• 분석과학
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• 제6권2호
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• pp.217-223
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• 1993

저항가열식 진공중착기를 이용하여 실온(ambient temp.)과 $250^{\circ}C$에서 알루미나 기판 위에 Au/Cr, Au/Ni/Cr 및 Au/Pd/Cr 박막을 제조하였으며, 공기 중에서 $300^{\circ}C$, $450^{\circ}C$, $600^{\circ}C$의 온도로 각각 1시간 동안 열처리하였다. Au, Ni(또는 Pd) 및 Cr 박막의 두께는 각각 $1000{\AA}$, $300{\AA}$, 및 $50{\AA}$이었다. 박막 제조시 기판의 온도와 박막 제조 후 열처리 온도는 각 층의 상호확산으로 인하여 박막의 면저항값에 영향을 주었다. Auger depth profile 분석결과, Au/Cr 시스템에서는 기판의 온도는 $250^{\circ}C$로 하여 박막을 제조할 때 이미 Cr은 Au 표면으로 확산되었으며, 열처리 후에는 Au의 분포도만 변화하였다. Au/Ni/Cr과 Au/Pd/Cr 시스템의 경우 Ni와 Pd 모두 확산현상이 발견되었으며, 특히 Ni(약 45 at.%)는 Au 박막 표면으로 확산되어 산화되었다.

• 한국분말재료학회지
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• 제24권5호
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• pp.406-413
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• 2017

A Nanosized $WO_3$ and CuO powder mixture is prepared using novel high-energy ball milling in a bead mill to obtain a W-Cu nanocomposite powder, and the effect of milling time on the structural characteristics of $WO_3-CuO$ powder mixtures is investigated. The results show that the ball-milled $WO_3-CuO$ powder mixture reaches at steady state after 10 h milling, characterized by the uniform and narrow particle size distribution with primary crystalline sizes below 50 nm, a specific surface area of $37m^2/g$, and powder mean particle size ($D_{50}$) of $0.57{\mu}m$. The $WO_3-CuO$ powder mixtures milled for 10 h are heat-treated at different temperatures in $H_2$ atmosphere to produce W-Cu powder. The XRD results shows that both the $WO_3$ and CuO phases can be reduced to W and Cu phases at temperatures over $700^{\circ}C$. The reduced W-Cu nanocomposite powder exhibits excellent sinterability, and the ultrafine W-Cu composite can be obtained by the Cu liquid phase sintering process.

• 센서학회지
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• 제9권1호
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• pp.44-50
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• 2000

적외선 센서는 대상 물체의 열 분포를 감지할 수 있고, 그것으로부터 얻은 영상은 물체 내부의 결함과 그 물체표면의 이물질 등의 효과가 모두 포함된 상태이므로 적외선 열 화상 자체만으로는 비정상적인 부분들을 찾아내기 어렵다. 따라서 본 논문에서는 적외선 센서로부터 얻은 영상을 가시화 하는 방법으로 가시광선 영상과의 중첩방법을 제시한다. 이를 위해서 평행이동 관계에 있는 두 가시광선 영상으로부터 열 화상에 대응하는 보간 영상을 생성하고, 이것을 적외선 센서에 의해 감지된 온도를 매핑한 열 화상과 중첩시킨다. 본 논문에서 제안한 가시화 기법은 적외선 센서의 특성을 최대한 고려할 수 있기 때문에 재해방지를 위한 비파괴 검사 등에 쓰여질 수 있다.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2018년도 춘계학술대회 논문집
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• pp.54-54
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• 2018

To optimize the deposition parameters of diamond films, the temperature, pressure, and distance between the filament and the susceptor need to be considered. However, it is difficult to precisely measure and predict the filament and susceptor temperature in relation to the applied power in the hot filament chemical vapor deposition (HFCVD) system. In this study the temperature distribution inside the system was numerically calculated for the applied powers of 12, 14, 16 and 18 kW. The applied power needed to achieve the appropriate temperature at a constant pressure and other conditions was deduced, and applied to actual experimental depositions. The numerical simulation was conducted using the commercial computational fluent dynamics software, ANSYS-FLUENT. To account for radiative heat-transfer in the HFCVD reactor, the discrete ordinate (DO) model was used. The temperatures of the filament surface and the susceptor at different power levels were predicted to be 2512 ~ 2802 K, and 1076 ~ 1198 K, respectively. Based on the numerical calculations, experiments were performed. The simulated temperatures for the filament surface were in good agreement with experimental temperatures measured using a 2-color pyrometer. The results showed that the highest deposition rate and the lowest deposition of non-diamond was obtained at a power of 16 kW.

• 대한공간정보학회지
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• 제19권2호
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• pp.55-61
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• 2011

토지이용이 인위적으로 이뤄져오면서 시외지역이나 공원지역에 비하여 도시지역의 온도가 상승하는 원인이 되어 왔다. 따라서 본 연구에서는 진주시를 대상으로 도시지역의 용도지역에 따른 온도변화를 Landsat TM/$ETM^+$ 영상을 이용하여 분석하였고, 정규식생지수와 온도변화와의 상관관계를 분석하는데 연구목적을 두었다. 그 결과 도시 표면온도의 분포가 용도지역별 정규식생지수(NDVI)값의 변화에 연계되어 있음을 알 수 있었다. 용도지역별 평균 온도를 고려하면 용도지역 중 공업지역이 가장 높은 반면 녹지지역은 가장 낮게 나타났다. 또한 도시온도와 정규식생지수와의 상관관계를 비교분석한 결과 녹지지역과 주거지역이 상업지역과 공업지역에 비해 높게 나타났으며, 이러한 연구결과는 도시열섬효과문제를 고려한 지속 가능한 도시계획을 수립하는데 중요한 요소로 활용될 것으로 기대된다.

• 한국자동차공학회논문집
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• 제14권1호
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• pp.68-78
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• 2006

In the past few years, considerable efforts have been directed towards the further development of Urea-SCR(selective catalytic reduction) technique for diesel-driven vehicle. Although urea possesses considerable advantages over Ammonia$(NH_3)$ in terms of toxicity and handling, its necessary decomposition into Ammonia and carbon dioxide complicates the DeNOx process. Moreover, a mobile SCR system has only a short distance between engine exhaust and the catalyst entrance. Hence, this leads to not enough residence times of urea, and therefore evaporation and thermolysis cannot be completed at the catalyst entrance. This may cause high secondary emissions of Ammonia and isocyanic acid from the reducing agent and also leads to the fact that a considerable section of the catalyst may be misused for the purely thermal steps of water evaporation and thermolysis of urea. Hence the key factor to implementation of SCR technology on automobile is fast thermolysis, good mixing of Ammonia and gas, and reducing Ammonia slip. In this context, this study performs three-dimensional numerical simulation of urea injection of heavy-duty diesel engine under various injection pressure, injector locations and number of injector hole. This study employs Eulerian-Lagrangian approach to consider break-up, evaporation and heat and mass-transfer between droplet and exhaust gas with considering thermolysis and the turbulence dispersion effect of droplet. The SCR-monolith brick has been treated as porous medium. The effect of location and number of hole of urea injector on the uniformity of Ammonia concentration distribution and the amount of water at the entrance of SCR-monolith has been examined in detail under various injection pressures. The present results show useful guidelines for the optimum design of urea injector for reducing Ammonia slip and improving DeNOx performance.

• Journal of Microbiology and Biotechnology
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• 제2권2호
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• pp.85-91
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• 1992

The intestinal microflora of humans is an extraordinarily complex mixture of microorganisms, the majority of which are anaerobic microorganisms. The distribution of amylolytic microorganisms in the human large intestinal tract was investigated in various individuals of differing ages using anaerobic culture techniques. A large percentage of the amylolytic microorganisms present belonged to the Genus Bifidobacteria. The number of Bifidobacteria increased significantly at two years of age. Adults and children above 2 years old carried about $0.8{\times}10^9-2.0{\times}10^{10}$ colony forming units (CFU/gram) of amylolytic Bifidobacteria. Among these amylolytic Bifidobacteria, Int-57 was chosen for further studies. Between 65% and 85% of the amylase produced was secreted and the remaining amylase was bound to the cell wall facing the outside. Amylase production could be induced by starch in a stable form. When cells were grown on maltose or glucose, amylase production was much lower than on starch and amylase activity disappeared after 24 hours growth on these media. Partially purified enzymes showed optimum activity at a temperature of $50^{\circ}C$ and at an optimum pH of 5.5, respectively. Heat treatment at $70^{\circ}C$ for 30 minutes almost completely inactivated amylase. The hydrolysis products of starch were mainly maltose and maltotriose. Soluble starch, amylose, amylopectin, and $\gamma$-cyclodextrin($\gamma$-CD) were easily hydrolyzed. The rate of hydrolysis of $\alpha$-CD and $\beta$-CD was slower than that of $\gamma$-CD. Carboxymethyl cellulose, $\beta$-1, 3-glucan and inulin were not hydrolyzed.

• 한국식품과학회지
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• 제18권1호
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• pp.61-65
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• 1986

홍옥(紅玉)을 시료(試料)로 하여 건조조건(乾燥條件)을 다르게하여 건조특성(乾燥特性), 수분이동현상(水分移動現像), 건조중(乾燥中) 시료온도(試料溫度) 및 내부수분(內部水分)의 분포(分布)를 조사하였다. 사과의 수분확산계수(水分擴散係數)는 $1.1470{\sim}2.2148{\times}10^{-5}cm^2/sec$, 확산활성화(擴散活性化)에너지는 6.6 kcal/g mole 이었으며 Fick's law에서 아래의 식을 유도할 수 있었다. $${\In}\;{\Delta}t=In\;{\Delta}to-{\frac{D{\pi}^2{\theta}}{4d^2}}$$ 건조중(乾燥中) 내부수분분포(內部水分分布)의 이론치(理論値)와 실측치(實測値)는 거의 일치하였다.

• 한국식품과학회지
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• 제21권1호
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• pp.52-57
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• 1989

보리 전분입을 구성하는 대입자와 소입자의 물리, 화학적 차이에 관해서 비교하였다. 대입자의 직경은 약 $28-30{\mu}m$이고. 소입자는 약 $6{\mu}m$ 이었으며, Hiproly 전분 입자의 수에 대한 소입자의 수는 95%정도 이었다. 아밀로오즈의 함량은 대입자가 소입자 보다 높게 나타났다. 아밀로오즈의 분자 형태에 관한 대입자 소입자 전분의 고찰로써, iso-amylase처리 전분의 구성성분의 차이, X선 회절도의 차이, 호화특성, 산분해성 등의 검토에 의하면, 아밀로펙틴의 미세결정 구조인 망상구조상에 있어서 대입자와 소입자가 서로 다른 구조를 하고 있으리라 예측된다.

• Carbon letters
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• 제1권2호
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• pp.69-75
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• 2000

Naphtha cracking bottom oil was reformed with heat treatment and then spun at $310^{\circ}C$. These pitch-based carbon fibers were carbonized at $1000^{\circ}C$ after oxidation at $280^{\circ}C$, for 90 min. These fibers were chemically activated with molar ratio of KOH/CF (1 : 1) at different temperatures ($250{\sim}900^{\circ}C$) for 1 hr. The process of activation was characterized with DTA, TGA, BET surface area and pore size distribution. The activation of fibers by KOH was performed by several process. One is the reduction process that carbon fiber was reacted with $K_2O$ produced from dehydration process above $400^{\circ}C$. The other is the process that $K_2CO_3$ was directly reacted with carbon fiber. At $800^{\circ}C$, the activation was performed by catalyzed mechanism that $K_2O$ was obtained from the reaction of metal potassium with $CO_2$, then was changed to $K_2CO_3$. At $870^{\circ}C$, the activation was also observed that activation mechanism was promoted by metal catalyst with $CO_2$ from decomposition of $K_2CO_3$. The specific surface area of prepared activated carbon fibers was dependent on the activation mechanism. The specific surface area was in the range of $1519{\sim}2000\;cm^3/g$ and was the largest prepared at $870^{\circ}C$. The pores developed were mostly micropores which was very narrow and uniform. The total pore volume was $0.58{\sim}0.77\;cm^3/g$.