• Journal of the Korean Society for Heat Treatment
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• v.16 no.5
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• pp.267-274
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• 2003

The effect of the thermo-mechanical treatment on the microstructural development and the electric conductivity of Cu-Ca alloys are studied for the thixoforming processed rotor of the induction motor The Cu-Ca alloys containing Ca less than 1.0wt% show the electrical conductivity higher than 80% IACS They also show broad melting range over $150^{\circ}C$ which is desirable for the thixoforming process The semi-solid microstructure of cast alloy changes from the dendrite structure to globular structure by prior deformation before reheating. The details of microstructural changes by the thermo-mechanical treatment are discussed.

• Korean Journal of Materials Research
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• v.9 no.4
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• pp.386-391
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• 1999

The charge-discharge, the high-rate dischargeability, and the self discharge characteristics of the electrodes composed of rapidly solidified ZrV\ulcornerMn\ulcornerMo\ulcornerNi\ulcorneralloy, which has the form of partial substitution of Mn, Mo, Ni for V in $ZrV_2$ were studied. The alloys were prepared using Arc & RSP(Rapid Solidification Process) at the rotating roller speed of 2000 and 5000 rpm. Some of them were received heat treatment at$ 560 ^{\circ}C$ for 1 hour after the solidification to investigate the effect of the heat treatment. It was fond that cycle life was significantly improved by RSP, whereas discharge capacity, activation rte and high rate dischargeability were decreased compared with the conventional arc melting method. The capacity loss seems to be due to the loss of the crystallinity and the increase of the cycle life ascribed to the presence of the amporphous phase as well as the refined grain size of less than 0.2$\mu\textrm{m}$. Heat treatment of the alloy cooled at 2000 rpm improved the cycle life. In case of the alloys cooled at 5000 rpm, both the discharge capacity and the activation rate were significantly improved by the heat treatment.

• International Journal of Automotive Technology
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• v.7 no.1
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• pp.69-74
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• 2006

Residual stresses are introduced in aluminum cylinder head during quenching at the end of the T6 heat treatment process. Tensile residual stress resulted from quenching is detrimental to fatigue behavior of a cylinder head when it is overlapped with stresses of engine operation load. Quenching simulation has been performed to assess the distribution of residual stress in the cylinder head. Analysis revealed that in-homogeneous temperature distribution led to high tensile residual stress at the foot of the long intake port, where high stresses of engine operation load are expected. Measurements of residual stress have been followed and compared with the calculated results. Results successfully proved that high tensile residual stress, which was large enough to accelerate fatigue failure of the cylinder head, are formed during quenching process at the end of heat treatment at the same critical position. Effect of quenching parameters on the distribution of residual stress in cylinder head has been investigated by choosing different combination of heat treatment parameters. It was demonstrated that changes of quenching parameters led to more homogeneous temperature distribution during cooling and could reduce tensile residual stress at the critical region of the cylinder head used in this study.

• Journal of the Korean Applied Science and Technology
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• v.27 no.3
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• pp.282-289
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• 2010

In preparation of silica aerogel-based hybrid coating materials, the combination of hydrophobic aerogel with organic polar binder material is shown to be very limited due to dissimilar surface property between two materials. Accordingly, the surface modification of the aerogel would be required to obtain compatibilized hybrid coating sols with homogeneous dispersion. In this study, the surface of silica aerogel particles was modified by using both surfactant adsorption and heat treatment methods. Four types of surfactants with different molecular weights and HLB values were used to examine the effect of chain length and hydrophilicity. The surface property of the modified aerogel was evaluated in terms of visible observation for aerogel dispersion in water, water contact angle measurement, and FT-IR analysis. In surface modification using surfactants, the effects of surfactant type and content, and mixing time as process parameter on the degree of hydrophilicity for the modified aerogel. In addition, the temperature condition in modification process via heat treatment was revealed to be significant factor to prepare aerogel with highly hydrophilic property.

• Journal of the Korean Society for Heat Treatment
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• v.19 no.3
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• pp.141-148
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• 2006

An experimental study is presented for water droplet impingement on a steel surface in the process of heat treatment. The objective of the present work is to examine characteristic of evaporation cooling due to surface roughness and droplet diameter under conductive heat input condition. The surface temperatures varied from $80{\sim}155^{\circ}C$, surface roughness was from $R_a=0.12{\mu}m$ to $R_a=1.14{\mu}m$ and droplet diameter was from 2.4 mm to 3.0 mm. The results show that the total evaporation time is shorter for the larger surface roughness and the smaller droplet size, the time average heat flux has maximum value for the larger surface roughness and the smaller droplet size. The total evaporation time has not influence on the nuclear boiling region.

• Transactions of Materials Processing
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• v.11 no.3
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• pp.211-216
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• 2002

The mechanical and thermal load, and thermal softening occuring by the rush temperature of die, in warm and hot forging, cause wear, heat cracking and plastic deformation, etc. This paper describes the effects of solid lubricants and surface treatments for warm forging die. Because cooling effect and low friction are essential to the long life of dies, optimal surface treatments and lubricants are very important to hot and warm forging process. The main factors affecting die hardness and heat transfer, are surface treatments and lubricants, which are related to heat transfer coefficient, etc. To verify the effects, experiments are performed for heat transfer coefficient in various conditions - different initial billet temperatures and different loads. Carbonitriding and ionitriding are used as surface treatments, and oil-base and water-base graphite lubricants are used. The effects of lubricant and surface treatment for warm and hot forging die life are explained by their thermal characteristics, and the new developed technique in this study for predicting tool life can give more feasible means to improve the tool life in hot forging process.

• Journal of the Korean Society for Heat Treatment
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• v.2 no.2
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• pp.17-26
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• 1989

This study has been performed to investigate into some effects of the Sursulf treatment time and the traveling speed of surface hardening treatment on the hardness and the wear characteristics by applying the combined heat treating techniques of Sursulf process followed by induction hardening treatment to mild steel. It has been shown that increasing the Sursulf treatment time increases the case depth, but both hardness and wear resistance are not considerably improved. When the combined heat treating technique of high frequency induction heating after Sursulf treatment is applied, an improvement in case depth as well as wear resistance is obtained. In particular, the hardness in diffusion zone is greatly increased due mainly to the formation of martensite and possibly lower bainite. Iron oxides formed during induction heating and subsequent water spray cooling in the outermost part of compound layer may be considered to cause some increases in hardness and wear resistance.

• Journal of the Korean Society for Heat Treatment
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• v.8 no.3
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• pp.213-221
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• 1995

Temperature distribution, transformation and residual stresses generated during the quenching process of carbon steel. It follows many difficulties in the analytical considerations on those quenching process because of the coupling effects on temperature and metallic structures. In this paper one of the basic study on the quenching stresses was carried out for the case of the round steel bar specimen(SM45C) with 40mm both in its diameter and length. The temperature distributions considering strain hysteresis were numerically calculated by finite element technique. In calculating the transient temperature field, the heat flux between water and rod surface was determined from the heat transfer coefficient. The gradient of temperature is almost same to geometric of specimen. At early stage of the quenching process, the abrupt temperature gradient has been shown in the surface of the specimen.

• Corrosion Science and Technology
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• v.22 no.5
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• pp.359-367
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• 2023

The localized corrosion resistance of the Ni-based Inconel 718 alloy after solution heat treatment was evaluated using electrochemical techniques in a solution of 25 wt% NaCl and 0.5 wt% acetic acid. Solution heat treatment at 1050 ℃ for 2.5 hours resulted in an increased average grain diameter. Both Ti carbides (10 ㎛ diameter) and Nb-Mo carbides (1 - 9 ㎛ diameter) were distributed throughout the material. Despite heat treatment, the shape and composition of these carbides remained consistent. An increase in solution temperature led to a decrease in pitting potential value. However, the pitting potential value of solution heat-treated Inconel 718 was consistently higher than that of as-received Inconel 718 at all tested temperatures. Localized corrosion initiation occurred at 0.4 V_SSE in a temperature environment of 80 ℃ for both as-received and solution heat-treated Inconel 718 alloys. X-ray photoelectron spectroscopic analysis indicated that the composition of the passive film formed on specimen surfaces remained largely unchanged after solution heat treatment, with O1s, Cr2p_3/2, Fe2p_3/2, and Ni2p_3/2 present. The difference in localized corrosion resistance between as-received and solution heat-treated Inconel 718 alloys was attributable to microstructural changes induced by the heat treatment process.

• Journal of the Korean Society for Precision Engineering
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• v.10 no.2
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• pp.66-75
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• 1993

This paper proposes a monitoring method for nondestructive and in-process measurement of the case depth in LASER surface heat treatment process. The method is essentially an eddy-current method, and measures sensing coil's electrical impedance which varies with the changes of the material microstructure due to hardening. To investigate te validity of the proposed method a series of experiments were performed for various hardning depths. The results show that the relationship between the eddy- current sensor output and the changes in case depth is almost linear. This indicates that the eddy-current measuring method can be used as one of the possible monitoring method for mesauring the hardened depth in LASER heat treatment processes.