• 열처리공학회지
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• 제27권2호
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• pp.72-78
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• 2014

Isothermal transformation behavior of a 10% Cr heat resistant steel fabricated by centrifugal casting process was investigated. Normalized specimen at $1100^{\circ}C$ for 1 hour was isothermally annealed at temperature range between $600^{\circ}C$ and $700^{\circ}C$ with various time. The annealed specimen had eutectoid structure which was generated along austenitic grain boundary during isothermal annealing. Areal fraction of eutectoid structure increased up to 25% after holding at $700^{\circ}C$ for 20 hours. It was observed that austenitic matrix was transformed to ferrite structure and fine $M_{23}C_6$ carbides with increase of annealing time. Time-temperature-transformation diagram of the centrifugally cast 10% Cr steel with 0.18 wt% C was plotted based on the results of isothermal transformation behavior.

• 한국공작기계학회:학술대회논문집
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• 한국공작기계학회 2001년도 추계학술대회(한국공작기계학회)
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• pp.336-340
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• 2001

Theoretical efforts were taken to investigate an optimum heat treatment process in martensitic stainlesssteel. The approach is based on the combination of the interpolation and extrapolation method of a standard heat treatment technology with the principle of quenching and tempering temperature difference. The relationship of macroscopic structure and fracture toughness and ductility as well as the Hardness and strength has been focused to induce a simple rule to apply with feasibility. As a result it was found that the grain size influences to the fracture toughness and ductility significantly.

• 한국공작기계학회논문집
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• 제14권1호
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• pp.24-29
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• 2005

Optimal heat treatment process in martensitic stainless steel such as SUS416 is investigated. The approach is based on the combination of the interpolation and extrapolation method of a standard heat treatment technology with the principle of quenching and tempering temperature difference. The relationship of the macroscopic structure, fracture toughness and ductility as well as the hardness and strength are considered to induce a simple rule to apply with feasibility. Consequently, Optimal heat treatment condition in martensitic stainless steel is proposed and is shown the better quality. It was found that the smaller pain size of microstructure gives the enhanced fracture toughness and ductility.

• 소성∙가공
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• 제11권5호
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• pp.388-393
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• 2002

Heat-treatment-free steels have been replacing for conventional quenched-and-tempered structural steels since the microalloyed forging steel was developed in early 1970s in Germany. Substantial cost reduction provides the driving force for this change. As a result of intensive R & D efforts and application trials, various kinds of grades, for example heat-treatment-free steels for hot forging, machining and cold heading, have been developed and moreover these steels are in tonnage production throughout the world. The developments in alloy steels, processing conditions and structure-property characteristics of the heat-treatment-free steels, are described and also recent trend and future prospect are summarized in this report.

• 한국전기전자재료학회논문지
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• 제11권7호
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• pp.502-507
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• 1998

The purpose of this study is to investigate the breakdown properties in joint interface of power cables with heat treatment. The specimens have the structure of XLPE/EPDM interface like the joint of distribution power cable. The breakdown characteristics of the SLPE/EPDM joint were studied with crosslinking by=products. AC breakdown voltages were measured with heat treatment time and interfacial materials and crosslinking by-products as testing factors. This study has shown that crosslinking by-product gases play an important role at the insulation properties of cable joints by heating. The dielectric strength shows the lowest values at 4 hours heat treatment. The AC breakdown strength in the untreated sample was increased with heat treatment time.

• Bulletin of the Korean Chemical Society
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• 제23권1호
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• pp.25-26
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• 2002

• 한국주조공학회지
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• 제10권2호
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• pp.144-153
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• 1990

Ductile cast iron has good ductility and toughness, for the graphite morphology is spheroidal. It has been reported that the strengthening and toughening of the ductile cast iron was resulted from the modification of matrix structure by the heat treatment or the addition of alloying elements. In this study, effects of various special heat treatments (cyclic heat treatment and intermediate heat treatment) and Ni addition on the toughness and strength of the austempered ductile cast iron were studied. The results obtained from this study were as follows : 1. The amount of fine pearlite was increased with the Ni content and the number of cycle in cyclic heat treatment. 2. When the specimens treated and not by special heat treatment at 820 was austempered, in the former the austenite was formed on grain boundary entirely, but in the latter on grain boundary partially. 3. The impact energy was decreased with the Ni content, because the coarisen austenite pools formed with the Ni content was transformed into martensite during quenching. 4. The mechanical properties of austempered ductile cast iron containing 2%Ni treated cyclic heat treatment(5 cycles)was very excellent in handness 99(HRB), impact energy 12(kg-m) maximum fracture load 1500(kg-f).

• 한국주조공학회지
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• 제9권6호
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• pp.463-473
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• 1989

This study is aimed to investigate the effect of cyclic heat treatment which is special heat treatment on the strength and toughness in Multi-phase(Ferrite-Bainite-Martensite) Ductile cast Irons. Spceimens were austenitized at eutectoid transformation temperature range(${\alpha}+{\gamma}$) for 30min and austempered at $300^{\circ}C$ and $400^{\circ}C$ for different holding times, and then quenched in ice water to obtain the multi-phase(Ferrite-Bainite-Martensite) structure from various prior structures, which was obtained by various cyclic heat treatments. As the number of cycle in cyclic heat treatment increased, volume fraction of pearlite increased and the its morphology was refined. As the number of cycle in cyclic heat treatment increased, the multi-phase(Ferrite-Bainite-Martensite) was dispersed in whole matrix as refined island phase. Particularly, martensite among the multi-phase gradually became a spherical shape. Good combination in impact energy and tensile strength was detained in $840^{\circ}C-300^{\circ}C-15min$ condition after 10 cycles in cyclic heat treatment, and its multi-phase volume fraction is Ferrite(50%)-Martensite(l3%)-Bainite(37%).

• Progress in Superconductivity
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• 제9권1호
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• pp.115-118
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• 2007

This study investigated the effects of different kinds of seed crystals with miscut angles and pretreatment on the characteristics of a RE-123 superconductor processed by a top-seeded melt-growth (TSMG) method. When the seed crystal was heat-treated in an oxygen atmosphere, the surface structure was cleaned removing hydroxide. When the seed crystal had a miscut angle, in addition, the surface structure showed a well defined hill-and-valley structure after heat-treatment. A better microstructure, with a well-distributed small RE-123 phase, was obtained using a high miscut angle after heat-treatment in an oxygen atmosphere. As a result of the microstructure improvement, the magnetic characteristics also improved. The experimental result can be explained by reduction of nucleation activation energy.

• 열처리공학회지
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• 제7권1호
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• pp.11-16
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• 1994

Anatase $TiO_2$ particles prepared by experiment were used to study the change of crystal structure by calcination temperature. The results were as follows. Crystallite size of anatase $TiO_2$ particles increased with calcination temperature. The rate of increasing the crystallite size of anatase $TiO_2$ particles was decreased below $700^{\circ}C$ and was markedly increased above $700^{\circ}C$. Unit cell volume of $TiO_2$ was expanded at low temperature and was contracted at high temperature. This result means that the growth of crystallite size was occured in the direction.