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Sintering Behavior and Mechanical Property of Mo Nanopowders (Mo 나노분말의 소결거동 및 기계적 특성)

  • Kim, Hai-Gon;Kim, Gil-Su;Oh, Sung-Tag;Suk, Myung-Jin;Kim, Young-Do
    • Journal of Powder Materials
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    • v.14 no.6
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    • pp.386-390
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    • 2007
  • The sintering behavior and mechanical property of Mo nanopowder was investigated as a function of various sintering condition. Mo oxide nanopowders were milled using a high energy ball-milling process. After the ball milling for 20h, the crystalline size of $MoO_3$ was about 20 nm. The $MoO_3$ nanopowders were reduced at the temperature of $800^{\circ}C$ without holding time in $H_2$ atmosphere. The sinterability of Mo nanopowder and commercial Mo powder was investigated by dilatometric analysis. Mo nanopowder and commercial Mo powder were sintered at $1200^{\circ}C$ for 1 hand $1500^{\circ}C$ for 3 h, respectively. In both specimens the measured relative density was about 95%. But the measured hardness values were 2.34 GPa for nanopowder and 1.87 GPa for commercial powder. Probably due to finer grain size of the sintered body prepared from Mo nanopowder than that prepared using commercial Mo powder. The mean grain sizes were measured to be about 1.4 mm and 6.2 mm, respectively.

Microstructure and Electric Contact Properties of Spark Plasma Sintered Ta-Cu Composite (방전플라즈마 소결법으로 제조된 Ta-Cu의 미세조직 및 전기접점 특성)

  • Ju, Won;Kim, Young Do;Sim, Jae Jin;Choi, Sang-Hoon;Hyun, Soong Keun;Lim, Kyoung Mook;Park, Kyoung-Tae
    • Journal of Powder Materials
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    • v.24 no.5
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    • pp.377-383
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    • 2017
  • Microstructure, electric, and thermal properties of the Ta-Cu composite is evaluated for the application in electric contact materials. This material has the potential to be used in a medium for a high current range of current conditions, replacing Ag-MO, W, and WC containing materials. The optimized SPS process conditions are a temperature of $900^{\circ}C$ for a 5 min holding time under a 30 MPa mechanical pressure. Comparative research is carried out for the calculated and actual values of the thermal and electric properties. The range of actual thermal and electric properties of the Ta-Cu composite are 50~300 W/mk and 10~90 %IACS, respectively, according to the compositional change of the 90 to 10 wt% Ta-Cu system. The results related to the electric contact properties, suggest that less than 50 wt% of Ta compositions are possible in applications of electric contact materials.

Characterization of the Microstructure and the Wear Resistance of the Flame-Quenched Cu-8.8Al-4.5Ni-4.5Fe Alloy (화염급냉 표면처리된 Cu-8.8Al-4.5Ni-4.5Fe 합금의 미세구조 분석 및 내마모성에 관한 연구)

  • Lee, M.K.;Hong, S.M.;Kim, G.H.;Kim, K.H.;Kim, W.W.
    • Journal of the Korean Society for Heat Treatment
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    • v.17 no.6
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    • pp.346-355
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    • 2004
  • The flame quenching process has been employed to modify the surfaces of commercial marine propeller material, aluminum bronze alloy (Cu-8.8Al-5Ni-5Fe), and the microstructure, hardness and wear properties of the flame-quenched layers have been studied. The thermal history was accurately monitored during the process with respect to both the designed maximum surface temperature and holding time. The XRD and EDX analyses have shown that at temperatures above $T_{\beta}$, the microstructure consisting of ${\alpha}+{\kappa}$ phases changed into the ${\alpha}+{\beta}^{\prime}$ martensite due to an eutectoid reaction of ${\alpha}+{\kappa}{\rightarrow}{\beta}$ and a martensitic transformation of ${\beta}{\rightarrow}{\beta}^{\prime}$. The ${\beta}^{\prime}$ martensite phase formed showed a face-centered cubic (FCC) crystal structure with the typical twinned structure. The hardness of the flame-quenched layer having the ${\alpha}+{\beta}^{\prime}$ structure was similar to that of the ${\alpha}+{\kappa}$ structure and depended sensitively on the size and distribution of hard ${\kappa}$ and ${\beta}^{\prime}$ phases with depth from the surface. As a result of the sliding wear test, the wear resistance of the flame-quenched layer was markedly enhanced with the formation of the ${\beta}^{\prime}$ martensite.

A Study on the Criteria Appropriateness of Experimental Materials & Facilities in Home Economics Education of Secondary School (중등학교 가정과 실험학습 교구.설비기준의 적정성에 관한 연구)

  • 강혜숙;윤인경
    • Journal of Korean Home Economics Education Association
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    • v.5 no.1
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    • pp.61-85
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    • 1993
  • Because of the specificity of subjects belong to middle school curriculum of Home Economics Education of function training is very important. but it pointed out that the existing standards are out-dated, and because of it , it incongruent to our realities. Therefore, whenever the curriculum o education and the national textbook are reorgrnized periodically, the reform of standards of educational materials & facilities must be followed by it. But in my opinion, in korean middle school, especially in Home Economics Education, educational facilities are not reformed at a proper time. Therefore to enhance the qualities of experimentation/practice of Home Economics Education, in the first place, the preparation for the given conditions of standards of educational materials & facilities are needed. But the educational facilities of Home Economics Education have many problem not only in the qualitative aspect but also in the quantitative aspect. And in addition to it, lost of educational facilities which cannot match contents of national textbook of Home Economics Education are exist. Therefore this thesis aims at examining comprehensively the problem of experimentation /practice of experimental materials & facilities of Home Economics Education connect with contents of Home Economics Education, holding several problems of experimentation/practice of Home Economics Education in middle school, grouping ; the principles and ways concerning the innovation experimental materials & facilities of Home Economics Education by which many teachers and students make sure of more efficient teaching/studying, and obtaining basic data which guarantee the ability of innovation concerning problems of the education of experimentation/practice of Home Economics Education. Method are : 1)grasp our educational realities with my original(question). 2)Integrate/analyse results of 1) 3)check the frequency, percentage with methods of X$^2$-test, T-test, and ‘One-way Analysis of Variances’. 4)suggest my own alternative proposal.

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로켓 모션테이블 실시간 모의시험

  • Sun, Byung-Chan;Park, Yong-Kyu;Choi, Hyung-Don;Cho, Gwang-Rae
    • Aerospace Engineering and Technology
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    • v.3 no.1
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    • pp.170-178
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    • 2004
  • This paper deals with six degree-of-freedom HILS(hardware-in-the-loop-simulation) of KSR-III rocket using a TAFMS(three axis flight motion simulator). This TAFMS HILS test is accomplished before main HILS tests in order to verify the control stability in the presence of TAFMS dynamic effects. The TAFMS HILS test includes initial attitude holding tests for INS initial alignment procedures, timer synchronization tests with an auxiliary lift-off signal, real-time calibration tests using an external thermal recorder, open-loop TAFMS operating tests, and final closed-loop TAFMS HILS tests using the TAFMS attitude measurements as inputs to the closed control loop. The HILS tests are accomplished for several flight conditions composed with nominal flight condition, TWD effect added condition, slosh modes and/or bending modes existing condition, and windy condition, etc.

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Digitally Divided by Choice and the Diffusion of ICTs (정보통신기술의 확산과 선택에 의한 정보격차)

  • Jung, Byung-Kul
    • Journal of Science and Technology Studies
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    • v.6 no.2 s.12
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    • pp.103-129
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    • 2006
  • In spite of decreased attention to digital divide, it has been pointed out as one of the main obstacles to realization of information society. At the outset, two conflicting explanations, optimism and pessimism, have directed their attention to objective basis of digital divide in common. They, however, have been neglected the fact that accessibilities can be varied not only by objective conditions but by subjective conditions such as individual recognition of necessity and willingness. Subsequent choices can be a crucial factor to determine whether to or not to access. In USA, over 50% of potential users determined not to access to the internet by their own will and choices. By the user survey on internet, 'do not feel the necessity' ranked the first reason not to use the internet in South Korea. The respondents who chose 'no time to use' tend to decrease but kept holding their shares, too. The relative importance of 'not to access' by individual choice have been increased. Whether the non-users of ICTs by choice is in or beyond the scope of digital divide, it evidently shows the necessity and importance of directing our attention to it on the way to information society.

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A New Policing Method for Markovian Traffic Descriptors of VBR MPEG Video Sources over ATM Networks (ATM 망에서의 마코프 모델기반 VBR MPEG 비디오 트래픽 기술자에 대한 새로운 Policing 방법)

  • 유상조;홍성훈;김성대
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.25 no.1A
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    • pp.142-155
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    • 2000
  • In this paper, we propose an efficient policing mechanism for Markov model-based traffic descriptors of VBR MPEG video traffic. A VBR video sequence is described by a set of traffic descriptors using a scene-basedMarkov model to the network for the effective resource allocation and accurate QoS prediction. The networkmonitors the input traffic from the source using a proposed new policing method. for policing the steady statetransition probability of scene states, we define two representative monitoring parameters (mean holding andrecurrence time) for each state. For frame level cell rate policing of each scene state, accumulated average cellrates for the frame types are compared with the model parameters. We propose an exponential bounding functionto accommodate dynanic behaviors during the transient period. Our simulation results show that the proposedpolicing mechanism for Markovian traffic descriptors monitors the sophisticated traffic such as MPEG videoeffectively and well protects network resources from the nalicious or misbehaved traffic.

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Effect of Resistance Spot Welding Parameters on AA1100 Aluminum Alloy and SGACD Zinc coated Lap Joint Properties

  • Chantasri, Sakchai;Poonnayom, Pramote;Kaewwichit, Jesada;Roybang, Waraporn;Kimapong, Kittipong
    • International Journal of Advanced Culture Technology
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    • v.3 no.1
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    • pp.153-160
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    • 2015
  • This article is aimed to study the effects of resistance spot welding (RSW) on the lap joint properties between AA1100 aluminum alloy and SGACD zinc coated steel and its properties. The summarized experimental results are as follows. The summarized experimental results are as follows. The optimum welding parameters that produced maximum tensile shear strength of 2200 N was a welding current of 95 kA, a holding time of 10 cycles, and a welding pressure of 0.10 MPa. Increasing of welding current, increased the tensile shear strength of the joint and also increased the amount of aluminum dispersion at the joint interface. The lap joint of steel over the aluminum (Type I) showed the higher joint tensile shear strength than a lap joint of aluminum over the steel (Type II). The indentation depth and the ratio of the indentation depth to the plate thickness decreased when the welding current was increased in the type I lap joint and also decreased when the welding current was decreased in the type II lap joint. The interface structure showed the formation of the brittle $FeAl_3$ intermetallic compound that deteriorated the joint strength.

Synthesis of Sub-Micron 2SnO·(H2O) Powders Using Chemical Reduction Process and Thermal Calcination (화학적 합성법을 이용한 마이크론 이하급 2SnO·(H2O) 분말의 합성과 하소 특성)

  • Chee, Sang-Soo;Lee, Jong-Hyun
    • Korean Journal of Materials Research
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    • v.23 no.11
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    • pp.631-637
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    • 2013
  • Synthesis of sub-micron $2SnO{\cdot}(H_2O)$ powders by chemical reduction process was performed at room temperature as function of viscosity of methanol solution and molecular weight of PVP (polyvinylpyrrolidone). Tin(II) 2-ethylhexanoate and sodium borohydride were used as the tin precursor and the reducing agent, respectively. Simultaneous calcination and sintering processes were additionally performed by heating the $2SnO{\cdot}(H_2O)$ powders. In the synthesis of the $2SnO{\cdot}(H_2O)$ powders, it was possible to control the powder size using different combinations of the methanol solution viscosity and the PVP molecular weight. The molecular weight of PVP particularly influenced the size of the synthesized $2SnO{\cdot}(H_2O)$ powders. A holding time of 1 hr in air at $500^{\circ}C$ sufficiently transformed the $2SnO{\cdot}(H_2O)$ into $SnO_2$ phase; however, most of the PVP (molecular weight: 1,300,000) surface-capped powders decomposed and was removed after heating for 1 h at $700^{\circ}C$. Hence, heating for 1 h at $500^{\circ}C$ made a porous $SnO_2$ film containing residual PVP, whereas dense $SnO_2$ films with no significant amount of PVP formed after heating for 1 h at $700^{\circ}C$.

Effect of Post-clad Heat Treatment on Microstructures and Mechanical Properties of Cu-NiCrBSi Dissimilar Laser Clads (후열처리에 따른 Cu-NiCrBSi 이종 레이저 클래드부의 미세조직 및 기계적 성질 변화)

  • Kim, Kyeong-Min;Jeong, Ye-Seon;Sim, Ahjin;Park, Wonah;Park, Changkyoo;Chun, Eun-Joon
    • Korean Journal of Materials Research
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    • v.30 no.9
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    • pp.465-473
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    • 2020
  • For surface hardening of a continuous casting mold component, a fundamental metallurgical investigation on dissimilar laser clads (Cu-NiCrBSi) is performed. In particular, variation behavior of microstructures and mechanical properties (hardness and wear resistance) of dissimilar clads during long-term service is clarified by performing high-temperature post-clad heat treatment (temperature range: 500 ~ 1,000 ℃ and isothermal holding time: 20 ~ 500 min). The microstructures of clad metals (as-clads) consist of fine dendrite morphologies and severe microsegregations of the alloying elements (Cr and Si); substrate material (Cu) is clearly confirmed. During the post-clad heat treatment, the microsegregations are totally homogenized, and secondary phases (Cr-based borides and carbides) precipitated during the short-term heat treatment are also almost dissolved, especially at the heat treatment conditions of 950 ℃ for 500 min. Owing to these microstructural homogenization behaviors, an opposite tendency of the surface mechanical properties can be confirmed. In other words, the wear resistance (wear rate) improves from 4.1 × 10-2 ㎣/Nm (as-clad condition) to 1.4 × 10-2 ㎣/Nm (heat-treated at 950 ℃ for 500 min), whereas the hardness decreases from 453 HV (as-clad condition) to 142 HV (heat-treated at 950 ℃ for 500 min).