• 제목/요약/키워드: Hot pressing

검색결과 581건 처리시간 0.025초

Permanent disposal of Cs ions in the form of dense pollucite ceramics having low thermal expansion coefficient

  • Omerasevic, Mia;Lukic, Miodrag;Savic-Bisercic, Marjetka;Savic, Andrija;Matovic, Ljiljana;Bascarevic, Zvezdana;Bucevac, Dusan
    • Nuclear Engineering and Technology
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    • 제52권1호
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    • pp.115-122
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    • 2020
  • A promising method for removal of Cs ions from water and their incorporation into stable crystal structure ready for safe and permanent disposal was described. Cs-exchanged X zeolite was hot-pressed at temperature ranging from 800 to 950 ℃ to fabricate dense pollucite ceramics. It was found that the application of external pressure reduced the pollucite formation temperature. The effect of sintering temperature on density, phase composition and mechanical properties was investigated. The highest density of 92.5 %TD and the highest compressive strength of 79 MPa were measured in pollucite hot-pressed at 950 ℃ for 3 h. Heterogeneity of samples obtained at 950 ℃ was determined using scanning electron microscopy. The pollucite hot-pressed at 950 ℃ had low linear thermal expansion coefficient of ~4.67 × 10-6 K-1 in the temperature range from 100 to 1000 ℃.

PDMS 쿠션을 갖는 Si 몰드에 의한 핫엠보싱 공정에서의 4 인치 웨이퍼 스케일 전사성 향상 (4 Inch Wafer-Scale Replicability Enhancement in Hot Embossing by using PDMS-Cushioned Si Mold)

  • 김흥규;고영배;강정진;허영무
    • 한국정밀공학회지
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    • 제23권8호
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    • pp.178-184
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    • 2006
  • Hot embossing is to fabricate desired pattern on the polymer substrate by pressing the patterned mold against the substrate which is heated above the glass transition temperature, and it is a high throughput fabrication method for bio chip, optical microstructure, etc. due to the simultaneous large area patterning. However, the bad pattern fidelity in large area patterning is one of the obstacles to applying the hot embossing technology for mass production. In the present study, PDMS pad was used as a cushion on the backside of the micro-patterned 4 inch Si mold to improve the pattern fidelity over the 4 inch PMMA sheet by increasing the conformal contact between the Si mold and the PMMA sheet. The pattern replicability improvement over 4 inch wafer scale was evaluated by comparing the replicated pattern height and depth for PDMS-cushioned Si mold against the rigid Si mold without PDMS cushion.

PMN-PZT 세라믹스에 있어서 열에이징 효과 (Effect of Thermal Aging in PMN-PZT Ceramics)

  • 이개명;박창엽
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1995년도 춘계학술대회 논문집
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    • pp.17-21
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    • 1995
  • Tw types of Pb(Mn$\sub$1/3/Nb$\sub$2/3/)O$_3$+PZT Ceramics had been fabricated by hot-pressing method. One had cause grain and the other had fine grain doe to Cr$_2$O$_3$ addition. These specimen were poled by applying the DC electric field in various steps. The effects of thermal aging on their piezoelectric characteristics and temperature stability of the frequency were investigated.

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상압소결과 열간정수압소결 질화규소의 기계적 성질 (Mechanical Properties of Sintered and HIPed Silicon Nitride)

  • 김창삼;하정수;이준근
    • 한국세라믹학회지
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    • 제24권3호
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    • pp.223-226
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    • 1987
  • Among many densification routes for silicon nitride, HIP(hot isostatic pressing) is becomming more popular these days, mainly due to the fact that it can produce highly reliable products with superior mechanical properties. This study involves in sintering of silicon nitride followed by HIP which requires no canning. Various property changes curing sintering and HIP are observed and analyzed in terms of microstructural changes. Porosity decrease and enhanced interlocking of grains by HIP are considered to be the major causes for improved mechanical properties of silicon nitride.

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세라믹 분말 성형체의 크리프 치밀화 및 결정립 성장의 해석 (Analysis for Creep Densification and Grain Growth of Ceramic Powder Compacts)

  • 권영삼;김기태
    • 한국세라믹학회지
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    • 제30권4호
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    • pp.251-258
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    • 1993
  • A constitutive model is proposed to analyze creep densification and grain growth of ceramic powder compacts. The creep strain rates for powder compacts are obtained from constitutive equations proposed by Rahaman et al. and Helle et al. The grain-growth rate is obtained by assuming time, grain size, and strain rate as its internal state variables. the proposed constitutive model is compared with experimental data for alumina compacts obtained by Venkatachari and Raj for sinter forging and by Son et al. for hot pressing.

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내열 Al합금 본드 다이아몬드 휠의 제조 및 연삭성 (The Fabrication and Grindability of Diamond Wheel Bonded with Heat Resistance Aluminum Alloy)

  • 최성국
    • 한국분말재료학회지
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    • 제2권2호
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    • pp.142-148
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    • 1995
  • 2219 aluminum alloy bonded diamond wheels containing intermetallic compounds were fabricated by powder metallurgy method. Nickel and titanium were added in aluminum matrix piece. The hot pressing condition was $600^{\circ}C$ and 20 Mpa in the furnace of the electric resistance type. The mechanical properties and grinding tests were carried out to confirm the wheel performance. Aluminum oxide ceramics were chosen for use in the grinding tests. The test proved that the heat resistance 2219 aluminum bonded diamond wheel containing 15 wt% nickel and 15 wt% titanium respectively showed the best performance.

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$Si_3N_4/SiC$ Nano Composite의 제조 (The Fabrication of $Si_3N_4/SiC$ Nano-Composite)

  • 이수영;이한섭
    • 연구논문집
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    • 통권23호
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    • pp.165-171
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    • 1993
  • $Si_3N_4/Sic$. nano-composites were fabricated by hot-pressing, gas pressure sintering. The composites contained up to 50 wt. % of SiC. The mechanical properties such as strength, toughness, and hardness of the composite are compared each other. The flexural strength of the composites was improved significantly by introducing fine SiC particles into $Si_3N_4$ matrix, while the fracture toughness was not improved. The increase in flexural strength is attributed to the formation of uniformly elongated $\beta -Si_3N_4$ grains as well as the reduction of grain size.

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티타늄 코팅 된 다이아몬드 지립이 다이아몬드 공구의 성능에 미치는 영향 (Effect of Ti Coated Diamond Grit on Performance of Diamond Tool)

  • 임동필;임대순;민언기;임종관
    • 한국윤활학회:학술대회논문집
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    • 한국윤활학회 1997년도 제25회 춘계학술대회
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    • pp.242-246
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    • 1997
  • Diamond grit was coated with Ti by RF Sputtering to investigate the effect of coated diamond particles on performance of diamond impregnated saw. Coated and uncoated powders were separately mixed with 70Co-30W(wt %) powders by conventional milling technique. Hot pressing was carried out to make specimens. The wear test were carried out with these two types of diamond impregnated specimens. It was demonstrated that Ti coating was effective in improving the ability of grit retention and thus enhanced the tribological performance of diamond tool.

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다공성 금속의 성형공정 후 열탄성 계수 (Thermoelastic Properties of Porous Metals After Material Forming Processes)

  • 이종원;김진원
    • 한국복합재료학회:학술대회논문집
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    • 한국복합재료학회 2003년도 추계학술발표대회 논문집
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    • pp.217-220
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    • 2003
  • The effective thermoelastic properties of porous metals are discussed herein after each material forming process such as hot pressing or extrusion. The voids in metal matrix are assumed to be initially spherical in shape and to be distributed randomly. Once the porous material deforms plastically due to each material forming process, the voids change their shape from a sphere to an ellipsoid and align in one direction. Since the voids are compressible in nature, the void volume fraction is assumed to be decreasing during each material forming process.

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