• Title/Summary/Keyword: Heating film

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Physical Properties of ZnO Thin Films Grown by Sol-Gel Process with Different Preheating Temperatures (예열 온도 변화에 따른 Sol-Gel 법에 의해 제작된 ZnO 박막의 물리적 특성 연구)

  • 김익주;한호철;이충선;송용진;태원필;서수정;김용성
    • Journal of the Korean Ceramic Society
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    • v.41 no.2
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    • pp.136-142
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    • 2004
  • A homogeneous and stable ZnO sol was prepared by dissolving the zinc acetate dihydrate(Zn(CH$_3$COO)$_2$$.$2H$_2$O) in solution of isopropanol((CH$_3$)$_2$$.$CHOH) and monoethanolamine(MEA:H$_2$NCH$_2$CH$_2$OH). ZnO thin films were prepared by sol-gel spin-coating method and investigated for c-axis preferred orientation and physical properties with preheating temperature. The c-axis growth had a difference as increaing preheating temperature. ZnO thin film preheated at 275$^{\circ}C$ and post-heated at 650$^{\circ}C$ was highly oriented along the (002) plane. After preheating at 200∼300$^{\circ}C$ and post-heating at 650$^{\circ}C$, the transmittance of ZnO thin films by UV-vis. measurement was over 85% in visible range and exhibited absorption edges at about 370 nm. The optical band gap energy was obtained about 3.22 eV, The photoluminescence emission characteristics of ZnO thin film preheated at 275$^{\circ}C$ and post-heated at 650$^{\circ}C$ was found to orange emission(620 nm, 2.0 eV) by PL measurement, which revealed the possibility for application of inorganic photoluminescence device.

Thick Film Gas Sensor Based on PCB by Using Nano Particles (나노 입자를 이용한 PCB 기반 후막 가스 센서)

  • Park, Sung-Ho;Lee, Chung-Il;Song, Soon-Ho;Kim, Yong-Jun
    • Journal of the Microelectronics and Packaging Society
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    • v.14 no.2 s.43
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    • pp.59-63
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    • 2007
  • This paper presented a low-cost thick film gas sensor module, which was based on simple PCB (Printed Circuit Board) process. The proposed sensor module included a $NO_2/H_2$ gas sensor, a relative humidity sensor, and a heating element. The $NO_2/H_2$ gas and relative humidity sensors were realized by screen-printing $SnO_2,\;BaTiO_3$ nano-powders on IDTS (Interdigital Transducer) of a PCB substrate, respectively. At first 1% $H_2$ gas flowed into the sensor chamber. After 4 min, air filled the chamber while $H_2$ gas flow stopped. This experiment was performed repeatedly. The Identical procedure was used for the $NO_2$ detection. The result for sensing $H_2$ gas showed the increase of voltage from 0.8V to 3.5V due to the conductance increase and its reaction response time by hydrogen flow was 65 sec. $NO_2$ sensing results showed 2.7 V voltage drop due to the conductance decrease and its response time was 3 sec through a voltage monitoring.

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Spot marking of the multilayer thin films by Nd:YAG laser (Nd:YAG 레이저에 의한 다층 박막의 미소 점 마킹)

  • Kim, Hyun-Jin;Shin, Yong-Jin
    • Korean Journal of Optics and Photonics
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    • v.15 no.4
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    • pp.361-368
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    • 2004
  • We separated the multilayer structure of CD-R(compact disk-recordable) and investigated optimal spot marking conditions and physical and chemical transitions in response to various laser beam energh levels. Spot marking(80 ${\mu}{\textrm}{m}$ spot size) was produced on the surface of each layer using a Q-switched Nd:YAG laser between 27 mJ and 373mJ. By investigating resulting pit formation with Optical Microscopy(OM) and Optical Coherence Tomography(OCT), we analyzed the formation process of spot marking in the multilayer structure of different chemical composition. The localized heating of the substrate in the multilayer thin film caused the short temporal thermal expansion, and absorbed optical energy between reflective and dye interfaces melted dye and increased the volume. During the cooling phase, formation of pit and surrounding rim can be explained by three distinct processes; effect of surface tension, evaporation by spontaneous temperature increase due to laser energy, and mass flow from the recoil pressure. Our results shows that the spot marking formation process in the multilayer thin film is closely related to the layers' physical, chemical, and optical properties, such as surface tension, melt viscosity, layer thickness, and chemical composition.

Development on Glass Formulation for Aluminum Metal and Glass Fiber (유리섬유 및 알루미늄 금속 혼합물 유리조성 개발)

  • Cho, Hyun-Je;Kim, Cheon-Woo
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.10 no.4
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    • pp.247-254
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    • 2012
  • Vitrification technology has been widely applied as one of effective processing methods for wastes generated in nuclear power plants. The advantage of vitrifying for low- and intermediate-level radioactive wastes has a large volume reduction and good durability for the final products. Recently, a filter using on HVAC(Heating Ventilating & Air Conditioning System) is composed with media (glass fiber) and separator (aluminum film) has been studied the proper treatment technology for meeting the waste disposal requirement. Present paper is a feasibility study for the filter vitrification that developing of the glass compositions for filter melting and melting test for physicochemical characteristic evaluation. The aluminum metal of film type is preparing with 0.5 cm size for proper mixing with glass frit, glass fiber is also preparing with 1 cm size within crucible. The glass compositions should be developed considering molten glass are related with wastes reduction. Glass compositions obtained from developing on glass formulation are mainly composed of $SiO_2$ and $B_2O_3$ for aluminum metal. A variety of factors obtained from the glass formulation and melting test are reviewed, which is feeding rate and glass characteristics of final products such as durability for implementing the wastes disposal requirement.

A Study on the Friction and Wear Characteristics of Contact Sealing Units for a Small Hydro-power Turbine Under Various Rubbing Conditions (마찰접촉조건에 따른 소수력 수차용 밀봉장치의 마찰.마멸특성 연구)

  • Kim, Chung-Kyun
    • Tribology and Lubricants
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    • v.22 no.6
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    • pp.314-319
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    • 2006
  • In this paper, the friction and wear characteristics of contact type sealing unit far a water turbine have been presented. The sealing unit for a small hydropower generation is to stop a leakage of circulating water from an outside of an impeller to an inside of a rolling bearing. The friction heating between a seal ring and a seal seat may radically increase a surface temperature in which increase a power loss and wear on the rubbing surface. The surface wear strongly affect to the seal life of a mechanical face seal. In this study, the hardness of a stainless steel in which is a heat-treated is 892.8 in Victors hardness and the hardness of silicone carbide of SiC is 714.1 in Victors hardness. The surface hardness of a heat-treated stainless steel is 25% high compared with that of a ceramic material of SiC. The contact modes of rubbing surfaces are a dry friction, a water film friction and a mixed friction that is contaminated by a dust, silt, and moistures, etc. These two factors of a contact rubbing modes and a material property are very important parameters on the tribological performance such as a friction and wear between a seal ring and a seal seat in primary sealing unit. The experimental result shows that the surface hardness of a seal material is very important on the friction coefficient and a wear volume. Thus, the results recommend higher hardness of a seal material, which may reduce a friction loss and increase a wear life of primary seal components.

Fabrication, temperature-dependent local structural and electrical properties of VO2 thin films

  • Jin, Zhenlan;Hwang, In-Hui;Park, Chang-In;Han, Sang-Wook
    • Proceedings of the Korean Vacuum Society Conference
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    • 2015.08a
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    • pp.169.2-169.2
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    • 2015
  • $VO_2$ is a well-known a metal-to-insulator-transition (MIT) material, accompanied with a first order structural phase transition near room temperature. Because of the structural phase transition and the MIT occur near a same temperature, there is an ongoing argument whether the MIT is induced by the structural phase transition. $VO_2$ exhibits a relatively weak anti-oxidization ability and can be oxidized to higher-valence oxides (e.g., $V_4$ $O_7$ or $V_2$ $O_5$) when annealed at a high temperature in an oxygen-rich atmosphere. We fabricated $VO_2$ films on $Al_2$ $O_3$ (0001) substrates using a DC magnetron sputtering deposition process with carefully control the $O_2$ percentage in an atmosphere. X-ray diffraction measurements from the films showed only (0l0) peaks with no extra peaks, indicating b-oriented films. The temperature-dependent local structural properties of $VO_2$ films were investigated by using in-situ X-ray absorption fine structure (XAFS) measurements at the V K edge. XAFS revealed that the structural phase transition was occurred nearly $70^{\circ}C$ for heating process and reproducible. Resistance measurements as a function of temperature (R-T) demonstrated that the resistance of $VO_2$ films was changed by a factor of 4 near $75^{\circ}C$ which was higher than $68^{\circ}C$ reported from a $VO_2$ bulk. We will discuss the MIT of $VO_2$ films, comparing with the local structural properties determined by XAFS measurements.

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A Numerical Study on Phonon Spectral Contributions to Thermal Conduction in Silicon-on-Insulator Transistor Using Electron-Phonon Interaction Model (전자-포논 상호작용 모델을 이용한 실리콘 박막 소자의 포논 평균자유행로 스펙트럼 열전도 기여도 수치적 연구)

  • Kang, Hyung-sun;Koh, Young Ha;Jin, Jae Sik
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.41 no.6
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    • pp.409-414
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    • 2017
  • The aim of this study is to understand the phonon transfer characteristics of a silicon thin film transistor. For this purpose, the Joule heating mechanism was considered through the electron-phonon interaction model whose validation has been done. The phonon transport characteristics were investigated in terms of phonon mean free path for the variations in the device power and silicon layer thickness from 41 nm to 177 nm. The results may be used for developing the thermal design strategy for achieving reliability and efficiency of the silicon-on-insulator (SOI) transistor, further, they will increase the understanding of heat conduction in SOI systems, which are very important in the semiconductor industry and the nano-fabrication technology.

Review on the Use of Solar Energy for Grain Drying (태양열을 이용한 곡물건조에 관한 연구)

  • 금동혁;고학균;최재갑
    • Journal of Biosystems Engineering
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    • v.3 no.1
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    • pp.64-76
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    • 1978
  • A dimensional supply of petroleum fuels and increased competition for petroleum products has made the conservation of energy in grain drying an important cost and management factor. Research on solar grain drying is directed toward utilization of a renewable energy source as an alternative to petroleum fuels for drying. There are many technical and economic problems in accepting and adopting solor energy as a new energy source for grain drying. The purpose of this study are to assess the state of the art of solar grain drying and to find out the problems by reviewing literatures available. The results obtained may be summarized as follows; 1.It may be considered that the weather conditions in October of Korea was satisfactory for the forced natural air and solar heated air drying. 2. Solar energy is considered more applicable to low-temperature, In-storage drying systems than to high-temperature, high-speed drying systems. In-storage drying systems require low levels of heat input. The costs of collector systems to provide low temperature are considerably cheaper than for high-temperature systems. 3. Tubular type collector made of polyvinyle film seems to be the most practical at this stage of development and black-painted bare-plate collectors mounted on the outside of a typical, round, low-temperature drying bin can supply an appreciable amount of the energy efficiently needed for low-temperature grain drying at a lower cost. 4. All of the grains in solar drying tests was successfully dried up to safe storaged moisture levels without significant spoilage. Drying rates with solar system were faster than natural air drying systems, and usually a little slower than similar low-temperature electric drying systems. 5. Final grain moisture levels were lower in solar tests than in natural air tests, and generally higher than in tests with continuous heated air. 6. Savings of energy by use of solar collectors ranged from 23% to 55%, compared to the natural and electric ileated air drying systems. However, total drying cost effectiteness tvas not significant. Therefore, it is desirable that solar grain dry-ing sIFstems tvhich could be suitable for multiple heating purposes on farms shouldbe developed. 7. Supplemental heat with solar radiation did little to reduce air flow requirementsbut refuced drying time and increased the p\ulcornerobability of successful drying duringdrying poriod.

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Structural and Thermal Properties of Polysulfone Membrane Including Graphene (그래핀을 포함하는 폴리설폰 멤브레인의 구조 및 열 특성)

  • Choi, Hyunmyeong;Choi, Yong-Jin;Sung, Choonghyun;Oh, Weontae
    • Membrane Journal
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    • v.28 no.1
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    • pp.37-44
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    • 2018
  • Polysulfone composites including graphene were prepared, and their thermal characteristics in membrane states were analyzed by using a custome-made residual stress analyzer and a thermal diffusivity analyzer based on laser flash method. The residual stress analysis was carried out on the polysulfone composite films deposited on Si (100) substrates for 1 cycle of heating and cooling runs. The flat membrane of graphene-embedded polysulfone composites were prepared by the phase transfer method in distilled water and the thermal conductivity was separately measured in the out-of-plane and the in-plane directions. The residual stress of the graphene-embedded polysulfone film was gradually decreased with increasing graphene loading and the out-of-plane thermal conductivity was distinguished from the in-plane thermal conductivity in the flat membranes. These thermal characteristics are caused by the structural uniqueness of graphene and the micro-void structures formed during membrane fabrication.

Thermal behavior of modified silicon surface by $CHF_3/C_2F_6$ reactive ion etching ($CHF_3/C_2F_6$ 반응성이온 건식식각에 의해 변형된 실리콘 표면의 열적 거동에 관한 연구)

  • Park, Hyung-Ho;Kwon, Kwang-Ho;Koak, Byong-Hwa;Lee, Joong-Whan;Lee, Soo-Min;Kwon, Oh-Joon;Kim, Bo-Woo;Seong, Yeong-Gwon
    • Korean Journal of Materials Research
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    • v.2 no.1
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    • pp.35-42
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    • 1992
  • Thermal behavior of residue and damaged layer formed by reactive ion etching (RIE) in $CHF_3/C_2F_6$ were investigated using X-ray photoelectron spectroscopy(XPS) and secondary ion mass spec-trometry(SIMS) techniques. Decomposition of polymer residue film begins at $200^{\circ}C$ and above $400^{\circ}C$ carbon compound as graphite mainly forms by in-situ resistive heating. It reveals that thermal decomposition of residue can be completed by rapid thermal anneal treatment above $800^{\circ}C$ under nitrogen atmosphere and out-diffusion of carbon and fluorine of damaged layer is observed.

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