• 제목/요약/키워드: Hexagonal-shaped

검색결과 76건 처리시간 0.019초

용융염법으로 합성한 Ba-ferrite 입자의 특성 (Properties of ba-ferrite Particles Synthesized by Molten Salt Method)

  • 오영우
    • 한국전기전자재료학회논문지
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    • 제13권6호
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    • pp.545-550
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    • 2000
  • In order to synthesize Ba-ferrite particles by molten salt method KCl and NaCl were added to basic composition to 50% by weight. X was varied from 0.0 to 1.0 to control the magnetic properties in $BaFe_{12-2x}$/ $Co_{x}$ / $Ti_{x}$ / $O_{19}$ and 1 mol% of $SiO_2$was added to control the aspect ratio of hexagonal platelets. And the effects of reaction temperatures were examined by varying the temperature from 85$0^{\circ}C$ to 120$0^{\circ}C$ with 5$0^{\circ}C$ intervals. Eutectic composition of NaCl and KCl lowered the crystallizing temperature of Ba-ferrite in molten salts than using KCl and NaCl separatly. The morphology of resulting Ba-ferrite particles was clearly hexagonal-shaped plates. $H_{c}$ and $M_{r}$ were decreased when F $e^{3+}$ was substitued with $Co^{2+}$ and $Ti^{4+}$ from x=0 to x=1.0 in $BaFe_{12-2x}$/ $Co_{x}$ / $Ti_{x}$ / $O_{19}$ . Adding 1mol% $SiO_2$in molten salt method increased the size but shortened c-axis of the hexagonal ferrites and this result is an opposite phenomenon compared with the result in solid-statge reaction.n.ion.n.

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Morphological Control of Periodic Mesoporous Organosilica with Agitation

  • 박성수;이치헌;전종현;조상준;박동호
    • Bulletin of the Korean Chemical Society
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    • 제22권9호
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    • pp.948-952
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    • 2001
  • Periodic mesoporous organosilicas with rope-based morphology from a reaction gel composition of 1 BTME : 0.57 ODTMABr : 2.36 NaOH : 353 H2O were synthesized. While long rope-shaped product dominated in case of static synthesis condition , gyroid type products instead of rope shaped product appeared and rope shaped product disappeared with agitation. PMO with such a long rope shaped morphology is firstly reported. Additionally, various rope-based morphologies depending on the degree of bending, twisting, folding and winding of rope such as spirals, discoids, toroids, and worm-like aggregates were observed. White powdered products were characterized by X-ray diffraction, N2 sorption measurement, SEM and TEM. From XRD pattern and TEM image, ODTMA-PMO with hexagonal symmetry was identified. The pore diameter and BET surface area of ODTMA-PMO are $32.9{\AA}$ and 799 m2g-1 , respectively. Hexagonally arrayed channels run with long axis of rope and rope-based shapes with various degree of curvature, which was elucidated by using TEM images.

다전극 산소 센서를 이용한 고분자 막의 산소 투과도 측정 장치 연구 (A Study on the Apparatus for Measuring Oxygen-Permeability of Membranes with a Multi-Electrode Oxygen Sensor)

  • 정일손;정재칠;김태진
    • 센서학회지
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    • 제21권3호
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    • pp.229-234
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    • 2012
  • The existing permeability measurements based on pressure differential between the polymer membrane that is permeable to measure the amount of oxygen used, but these methods must be kept in a vacuum, and the measurement of the membrane with low permeability in the membrane is too time consuming. In recent years by using electrochemical method polymer membrane currents caused by the amount of oxygen is a measure of how much is used. In this study, apparatus consisting of one anode and six cathodes for multi-oxygen permeability tester used the same number of membranes produced by electrochemical oxygen permeation characteristics. In this study, one silver/silver chloride anode electrochemical method with a hexagonal sensor to put various kinds of polymer membranes with the six oxygen permeability for simultaneous measurement in real-time systems. Six cathodes (Pt), and one of the coil-shaped anode (Ag/AgCl) to form a hexagonal one of the polarographic oxygen sensor in a single measurement system by six sensors. Each sensor for making hexagonal specificity of the sensor to compensate for the conditions obtained in a pure nitrogen gas and pure oxygen gas conditions. With this study, self-developed hexagonal sensor capable of measuring sensors and oxygen permeability tester, for a multi-six different oxygen permeability characteristics of the membrane measured at the same time.

육각형 대칭 패턴 프랙탈 모노폴 안테나에 대한 연구 (A Study on Fractal Monopole Antenna with Hexagonal Symmetrical Pattern)

  • 장대순;강상원
    • 한국인터넷방송통신학회논문지
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    • 제22권1호
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    • pp.121-126
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    • 2022
  • 본 연구는 변형된 힐버트 커브 프랙탈 모노폴 구조를 단순화하여 육각형 대칭 패턴을 가지면서 모노폴 형태로 구현한 안테나에 대한 것이다. 힐버트 커브 프랙탈 모노폴 구조를 단순화하여 소형화했을 뿐 아니라 성능 개선을 모색하기 위해 복사기 구조를 육각형 대칭 패턴으로 구현했다. 기판 유전체의 비유전율은 4.7이며, 미앤더 형태로 대칭 구조를 갖는 총 선로길이는 59 mm이다. 안테나의 크기는 10 mm × 10 mm × 0.8 mm이고, 선폭은 0.4 mm이다. 안테나 측정 지그의 크기는 64 mm × 21 mm × 1 mm이다. 공진주파수는 1.57 GHz 이고, 주파수 범위는 1.51 ~ 1.615 GHz이다. 주파수대역폭은 105 MHz이다. 안테나 이득은 YZ-plane의 측정이득은 2.32 dBi 이고, XZ-plane의 경우 -1.03 dBi를 얻었다. 결과적으로 육각형 대칭 패턴 프랙탈 구조를 이용하여 안테나 소형화를 이루었으며, 복사기 구조 변화로 안테나 성능 개선이 용이함을 확인했다.

공기 중에서 열증발법에 의하여 제작된 튜브 형상의 ZnO 결정 (Tubular-shaped ZnO Crystals by Thermal Evaporation Technique in Air)

  • 이정헌;이근형;남춘우
    • 한국전기전자재료학회논문지
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    • 제27권3호
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    • pp.141-145
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    • 2014
  • Tubular-shaped ZnO crystals were synthesized by thermal evaporation technique under air atmosphere. Mixture of Zn and Mg powder was used as the source material. The thermal evaporation and oxidation of Zn/Mg mixture were carried out for 1 hr at $1,000^{\circ}C$ and $1,200^{\circ}C$ under in air under atmospheric pressure. When only Zn powder was used as a source material, tetrapod-shaped ZnO crystals were synthesized. This provides that Mg played a key role in the formation of the tubular-shaped crystals. SEM images showed that the tubular-shaped ZnO crystals grew along [0001] direction. XRD spectrum revealed that the ZnO tubes had hexagonal wurtzite structure. Two emission peaks at 380 nm and 510 nm were observed in the room temperature cathodoluminescence spectrum.

고속 블록 정합 움직임 측정을 위한 십자-다이아몬드-삼각 탐색 알고리즘 (A Cross-Diamond-Triangle Search Algorithm for Fast Block-Matching Motion Estimation)

  • 김성훈;신재민;오승준;안창범;박호종;심동규
    • 방송공학회논문지
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    • 제10권3호
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    • pp.357-371
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    • 2005
  • 본 논문에서는 CDS(Cross-Diamond Search algorithm) 및 CDHSs(Cross-Diamond-Hexagonal Search algorithms)의 성능을 향상시키기 위하여 탐색 영역의 위치에 따라 최적의 탐색 형태를 적용하는 CDTS(Cross-Diamond-Triangle Search algorithm)를 제안한다. CDTS에서 탐색 영역의 위치에 따라 최적의 탐색 형태를 적용하기 위하여 다양한 실험 영상들의 움직임 분포를 먼저 분석하였다. 분석된 움직임 분포에 근거하여 CDTS 구현 시 탐색 영역 중심부에서는 십자 탐색 형태와 다이아몬드 탐색 형태를 적용하고, 나머지 탐색 영역에서는 삼각 탐색 형태와 다이아몬드 탐색 형태를 적용한다. CDTS에서 제안하는 삼각 탐색 형태는 기존 탐색 알고리즘에서 사용하는 대칭형 구조와는 다르게 비대칭형 구조를 가지고 탐색점을 더욱 감소시키는 효과를 제공하면서도 화질을 유지할 수 있다. CDTS를 CDS 및 CDHSs와 비교하였을 때 화질 열화 없이 각각 평균 16.22$\%$ 및 3.09$\%$ 정도의 탐색점 감소 효과가 나타났다.

Steel hexagonal damper-brace system for efficient seismic protection of structures

  • Mohammad Mahdi, Javidan;Jinkoo, Kim
    • Steel and Composite Structures
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    • 제45권5호
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    • pp.683-695
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    • 2022
  • Conventional braces are often used to provide stiffness to structures; however due to buckling they cannot be used as seismic energy dissipating elements. In this study, a seismic energy dissipation device is proposed which is comprised of a bracing member and a steel hysteretic damper made of steel hexagonal plates. The hexagonal shaped designated fuse causes formation of plastic hinges under axial deformation of the brace. The main advantages of this damper compared to conventional metallic dampers and buckling-restrained braces are the stable and controlled energy dissipation capability with ease of manufacture. The mechanical behavior of the damper is formulated first and a design procedure is provided. Next, the theoretical formulation and the efficiency of the damper are verified using finite element (FE) analyses. An analytical model of the damper is established and its efficiency is further investigated by applying it to seismic retrofit of a case study structure. The seismic performance of the structure is evaluated before and after retrofit in terms of maximum interstory drift ratio, top story displacement, residual displacement, and energy dissipation of dampers. Overall, the median of maximum interstory drift ratios is reduced from 3.8% to 1.6% and the residual displacement decreased in the x-direction which corresponds to the predominant mode shape of the structure. The analysis results show that the developed damper can provide cost-effective seismic protection of structures.

Synthesis, Structural Characterization, and Catalytic Activity of Flower Like ZnO Nanostructures

  • Ramachandran, K.;Kumar, G. Gnana;Kim, Ae Rhan;Yoo, Dong Jin
    • Bulletin of the Korean Chemical Society
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    • 제35권4호
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    • pp.1091-1097
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    • 2014
  • Tageteserecta flower like zinc oxide nanostructures composed of hexagonal nanorods were synthesized via sonochemical method at room temperature. The synthesized nanomaterials exhibited wurtzite hexagonal phase structure with the single crystalline nature. The diameter of the individual nanorods that constitute the flower shaped zinc oxide structures is in the range of 120-160 nm. The sonication time effectively determined the morphological properties of the prepared materials. The catalytic activity of prepared zinc oxide nanostructures towards N-formylation reactions were evaluated without any surface modification and the nanostructures exhibited good reaction yield with the prompt recyclability behavior.

비축대칭 전후방압출공정의 UBET해석 (A UBET Analysis of Non-axisymmetric Forward and Backward Extrusion)

  • 이희인;김진규;황범철;배원병
    • 한국정밀공학회지
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    • 제18권1호
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    • pp.154-161
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    • 2001
  • A UBET analysis has been carried out to predict the forming load and the extruded length of forward and backward extrusion of hexagonal and trochoidal wrench colts. For the upper bound load and the average length of the extruded billets are determined by minimizing the total energy consumption rate which is a function of unknown velocities and parameters at each element. Experiments are carried out with antimony-lead billets at room temperature using hexagonal and trochoidal shaped punches. The theoretical predictions of the forming load and the extruded length are in good agreement with the experimetal results.

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Mn 분말을 환원제로 사용하여 열증발법에 의해 생성된 ZnO 마이크로/나노결정 (ZnO Micro/Nanocrystals Synthesized by Thermal Evaporation Method using Mn Powder as the Reducing Agent)

  • 소호진;이근형
    • 한국재료학회지
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    • 제29권7호
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    • pp.432-436
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    • 2019
  • Zinc oxide(ZnO) micro/nanocrystals are grown via thermal evaporation of ZnO powder mixed with Mn powder, which is used as a reducing agent. The ZnO/Mn powder mixture produces ZnO micro/nanocrystals with diverse morphologies such as rods, wires, belts, and spherical shapes. Rod-shaped ZnO micro/nanocrystals, which have an average diameter of 360 nm and an average length of about $12{\mu}m$, are fabricated at a temperature as low as $800^{\circ}C$ due to the reducibility of Mn. Wire-and belt-like ZnO micro/nanocrystals with length of $3{\mu}m$ are formed at $900^{\circ}C$ and $1,000^{\circ}C$. When the growth temperature is $1,100^{\circ}C$, spherical shaped ZnO crystals having a diameter of 150 nm are synthesized. X-ray diffraction patterns reveal that ZnO had hexagonal wurtzite crystal structure. A strong ultraviolet emission peak and a weak visible emission band are observed in the cathodoluminescence spectra of the rod- and wire-shaped ZnO crystals, while visible emission is detected for the spherical shaped ZnO crystals.