• Journal of the Korean Society for Heat Treatment
• /
• v.36 no.5
• /
• pp.261-269
• /
• 2023

This study aims to investigate the effects of tungsten additions on the microstructure, corrosion characteristics, and hardness of super duplex stainless steel heat-treated at two different annealing temperatures. Under the annealing temperature of 1100℃, the microstructure of the stainless steels consisted mainly of ferrite, while under the annealing temperature of 1000℃, significant amounts of austenite and secondary phases were also observed. In terms of corrosion characteristics in 3.5 wt%NaCl solution, there was not a significant difference due to W addition at the 1100℃ conditions. However, at the 1000℃, a tendency of decreased corrosion resistance was observed with increasing the tungsten content. On the other hand, the micro-hardness of the stainless steel heat-treated 1000℃ showed an increasing trend with tungsten addition. This increase can be mainly attributed to the higher fraction of secondary phases, primarily sigma, known for their high hardness.

• Journal of Korean Society of Steel Construction
• /
• v.14 no.5 s.60
• /
• pp.647-656
• /
• 2002

High-strength steel in steel bridges is the key to achieving cost-efficiency because it facilitates lightweight construction and rationalizes structure. The future of high-strength steel is bright, with its use projected to expand. As such, it is necessary to evaluate precisely various factors affecting the process of fabricating high-strength steel, i.e., welding heat, strain hardening, and weldability and performance of the welded joints. This study therefore performed the maximum hardness test and y-groove weld crack test using welding processes such as SAW, FCAW, and GMAW, in order to investigate the welding performance and characteristics of welded Joints or high-strength steel produced in Korea such as SM570, POSTEN60, and POSTEN80. In addition, a series of welding tests was carried out to estimate the tensile strength, bending characteristics, absorbed energy, and hardness in welded joints.

• Journal of the Korean Society for Heat Treatment
• /
• v.6 no.2
• /
• pp.98-106
• /
• 1993

Ultra high carbon steel (Fe-1.4%C) was prepared by means of a high frequency induction furnace. The preferred nucleation site of martensite was observed. The changes of hardness and impact thoughness due to tempering temperatures, and the spheroidization of cementite by controlled -rolling were also studied for the steel. The preferred nucleation site of martensite in the ultra high carbon steel is prior austenite grain boundary. The hardness of the steel is slightly increased up to about $300^{\circ}C$, and then decreased with further tempering temperature. However, the impact energy keeps a almost constant value, independent of the tempering temperature. The spheroidization of cementite is accelerated as the reduction in thickness per rolling pass is increased and the number of the rolling passes becomes greater.

• Transactions of the Korean Society of Mechanical Engineers
• /
• v.19 no.3
• /
• pp.705-712
• /
• 1995

The wear characteristics and wear mechanisms in TiN coating deposited on high speed steel and alloy tool steel by ion plating were investigated. Pin on V-block wear tester was used for a wear test method. The specimen was composed of three kinds of high speed steel and alloy tool steel which had different hardness by changing the heat treating condition. Three kinds of coating thickness were also applied to each specimen. Microscopic observation of worn surfaces was made by SEM. The scratch test of coating surface by the ion plating showed that critical load to break the coating interface was greater than 50N. The critical load increased with both substrate hardness and coating thickness. The wear resistance of TiN coated high speed steel became 10 times greater than that of non-coated ones. SEM observation showed that leading edge of contact was compressive and trailing edge was under maximum tensile stress and then surface cracking broke out perpendicular to sliding direction.

• Journal of Surface Science and Engineering
• /
• v.38 no.2
• /
• pp.79-82
• /
• 2005

This study investigated the effect of nitriding on the hardness and adhesion properties of $TiB_2$ coatings. Inductively coupled plasma (ICP) was used for both nitriding and deposition. By applying ICP, H13 steel was nitrided at a high rate of $50\;{\mu}m/hr$. After nitriding, a Fe4N compound layer or a diffusion layer was formed according to the hydrogen/nitrogen ratio. Both layers could improve the load-bearing capacity of the substrate by increasing the substrate hardness. The adhesion of the $TiB_2$ coatings increased to $\~30N$ after nitriding, but the hardness of the coating was lowered to 20-30 GPa. However, the adhesion of the $TiB_2$ coatings with a high hardness (>60 GPa) could not be improved substantially by nitriding due to the large difference in hardness between the coating and the substrate. The grain size of the $TiB_2$ coating was larger on the nitrided substrates, resulting in a decrease in the hardness of the coating.

• Journal of the Korean Society for Heat Treatment
• /
• v.37 no.4
• /
• pp.182-187
• /
• 2024

To improve and control the mechanical properties of low alloy steel, the influence of quenching and tempering process conditions was investigated. In the case of quenching heat treatment, a comparison was made between the conventional method of heating to the austenite region followed by single quenching and a method involving double quenching, followed by high-temperature tempering. It was observed that specimens subjected to double quenching exhibited significantly finer tempered microstructures compared to those subjected to conventional quenching, resulting in noticeably higher hardness. Additionally, a study was conducted to investigate the variation in hardness with changes in tempering temperature and time after the same conventional quenching treatment. As expected, an increase in tempering temperature or time led to a decrease in hardness, and the correlation between hardness and the Hollomon-Jeffe Parameter was confirmed. It was also observed that during high-temperature tempering, the size of carbides significantly increased.

• Nuclear Engineering and Technology
• /
• v.31 no.6
• /
• pp.561-571
• /
• 1999

Microstructure and mechanical properties of five Cr-Mo steels for nuclear industry applications have been investigated. Transmission electron microscopy, energy dispersive spectrometer, differential scanning calorimeter, hardness, tensile, and impact test were used to evaluate the Cr and W effect on the microstructure and mechanical properties. Microstructures of Cr-Mo steels after tempering are classified into three types : bainitic 2.25Cr-lMo steel, martensitic Mod.9Cr-lMo, HT9M, and HT9W steels, and dual phase HT9 steel. The majority of the precipitates were found to be M$_{23}$C$_{6}$ carbides. As minor phases, fine needle-like V(C,N), spherical NbC, fine needle-like Cr-rich Cr$_2$N, and Cr-rich M$_{7}$C$_3$were also found. Addition of 2wt.% W in Cr-Mo steels retarded the formation of subgrain and dissolution of Cr$_2$N precipitates. Hardness and ultimate tensile strength increased with increasing Cr content. Though Cr content of HT9W steel was lower than that of HT9 steel, the hardness of HT9W was higher due to the higher W content. W added HT9W steel had the highest ultimate tensile strength above $600^{\circ}C$. But impact toughness of W added steel (HT9W) and high Cr steel (HT9) was low.w.w.

• Journal of the Korean Society for Heat Treatment
• /
• v.20 no.4
• /
• pp.175-180
• /
• 2007

The hardness of cold-forged products is in close relationship with its effective strain. This study presented the estimating method of hardness for cold-forged SKH9 products without hardness tests in view of resistance to plastic deformation using finite element code, DEFORM$^{TM}$. The flow stress equation obtained from the compression test was only used as a basic data to estimate the relationship between effective strain and hardness. In addition, this new estimating method was applied to the cold-forged product which was widely used in industrial field to show the feasibility. As a result, the predicted hardness numbers through FE simulation showed good agreement with the measured hardness numbers. It is possible to estimate the hardness not by hardness tests, but by only computer simulations for the deformed products. Also, effective strain values were possibly estimated by measuring hardness numbers, and vice versa.

• Laser Solutions
• /
• v.14 no.1
• /
• pp.19-24
• /
• 2011

This work reports the results for laser shock peening of duplex stainless steel (22% Chromium - 5% Nickel) using a pulsed Nd:YAG laser (wavelength = 532nm, pulse width = 8ns). for the application to high-capacity pumps for seawater desalination plants. By properly selecting the process parameters such as laser intensity of 10GW/$cm^2$, laser pulse density of 75pulse/$mm^2$, and $100{\mu}m$ thick aluminum foil as an absorbent coating layer, the surface hardness of duplex stainless steel could be enhanced by 26%, from 256HV to 323HV with little changes in surface morphology and roughness. The depth of laser shock peened layer was measured to be around 2mm. The large enhancement of surface hardness is considered to have high practical importance in minimizing abrasive and corrosive deterioration of pump parts.

• Journal of the Korean Society for Heat Treatment
• /
• v.25 no.3
• /
• pp.115-120
• /
• 2012

It has been known that the ferritic stainless steel can be changed to martensitic stainless steel when nitrogen is added. However the high hardness of martensitic stainless steel prevents the plastic deformation. In this study, instead of martensite, the surface microstructure was changed into nitrogen pearlite to increase the plastic deformation easily by isothermal heat treatment after high temperature gas nitriding (HTGN) the AISI 430 ferritic stainless steel. The isothermal treatment was carried out at $780^{\circ}C$ for 4, 6, and 10 hrs, respectively, after HTGN treatment at $1100^{\circ}C$ for 10 hrs. The surface layer of isothermal-treated steel appeared nitrogen pearlite composed with fine chromium nitride and ferrite. Hence, the interior region that was not affected by nitrogen permeation exhibited ferrite phase. When quenching the isothermal treated steel at 1100oC, martensitic phase formed at the surface layer. The hardness of surface layer of isothermal-treated steel and quenched steel measured the value of 150~240 Hv and 630 Hv, respectively.