• 한국식품위생안전성학회지
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• 제18권2호
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• pp.43-50
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• 2003

A liquid chromatographic method, using matrix solid-phase dispersion (MSPD) is developed for the extraction of residual furazolidone in chicken eggs. Blank or fortified egg samples (0.5 g) were blended with Octadecylsilyl (Bulk $C_{18}$, 40${\mu}{\textrm}{m}$, 18%. load, endcapped. 2 g) derivatized silica. After homogenization, $C_{18}$/egg and Na$_2$S $O_4$matrix were transferred to a column made of 10 ml glass syringe and filter paper and compressed 4.0∼4.5 ml volume. The column was washed with 8 ml of hexane and dried under $N_2$ gas. Furazolidone was eluted with acetonitrile (8 ml) under gravity. The eluate containing furazolidone was free from interfering compounds when analyzed by HPLC with UV detection (365 nm, photodiode array). Calibration curves were linear (r = 0.99985) and inter- (1.47%) and intra-assay (5.29%) variabilities for the concentration range examined (7.8∼497 ng/g of eggs, 20 ${mu}ell$ injection volume) were indicative of an acceptable methodology for the analysis of furazolidone. Average recovery of furazolidone added to egg was 96.2%. The limit of detection for the proposed method was 1 ng/g for furazolidone. The method using MSPD is proposed as an alternative assay to the classical method which involves the use of large volumes of a harmful solvent and requires a long tedious separation and clean-up processes prior to its determination.

• Structural Engineering and Mechanics
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• 제61권2호
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• pp.209-220
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• 2017

The purpose of this paper is to study the geometrically nonlinear free vibration of functionally graded nano/micro beams (FGNBs) based on the modified couple stress theory. For practical applications, some analytical expressions of nonlinear frequencies for FGNBs on a nonlinear Pasternak foundation are developed. Hamilton's principle is employed to obtain nonlinear governing differential equations in the context of both Euler-Bernoulli and Timoshenko beam theories for a comprehensive investigation. The modified continuum theory contains one material length scale parameter to capture the size effect. The variation of two-constituent material along the thickness is modeled using Reddy's power-law. Also, the Mori-Tanaka method as an accurate homogenization technique is implemented to estimate the effective material properties of the FGNBs. The results are presented for both hinged-hinged and clamped-clamped boundary conditions. The nonlinear partial differential equations are reduced to ordinary differential equations using Galerkin method and then the powerful method of homotopy analysis is utilized to obtain the semi-analytical solutions. Eventually, the presented analytical expressions are used to examine the influences of the length scale parameter, material gradient index, and elastic foundation on the nonlinear free vibration of FGNBs.

• Geomechanics and Engineering
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• 제38권3호
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• pp.261-273
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• 2024

This study presents a groundbreaking analytical approach to find an exact solution for the bearing capacity of strip footings on reinforced slopes, utilizing the two-phase approach and slip line method. The two-phase approach is considered as a generalized homogenization technique. The slip line method is leveraged to derive the stress field as a lower bound solution and the velocity field as an upper bound solution, thereby facilitating the attainment of an exact solution. The key finding points out the variation of the bearing capacity factor N_γ with influencing factors including the backfill soil friction angle, the footing setback distance from the slope crest edge, slope angle, strength, and volumetric fraction of inclusion layers. The results are evaluated by comparing them with those of relevant studies in the literature considering analytical and experimental studies. Through the application of the two-phase approach, it becomes feasible to determine the tensile loads mobilized along the inclusion layers associated with the failure zone. It is attempted to demonstrate the results by utilizing non-dimensional graphs to clearly illustrate variable impacts on reinforced soil stability. This research contributes significantly to advancing geotechnical engineering practices, specifically in the realm of static design considerations for reinforced soil structures.

• Transactions on Electrical and Electronic Materials
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• 제9권5호
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• pp.209-212
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• 2008

We developed a simple and effective purification method to obtain high-purity single-walled carbon nanotubes (SWCNTs) with low surface damage. The purification process consists of oxidization at $430^{\circ}C$ for 1 h in a furnace system of air atmosphere and homogenization in dilute hydrochloric acid solution for extremely short time. The role of homogenizer was examined during purification process in terms of purity and quality of purified SWCNTs. High-purity and low surface damage of SWCNT products was obtained using homogenizer which was operated at 8500 rpm for 10 min in the environment of 7 % HCI solution. From XRD spectra, we observed that metal catalysts were thoroughly removed. Raman spectra showed that the intensity values of crystallization ($I_{G}/I_{D}$) of purified SWCNTs were very similar with that of pristine SWCNTs. Moreover, the structure damage of purified SWCNTs was hard to find from electron microscopy. Consequently, homogenizing, which is a quick and simple manner, can be promising method for obtaining final SWCNTs with clearly high purity and crystallinity.

• Structural Engineering and Mechanics
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• 제24권4호
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• pp.447-461
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• 2006

Here, the axisymmetric free flexural vibrations and thermal stability behaviors of functionally graded spherical caps are investigated employing a three-noded axisymmetric curved shell element based on field consistency approach. The formulation is based on first-order shear deformation theory and it includes the in-plane and rotary inertia effects. The material properties are graded in the thickness direction according to the power-law distribution in terms of volume fractions of the constituents of the material. The effective material properties are evaluated using homogenization method. A detailed numerical study is carried out to bring out the effects of shell geometries, power law index of functionally graded material and base radius-to-thickness on the vibrations and buckling characteristics of spherical shells.

• Advances in aircraft and spacecraft science
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• 제5권6호
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• pp.691-729
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• 2018

In this paper the hygro-thermo-mechanical vibration and buckling behavior of embedded FG nano-plates are investigated. The Eringen's and Gurtin-Murdoch theories are applied to study the small scale and surface effects on frequencies and critical buckling loads. The effective material properties are modeled using Mori-Tanaka homogenization scheme. On the base of RPT and HSDPT plate theories, the Hamilton's principle is employed to derive governing equations. Using iterative and GDQ methods the governing equations are solved and the influence of different parameters on natural frequencies and critical buckling loads are studied.

• The International Journal of Costume Culture
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• 제4권3호
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• pp.195-202
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• 2001

Re purpose of this study is to indicate the framework to analyze the contemporary fashion phenomena taking on aspect as above by grafting the mass culture theory onto the study for fashion phenomena. The contemporary culture phenomena look like a same thing apparently, but various individual characters appeared in them. And all cultures are mixed in the name of mass culture, but the subordinate concepts which can classify the culture are still in existence. And this equally appear in the contemporary fashion, one of culture phenomena. The concept of the contemporary mass culture can be explained with the taste culture, Cans' theory indicated, divided into highbrow culture, middlebrow culture, and lowbrow culture. And the phenomena of the contemporary mass culture also can be explained with globalization that came down to homogenization, regionalization hybridization.

• 한국정밀공학회지
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• 제22권7호
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• pp.170-176
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• 2005

Analysis of structures which are composed of numerous repeated unit structures can be simplified by using homogenized properties. If the unit structure is repeated in one direction, the whole structure may be regarded as a beam. Once the effective stiffness is obtained from the analysis of the unit structure in a proper way, the effort for the detail modeling of the global structure is not required, and the real structure can be replaced simply with a beam. This study proposes a kinematical periodicity constraint to be imposed on the FE model of the unit structure, which improves the accuracy of the effective stiffness. The method is employed to a one dimensionally arrayed 3D structure containing periodically repeated un-symmetric holes. It is demonstrated that the deformation behavior of the homogenized beam agrees well with that of the real structure.

• 소성∙가공
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• 제16권4호
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• pp.276-281
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• 2007

The hardening and the constitutive equation based on the crystal plasticity are introduced for the numerical simulation of hemispherical sheet metal forming. For calculating the deformation and the stress of the crystal, Taylor's model of the crystalline aggregate is employed. The hardening is evaluated by using the Taylor factor, the critical resolved shear stress of the slip system, and the sum of the crystallographic shears. During the hemispherical forming process, the texture of the sheet metal is evolved by the plastic deformation of the crystal. By calculating the Euler angles of the BCC sheet, the texture evolution of the sheet is traced during the forming process. Deformation texture of the BCC sheet is represented by using the pole figure. The comparison of the strain distribution and punch force in the hemispherical forming process between the prediction using crystal plasticity and experiment shows the verification of the crystal plasticity-based formulation and the accuracy of the hardening and constitutive equation obtained from the crystal plasticity.

• 한국표면공학회지
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• 제31권2호
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• pp.73-80
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• 1998

The aim of this study is to develop sintered stainless steels (SSS) with good mechanical strength, wear resistance, and corrosion resistance by nitrogen ion implantation on the Culated SSS surface. Stainless steel compacts containg Cu (2-10 wt%) were prepared by electroless Cu-pating method which results in the increased3 homogenization in alloying powder. Nitrogen ion implantation was carried out by using N2 gas as the ion source. Nitrogen ions were embedded by an acceleratol of 130keV with doese $3.0\times10^{17}\;ions/\textrm{cm}^2$ on the SSS at $25^{\circ}C$ in$2\times10^{-6}$ torr vacuum. The nitrogen ion implanted SSS obtained from anodic ploarization curves revealed higher corrosion potential than that of nitrogen ion unimplante one. And nitrogen ion implanted 316LSSS had good resistance to pitting corrosion due to the synergistic effect of Mo and N, and the inhibition of $NH_4\;^+$<\TEX>, against $CI^-$<\TEX>.