• Title/Summary/Keyword: High hardness

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The Effect of Disintegrants on the Properties of Salicylamide Tablets (수종의 붕해제가 살리실아미드정제의 제제특성에 미치는 영향)

  • Hwang, Sung-Joo;Rhee, Gye-Ju;Jee, Ung-Kil;Kwak, Hyo-Sung;Kim, Chong-Kook
    • Journal of Pharmaceutical Investigation
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    • v.22 no.1
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    • pp.41-48
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    • 1992
  • Six common tablet disintegrants (corn starch, Avicel PH102, calcium carboxymethylcellulose, Primojel, Kollidon CL and Ac-Di-Sol) were used at the concentration of 0, 2, 4 and 6% (w/w) in salicylamide tablets made with wet granulation method. Certain physical parameters of the disintegrants (moisture sorption, hydration capacity and bulk density) were determined to evaluate their relative efficiency. The disintegration time and dissolution rate of the tablets were correlated well with the ranks of initial rate of moisture sorption for each disintegrant as follows; Ac-Di-Sol, Kollidon CL, primojel, calcium CMC, corn starch and Avicel PH102. The initial rate of moisture sorption was important for the disintegration capacity as well as hydration capacity. The effect of storage at different temperatures and relative humidity upon the tablets containing various disintegrants was evaluated in terms of tablet hardness and disintegration time. Storage at high temperature reduced the hardness substantially and retarded the disintegration of the all tablets studied. Especially, the hardness of tablets containing Kollidon CL was significantly reduced. Although the tablet hardness was decreased and the disintegration time was increased under a moderate humid condition, both of them were decreased under the severely high humid condition of 80 or 90% RH, which was due to the breakrupture of tablet matrix bonds by the excessive uptake of moisture. Therefore, the stability caused by moisture sorption should be considered, when disintegrants having high moisture sorption such as Kollidon CL, Ac-Di-Sol and Primojel were employed in the tablets containing water-labile or hygroscopic drugs.

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Dynamics of Hexavalent Chromium in Four Types of Aquaculture Ponds and Its Effects on the Morphology and Behavior of Cultured Clarias gariepinus (Burchell 1822)

  • Mustapha, Moshood Keke
    • Toxicological Research
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    • v.33 no.2
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    • pp.119-124
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    • 2017
  • Hexavalent chromium is a bio accumulative toxic metal in water and fish. It enters aquaculture ponds mainly through anthropogenic sources. Hexavalent chromium concentrations and its effects on the morphology and behavior of Clarias gariepinus were investigated from four aquaculture ponds for 12 weeks. Chromium was measured using diphenyl carbohdrazide method; alkalinity and hardness were measured using colometric method and analyzed with Bench Photometer. Temperature and pH were measured using pH/EC/TDS/Temp combined tester. Temporal and spatial replications of samples were done with triplicates morphological and behavioural effects of the metal on fish were observed visually. Chromium ranged from no detection to 0.05 mg/L, alkalinity 105 to 245 mg/L, hardness 80 to 165 mg/L, pH 6.35 to 8.03 and temperature 29.1 to $35.9^{\circ}C$. Trend in the chromium concentrations in the ponds is natural > earthen > concrete > collapsible. There was a significant difference (P < 0.05) in chromium, alkalinity, water hardness, pH and temperature among the four ponds. Significant positive correlation also existed between alkalinity, water hardness, pH, with chromium. Morphological and behavioural changes observed in the fish include irregular swimming, frequent coming to the surface, dark body colouration, mucous secretion on the body, erosion of gill epithelium, fin disintegration, abdominal distension and lethargy. High chromium concentration in natural pond was due to anthropogenic run-off of materials in to the pond. Acidic pH, low alkalinity, low water hardness also contributed to the high chromium concentration. Morphological and behavioural changes observed were attributed to the high concentrations, toxicity and bio accumulative effect of the metal. Toxicity of chromium to fish in aquaculture could threaten food security. Watershed best management practices and remediation could be adopted to reduce the effects of toxicity of chromium on pond water quality, fish flesh quality and fish welfare.

Hardness and EDM Processing of MoSi$_2$Intermetallics for High Temperature Ship Engine (고온선박엔진용 MoSi$_2$금속간화합물의 경도와 방전가공특성)

  • 윤한기;이상필
    • Journal of Ocean Engineering and Technology
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    • v.16 no.6
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    • pp.60-64
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    • 2002
  • This paper describes the machining characteristics of the MoSi$_2$--based composites through the process of electric discharge drilling with various tubular electrodes. In addition to hardness characteristics, microstructures of Nb/MoSi$_2$laminate composites were evaluated from the variation of fabricating conditions, such as preparation temperature, applied pressure, and pressure holding time. MoSi$_2$-based composites have been developed in new materials for jet engines of supersonic-speed airplanes and gas turbines for high-temperature generators. These high performance engines may require new hard materials with high strength and high temperature-resistance. Also, with the exception of grinding, traditional machining methods are not applicable to these new materials. Electric discharge machining (EDM) is a thermal process that utilizes a spark discharge to melt a conductive material. The tool electrode is almost -unloaded, because there is n direct contact between the tool electrode and the work piece. By combining a non-conducting ceramic with more conducting ceramic, it was possible to raise the electrical conductivity. From experimental results, it was found that the lamination from Nb sheet and MoSi$_2$ powder was an excellent strategy to improve hardness characteristics of monolithic MoSi$_2$. However, interfacial reaction products, like (Nb, Mo)SiO$_2$and Nb$_2$Si$_3$formed at the interface of Nb/MoSi$_2$, and increased with fabricating temperature. MoSi$_2$composites, with which a hole drilling was not possible through the conventional machining process, enhanced the capacity of ED-drilling by adding MbSi$_2$, relative to that of SiC or ZrO$_2$reinforcements.

The Relationship between Hardness and Vitreousity of Korean Wheat Cultivars

  • Go Eun Lee;Kyeong-Hoon Kim;Jinhee Park;Kyeong-Min Kim;Chang-Hyun Choi;Mina Kim;Myoung Hui Lee;Chon-Sik Kang;Jiyoung Shon;Jong-Min Ko
    • Proceedings of the Korean Society of Crop Science Conference
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    • 2022.10a
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    • pp.298-298
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    • 2022
  • Milling is an important process that determines the quality of flour and is affected by milling machine type, scale, and tempering conditions. In addition, seed hardness is an important factor in determining the amount of tempering water and has been reported to affects flour yield and flour quality. There are reports that vitreousity is used as a measure to distinguish between soft and hard seeds, and the higher the vitreousity, the higher the protein contents. However, there is no established system for measuring viterousity of seeds and studies on the vitreousity and quality characteristics of flour are insufficient. Therefore, in this study, vitreousity, hardness, and milling characteristics were evaluated for 46 major domestic varieties, and their relationship was confirmed. After cutting the seeds using a seed cutter, vitreousity was measured, and seed hardness and flour particle size was measured using SKCS and PSI, respectively. As for the seed hardness index, 'Joa' was the lowest with 11.6, 'Yeonbaek' was the highest with 78.7. As for the milling yield, 'Saeol' had the lowest at 58.1%, and 'Hcjoong' had the highest at 88.6%. Seed hardness index and wheat flour production showed a high positively correlation, showing a similar to that of previous studies. Also, in flour particle size, 'Gobun' was the largest at 75.5 pm, and 'Joa' was the smallest at 43.1 um. Flour yield and flour particle size showed a high positively correlation. As a result of vitreousity, 'Hwangeumal' (55.2%), 'Saekeumkang' (59.1%), 'Baekkang' (52.3%), 'Goso' (44.6%), and 'Joa' (19.2%) were showed. Seed hardness and vitreousity showed a high positively correlation. Also as the vitreousity increased, the flour yield also showed a tendency to increase. In addition, as the seed hardness increased, particle size of the flour yield also showed a tendency to increase. It is thought that this result can be used as a measure to determine the quality of flour with vitreousity. However, further analysis of wheat varieties and methods of analyzing vitreousity are needed.

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Monitoring and machinability evaluation in high-speed machining of high hardness steel(SKD11) (고경도강(SKD11)의 고속가공에서 가공성 평가 및 감시)

  • 김전하;김경균;강영창;김정석;김기태
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2000.05a
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    • pp.987-990
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    • 2000
  • In modern manufacturing industry such as aerospace, vehicle and die/mold industry, the high hardness malarial which is remarkable in aspects of durability is effectively used. The high-speed and precision machining technology has been applied in these fields. In this study, efficient sensors in high-speed machining by observing similar tendency through comparing cutting force with AE signal, gap sensor signal and accelerometer signal are selected, and machinability of high-speed machining is experimentally evaluated. We performed a basic research for sensing system construction to monitor a machine tool and machining condition.

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Hardness and Dimensional Stability of Thermally Compressed Domestic Korean Pine (국내산 잣나무 열압밀화재의 경도와 치수안정성)

  • Hwang, Sung-Wook;Cho, Beom-Geun;Lee, Won-Hee
    • Journal of the Korean Wood Science and Technology
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    • v.43 no.1
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    • pp.68-75
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    • 2015
  • We conducted a thermal compression of domestic Korean pinewood for a use in flooring. For the evaluation of flooring material, we measured dimensional stability and surface hardness of thermally compressed wood. It is possible to make high-specific gravity woods with a range of 0.82-0.92 after the thermal compression with 50% compression set. The surface hardness increased with an increase in the pressing temperature. The highest value of surface hardness was $23.6N/mm^2$, which was obtained from the thermal compressed wood with pressing temperature of $160^{\circ}C$ and 30 minutes of pressing time. However, the surface hardness of woods treated at high temperature of $180^{\circ}C$ or greater decreased. The recovery of thickness decreased with increasing the pressing temperature. For dimensional stability, compression temperature was more dominant than compression time.

Evaluation of Brinell Hardness of Coated Surface Using Finite Element Analysis: Part 3 - Application to Multilayer Coatings (유한요소해석에 의한 코팅면의 브리넬 경도 평가: 제3보 - 다층 코팅에 적용)

  • Park, TaeJo;Kang, JeongGuk
    • Tribology and Lubricants
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    • v.37 no.6
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    • pp.240-245
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    • 2021
  • Ceramic coatings with high hardness and excellent chemical stability have been successfully applied to various machine elements, tools, and implants. However, in the case of monolayer coating on soft substrates, a high-stress concentration at the interface between the coating and the substrate causes delamination of the coating layer. Recently, to overcome this problem, multilayer coatings with a metal layer with a low modulus of elasticity added between the ceramic and the substrate have been widely applied. This study presents the third part of a recent study and focuses on the effect of the number of coating layers on the Brinell hardness of multilayered coating with TiN/Ti, following the two previous studies on a new Brinell hardness test method for a coated surface and on the influence of substrate and coating thickness. Indentation analyses are performed using finite element analysis software, von Mises stress and equivalent plastic strain distributions, load-displacement curves, and residual indentation shapes are presented. The number of TiN/Ti layers considerably affect the stress distributions and indentation shapes. Moreover, the greater the number of TiN/Ti layers, the higher is the Brinell hardness. The stress and plastic strain distributions confirm that the multilayer coatings improve the wear resistance. The results are expected to be used to design and evaluate various coating systems, and additional study is required.

Effects of Co Addition in High Strength and Low Thermal Expansion Invar Alloy (고강도 저열팽창 인바합금에 있어서 CO 첨가의 영향)

  • Kim, Bong-Seo;Jo, Yeong-Am;Yoo, Kyung-Jae;Kwon, Hae-Woong;Lee, Hui-Ung;Kim, Byung-Geol
    • Proceedings of the KIEE Conference
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    • 1999.07d
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    • pp.1901-1903
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    • 1999
  • To investigate invar alloy as a core material for increased capacity over-head transmission line which have high strength and low thermal expansion coefficient, hardness and thermal expansion coefficient of Fe-Ni-Co alloy have been studied. It is necessary that invar alloy have low thermal expansion coefficient and high strength for increased capacity over-head transmission line. In this paper. we tried to find out the effect of Ni and Co which has ferromagnetic properties and high saturation magnetization. It was found that Ni decrease thermal expansion coefficient and hardness, Co decrease thermal expansion coefficient but increase hardness in Fe-xNi-Co system. In Fe-(29-x)Ni-Co system, the material has no low thermal expansion properties substituting Co instead of Ni in concentration range of $1\sim7$%Co.

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High Temperature Properties of the High Speed Steel Roll of Hot Finishing Mill (열간 압연용 고속도강 롤의 고온 특성)

  • Kim, Tae-Woo;Choi, Jin-Won;Kim, Dong-Gyu
    • Journal of Korea Foundry Society
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    • v.16 no.2
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    • pp.124-131
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    • 1996
  • High temperature properties such as hot hardness and thermal fatigue resistance of high speed steel roll of hot finishing mill have been investigated. Two kinds of roll having compositions, Fe-1.75%C-5.9%Cr-1.74%Mo-4.94%V-2.03%W(A specimen) and Fe-2.27%C-8.86%Cr-2.91%Mo-3.92%V-1.86%W(B specimen)were prepared for investigating the microstructure and crack propagation mode. A specimen has greater amounts of $M_7C_3$ type carbides and less amounts of MC type carbides in comparison with B specimen. Hot hardness showed sudden decrease over $400^{\circ}C$, resulting in the hardness decrease of 50% at the temperature of $600^{\circ}C$, and showed little variation with time at $500^{\circ}C$ and $800^{\circ}C$. Thermal crack was developed at $550^{\circ}C$ in A specimen and $600^{\circ}C$ in B specimen.

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Corrosion Resistance and Low Friction Property of Sintered Steel Parts via Chromizing Treatment (크로마이징 처리 된 철계 소결 부품의 내식성 및 저 마찰특성)

  • Kim, Sang-Gweon;Park, Yong-Jin;Yeo, Kuk-Hyun;Lee, Jae-Hoon
    • Korean Journal of Metals and Materials
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    • v.50 no.11
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    • pp.809-815
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    • 2012
  • Recently, as the interest in improving energy efficiency has grown, the demand for vehicle and machine parts that are resistant in high temperature corrosive conditions and abrasive environments has increased. Pack chromizing treatment of sintered steels is a profitable method that satisfies both corrosion resistance and low friction properties. Since austenitic stainless steels have good corrosion resistance but low mechanical hardness, if they are replaced by sintered steel parts with pack chromizing treatment, all the desirable properties such as low price, easy molding, high hardness, low frictional coefficient, and high corrosion resistance, can be obtained. The higher corrosion resistance of the chromized parts over that of the austenitic stainless steels was acquired by coating chromium carbides and a thin chromium oxides layer on the surface. Moreover, the surface morphology of chromized parts, which were composed of chromium rich phases and hardened chromium carbides by diffusing and alloying, had a peak-and-valley shape so that the dimple effect by the wrinkled morphology and high hardness induced a low friction coefficient.