• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2018년도 추계 학술논문 발표대회
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• pp.81-82
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• 2018

The structure of the RC structure is actively reinforcing the structure of the building which has suffered from aging, artificial and natural damage of the building. Among various reinforcement methods, epoxy adhesive is used to attach FRP in FRP reinforcement method which is reinforcing by attaching FRP to the structural part. At this time, the epoxy adhesive having a low critical temperature has a sudden adhesive failure upon exposure to heat, and thus, the development of an inorganic fireproof adhesive having a high critical temperature has progressed. Therefore, in this study, the compositional change of inorganic fire - resistant adhesive exposed to high temperature heat was analyzed by XRD.

• 보존과학회지
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• 제32권4호
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• pp.511-520
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• 2016

본 연구는 고온 XRD 분석법을 적용하여 우즈베키스탄 카라테파 불교사원에서 수습한 점토 재질로 된 벽돌의 소성온도를 추정하는데 목적이 있다. 사원에서 수습한 점토벽돌의 구성광물은 석영, 사장석, 알칼리장석, 운모, 녹니석, 석회석, 각섬석 등이 동정되고, 일부 시료에서 석고가 확인되며, 석고는 벽돌의 점착력을 향상시킬 목적으로 사용된 것으로 판단된다. 소성온도 추정결과, 구운 벽돌인 UZ-1시료에서 석영, 사장석, 휘석계열의 광물이 동정되어 지질온도계를 이용한 소성온도는 $900{\sim}1200^{\circ}C$로 추정된다. 반면 점토벽돌인 UZ-5에 고온 XRD 분석법을 적용해 보면, $1000^{\circ}C$에서 석회석이 소멸하고, $1050^{\circ}C$에서 녹니석의 회절 피크가 약해지는 것으로 보아 소성온도는 $1000{\sim}1050^{\circ}C$인 것으로 추정된다. 또한 휘석계열의 광물은 재현실험에서 $1050^{\circ}C$에서 생성되는 것을 확인하였다. 결과적으로 고온 XRD 분석 결과에 의한 소성온도 추정은 일반적인 광물 동정법에 비해 보다 정확한 추정이 가능하며, 실험 하에서 광물의 소멸 및 생성 온도 영역을 살펴볼 수 있는 분석법임을 확인하였다.

• 한국구조물진단유지관리공학회 논문집
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• 제19권6호
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• pp.63-71
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• 2015

본 연구는 섬유를 혼입한 고강도 콘크리트의 온도 변화에 따른 내화특성 분석에 관한 연구로 고강도 콘크리트에 고온이 가해질 경우 발생되는 폭렬현상에 대하여 방지효과가 있는 것으로 알려져 있는 하이브리드섬유와 강섬유를 함께 혼입하여 만든 복합섬유를 사용하여 온도 변화($100{\sim}800^{\circ}C$)에 따른 고강도 콘크리트의 내화특성 및 역학적 메커니즘을 분석하였다. 또한 본 논문에서는 고강도 콘크리트 구조물에서 가장 문제가 되는 폭렬현상을 막는 대책 중의 하나인 섬유 혼입을 통한 방법을 사용하여 SEM 및 XRD 분석 등의 방법으로 고온을 받은 고강도 콘크리트의 열적 특성 및 역학적 특성을 규명하고자 하였다.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2015년도 추계 학술논문 발표대회
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• pp.24-25
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• 2015

To secure fundamental materials for the performance change in concrete structure damaged by fire, this study analyzed SEM and XRD of hardened cement depending on high temperature conditions. As a result, at more than 200℃, SEM and XRD were not observed because of dehydration of Ettringite; at more than 500℃, calcium hydroxide was rapidly decomposed; at more than 700℃, calcium oxide was found; at 1000℃, the highest peak point appeared.

• Journal of Welding and Joining
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• 제16권3호
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• pp.121-128
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• 1998

The degradation of mechanical properties in the high nitrogen steel HN3 developed for nuclear fusion reactor has been evaluated quantitatively using the small punch(SP) test, X-ray diffraction (XRD) analysis has also been conducted to identify carbides or nitrides precipitated on grain boundaries of the heat treated samples. Mechanical properties of the steel HN3 significantly decreased with increasing heat treatment time and temperature or with decreasing testing temperature. Combination of XRD and metallurgical observation, revealed that the material degradation in the thermally aged steel was caused by precipitation of carbides on the grain boundaries. While the weld metal showed the lowest mechanical properties among various microstructures in GTA weldments. By combining SP test and XRD analysis, cryogenic fracture behaviors and aging degradation for high nitrogen steel could be successfully evaluated in nondestructive manner.

• 한국신뢰성학회지:신뢰성응용연구
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• 제16권1호
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• pp.41-47
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• 2016

Purpose: The purpose of this study was to evaluate electrical and structural degradation of flexible CIGS sollar cell exposed to high temperature and humid atmosphere. Method: Accelerated degradation was performed for various time under $85^{\circ}C/85%RH$ and then electrical and structural properties were analyzed by 4-point probe method, scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), and X-ray diffraction (XRD). Results: Sheet resistance of the top ITO layer increased with exposure time to the high temperature and humid atmosphere. Blunting of the protrusion morphology of ITO layer was observed for the degraded specimen, while no phase change was detected by XRD. Oxygen was detected at the edge area after 300 hours of exposure. Conclusion: Increase in electrical resistance of the degraded CIGS solar cell under high temperature and humid environment was attribute to the oxygen or water absorption.

• 한국재료학회지
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• 제27권11호
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• pp.577-582
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• 2017

Self-cleaning and photocatalytic $TiO_2$ thin films were prepared by a facile sol-gel method followed by spin coating using peroxo titanic acid as a precursor. The as-prepared thin films were heated at low temperature($110^{\circ}C$) and high temperature ($400^{\circ}C$). Thin films were characterized by X-ray diffraction(XRD), Field-emission scanning electron microscopy(FESEM), UV-Visible spectroscopy and water contact angle measurement. XRD analysis confirms the low crystallinity of thin films prepared at low temperature, while crystalline anatase phase was found the for high temperature thin film. The photocatalytic activity of thin films was studied by the photocatalytic degradation of methylene blue dye solution. Self-cleaning and photocatalytic performance of both low and high temperature thin films were compared.

• 한국화재소방학회논문지
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• 제12권4호
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• pp.31-40
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• 1998

고온에 노출된 콘크리트 미세조직의 변화가 강도에 미치는 영향을 규명하기 위하여 현 재 건설현장에서 가장 많이 이용하고 있는 배합비와 쇄석으로 시험체를 제작하여 고온에 노출시킨 후 SEM!EDX, XRD 및 DSC-TG로 분석하여 각 온도별로 강도와 미세조직 특 성을 분석하였다.

• Carbon letters
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• 제5권1호
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• pp.27-33
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• 2004

Structural changes of high modulus carbon fiber by oxidation in carbon dioxide gas using SEM, TEM, and XRD have been observed. It was shown that the originally high modulus carbon fiber is composed of highly ordered graphitic crystalline area and non-crystalline area. It was observed that the La increases during the whole oxidation process. It was shown that the oxidation of high modulus carbon fiber initiates at the non-crystalline area and at the ends of fiber. The large pores developed in fiber by direction of fiber length at high temperature ($1,100^{\circ}C$), and the small pores developed on the fiber surface at low temperature ($900^{\circ}C$). In conclusion, it is found that the oxidation of the carbon fiber was progressed through the imperfection.

• 한국재료학회지
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• 제25권7호
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• pp.347-351
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• 2015

To study the characteristics of ZTO, which is made using a target mixed $ZnO:SnO_2=1:1$, the ZnO and $SnO_2$ were analyzed using PL, XRD patterns, and electrical properties. Resulting characteristics were compared with the electrical characteristics of ZnO, $SnO_2$, and ZTO. The electrical characteristics of ZTO were found to improve with increasing of the annealing temperature due to the high degree of crystal structures at high temperature. The crystal structure of $SnO_2$ was also found to increase with increasing temperatures. So, the structure of ZTO was found to be affected by the annealing temperature and the molecules of $SnO_2$; the optical property of ZTO was similar to that of ZnO. Among the ZTO films, ZTO annealed at the highest temperature showed the highest capacitance and Schottky contact.