphite at 135$0^{\circ}C$ in $N_2-H_2$ atmosphere. The $\beta$-Sialon powders were sintered at 175$0^{\circ}C$ by the pressureless sintering for 90min and the hot-pressing for 60 min respectively. All the sintered bodies showed their relative densities higher than 94% The values of M.O.R fracture toughness(KIC) and hardness showed 32.9kpsi 2.9MN/$m^{1.5}$ , 12.1GN/$m^2$ for the pressure-less sitnered bodies and 48.6kpsi, 4.6 MN/4m^{1.5}$ 15.3GN/$m^2$ for the hot-pressed bodies respectively.

  • PDF

급냉응고된 Ribbon을 이용한 CuAINi 형상기억합금의 결정미세화 (Grain Size Refinement in CuAlNi Shape Memory Alloy using Melt-spun Ribbon)

  • 최영택
    • 연구논문집
    • /
    • 통권22호
    • /
    • pp.127-139
    • /
    • 1992
  • The mechnial properties such as fracture strength, ductility and fatigue strength of Cu shape memory alloy are lower than those of Ti-Ni SMA, because of their high elastic anisotropy and large grain size. And in order to improve the mechanical property of Cu SMA, some techniques such as casting method by addition of refining element, powder metallurgy and rapid solidification process have been studied on the refinement of the grain size of Cu SMA. This study was carried out to refine the grain size of CuAlNi SMA by applying the melt spinning method. According to this study, the conclusions are as follows; - grain size of the melt-spun ribbon was about $1\mum$ - there was not change in grain size, although increasing of hot pressing temperature -grain size of the hot-extruded specimen was about $30-40\mum$, it is more refiner than that of castings

  • PDF