• Title/Summary/Keyword: High-speed melt spinning

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Preparation and Physical Properties of Biodegradable High Performance PLA Fiber using Process Parameters (용융방사에 의한 생분해성 고강도 PLA 섬유 제조 공정 상 주요 공정 변수에 관한 연구)

  • Jeung, Woo Chang;Kim, Sam Soo;Lee, Sang Oh;Lee, Jaewoong
    • Textile Coloration and Finishing
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    • v.34 no.3
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    • pp.197-206
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    • 2022
  • The purpose of this study was to confirm the optimal spinning conditions for PLA (Polylactic acid) as a fiber forming polymer. According to the melt spinning test results of PLA, the optimal spinning temperature was 258℃. However, it needs to note that relatively high pack pressure was required for spinning at 258℃. At an elevated temperature, 262℃, mono filament was broken easily due to hydrolysis of PLA at a higher temperature. In case of fiber strength, it was confirmed that the draw ratios of 2.7 to 3.3 were optimal for maximum strength of melt spun PLA. Above the draw ratio, 3.3, the strength of the PLA fibers was lowered. It was presumed that cleavage of the PLA polymer chain over maximum elongation. The heat setting temperature of GR (Godet roller) showed that the maximum strength of the PLA fibers was revealed around 100℃. The degree of crystallinity and the strength of the PLA fibers were decreased above 100℃. The optimal take-up speed (Spinning speed) was around 4,000m/min. Thermal analysis of PLA showed 170℃ and 57℃ as Tm (melting temperature) and Tg (glass transition temperature), respectively.

Effects of Spinning Conditions on Properties of Polyester Yarn Prepared using an Ultra-high-speed Melt Spinning Technique Equipped with a Steam Chamber

  • Ho, Yo-Seung;Kim, Hak-Yong;Jin, Fan-Long;Park, Soo-Jin
    • Bulletin of the Korean Chemical Society
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    • v.31 no.11
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    • pp.3252-3258
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    • 2010
  • In this study, the effects of the various parameters of spinning and drawing processes on the properties of polyester full drawn yarn (FDY) prepared by steam processing during high-speed spinning were investigated using several techniques. The wet shrinkage ratio of the FDY was able to be manipulated by controlling the temperature and draw ratio. The FDY made using the steam high speed spinning technique exhibited identical properties (such as tenacity, elongation, and wet shrinkage ratio) to that of regular FDY, made using the spin-draw process. FDY prepared using the steam process during high-speed spinning showed excellent dyeability. The dye pick-up of the polyester yarn spun at high-speed spinning was found to be improved when dyed under an atmospheric pressure of $100^{\circ}C$. This result was the same as regular FDY dyed under a high pressure of $130^{\circ}C$.

Preparation of Polyethylene Micro-fibers by High Speed Centrifugal Melt Spinning (초고속 용융 원심방사를 이용한 폴리에틸렌 마이크론 섬유의 제조)

  • Yang, Seong Baek;Lee, Jungeon;Ji, Byung Chul;Joo, Nam Sik;Yeum, Jeong Hyun
    • Textile Coloration and Finishing
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    • v.32 no.4
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    • pp.239-244
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    • 2020
  • Polyethylene (PE) micro-fiber have been prepared at different hot air temperature (60, 80 and 100 ℃) and different pressure (20, 40, 60 and 80 kPa) by melt centrifugal spinning technique. The parameters of melting centrifugal spinning including polymer contents, rotational velocity, temperature of hot air and pressure were optimized for the fabrication process. The study showed that 8000 rpm rotational velocity, 80 ℃ heated hot air and 40 kPa air pressure are the best condition to obtain uniform and strong PE fiber. The prepared PE fibers were analyzed by field emission scanning electron microscope and universal testing machine and found that fibers with reduced diameter and improved tensile strength are obtained at hot air condition.

Effects of Spinning Speed and Heat Treatment on the Mechanical Property and Biodegradability of Polylactic Acid Fibers (제사속도와 열처리에 따른 polylactic acid 섬유의 물성 및 생분해성 변화)

  • Park Chung-Hee;Hong Eun-Young
    • Journal of the Korean Society of Clothing and Textiles
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    • v.30 no.4 s.152
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    • pp.607-614
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    • 2006
  • This study was carried out to suggest the optimal spinning process condition which provides a proper range of tenacity and biodegradability as textile fibers. The effects of the melt spinning speed and heat treatment on the mechanical property and biodegradability of polylactic acid fiber were investigated. Polylactic acid(PLA) was spun in a high spinning speed of $2000{\sim}4000m/min$. Each specimen was heat-treated at $100^{\circ}C$ during 30min. Mechanical properties such as breaking stress and the degree of crystallinity were evaluated using WAXS. Biodegradability was estimated from the decrease of breaking stress, weight loss, and the degree of crystallinity after soil burial. Experimental results revealed that heat treated specimens showed higher breaking stress than untreated specimens, but the increase was not so high as was expected from the remarkable change of crystallinity by heat treatment. It was concluded that breaking stress was more influenced by spinning speed than heat treatment. In the soil burial test, however biodegradability calculated from weight loss was more influenced by heat treatment than spinning speed.