• 한국세라믹학회지
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• 제31권11호
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• pp.1315-1322
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• 1994

In this study, stable PbTiO3 coating solution was prepared using diethanolamine(DEA) complexing agent and deposited on indium-tin oxide(ITO) coated glass substrate. Prepared thin films were dense and crack-free. Perovskite-type PbTiO3 thin films could be obtained above 50$0^{\circ}C$, while the films heat-treated above $650^{\circ}C$ showed undesired properties due to interface reactions between films and substrates and warpage phenomena of substrates. Measured maximum dielectric constant and loss tangent were found to be 144 and 0.0163 at 1 kHz, 55$0^{\circ}C$ heat-treatment, respectively.

• 한국세라믹학회지
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• 제27권7호
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• pp.907-915
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• 1990

The hydroxyapatite powder was prepared by the precipitation method. The obtained powder was heat-treated and its products were investigated in order to characterize its decomposition process. The powder was Ca-deficient hydroxyapatite with no relation to the Ca/P mole ratio in the initial solution. The obtained hydroxyapatite was thermally decomposed into tricalcium phosphate [Ca3(PO4)2, TCP] after heat-treatment above 80$0^{\circ}C$ and the extent of the decomposition was dependent on the nonstoichiometry of obtained hydroxyapatite, and the resultant hydroxyapatite and tricalcium phosphate maintained stable forms up to 120$0^{\circ}C$. The hydroxyapatite powder had the better stability with the samller the nonstoichinometry of hydroxyapatite. And the quantities of tricalcium phosphate obtained after decomposition were decreased, and also the corresponding decomposition temperatures were increased with decreasing extent of nonstoichiometry in precipitated hydroxyapatite.

• BMB Reports
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• 제28권1호
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• pp.62-67
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• 1995

Thioredoxin f from pea leaves was purified to homogeneity and characterized. The purification steps involved ammonium sulfate fractionation, heat treatment, Sephadex G-75 and G-50 gel filtration, and hydroxyapatite and DEAE ion exchange chromatography. The monomeric molecular weight of purified pea thioredoxin f determined by SDS polyacrylamide gel electrophoresis was 12,000. The purified protein was active in the presence of reducing agents, such as dithiothreitol, at an alkaline pH (7.8~8.5). It was stable against heat such that more than 40% of its maximum activity remained after treatment at $90^{\circ}C$ for 10 min. Pea thioredoxin f was able to reduce insulin and was specific only to pea chloroplast fructose-1,6-bisphosphatase.

• Journal of Mechanical Science and Technology
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• 제16권5호
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• pp.710-719
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• 2002

This study investigates a nonlinear inverse convection problem for a laminar-forced convective flow between two parallel plates. The upper plate is exposed to unknown heat flux while the lower plate is insulated. The unknown heat flux is determined using temperature measured on the lower plate. The thermophysical properties of the fluid are temperature dependent, which renders the problem nonlinear. The sequential gradient method is applied to this nonlinear inverse problem in order to solve the problem efficiently. The function specification method is incorporated to stabilize the sequential estimation. The corresponding adjoint formalism is provided. Accuracy and stability have been examined for the proposed method with test cases. The tendency of deterministic error is investigated for several parameters. Stable solutions are achieved eve]1 with severely impaired measurement data.

• 제어로봇시스템학회:학술대회논문집
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• 제어로봇시스템학회 1990년도 한국자동제어학술회의논문집(국제학술편); KOEX, Seoul; 26-27 Oct. 1990
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• pp.1284-1288
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• 1990

In this paper, we are going to study the stabilization of the semilinear heat equation with inhomogenous boundary conditions, whose solutions are not (in general) stable. Here, we use the discrete-time feedback inputs through the boundary of geometric domain to the semilinear system under some additional conditions and assumptions. It is shown that under these conditions, the stabilization can be realized by applying pole assignment argument to the principal linear part of the system and that the solutions exist globally in discrete-time t without any finite escape time.

• 한국원자력학회:학술대회논문집
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• 한국원자력학회 1996년도 추계학술발표회논문집(1)
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• pp.224-229
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• 1996

An experimental study on critical heat flux (CHF) and two-phase flow visualization has been performed for water flow in internally-heated, vertical, concentric annuli under near atmospheric pressure. Tests have been done under stable forced- circulation, upward and downward flow conditions with three test sections of relatively large gap widths (heated length = 0.6 m. inner diameter = 19 mm, outer diameter = 29, 35 and 51 mm). The outer wall of the test section was made up of the transparent Pyrex tube to allow the observation of flow patterns near the CHF occurrence. The CHF mechanism was changed in the order of flooding, chum-to-annular flow transition, and local dryout under a large bubble in churn flow as the flow rate was increased from zero to higher values. Observed parametric trends are consistent with the previous understanding except that the CHF for downward flow is considerably lower than that for upward flow.

• 한국원자력학회:학술대회논문집
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• 한국원자력학회 1996년도 추계학술발표회논문집(1)
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• pp.242-247
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• 1996

Flow oscillations in boiling channels induces a drastic reduction of the (critical heat flux) CHF or premature burnout. However, most of CHF works and correlations have been focused on stable flow conditions without considering flow oscillation. Therefore to improve the understanding on flow oscillation CHF, in this paper a new CHF correction factor to predict the CHF values under flow oscillation conditions has been developed from 126 experimental data. Also to investigate the dominant factor on flow oscillation CHF parametric trends are analyzed by using the developed correction factor. The overall mean accuracy ratio of the developed correction factor is 1.033 with a standard deviation of 0.195. The RMS errors 0.198. Its assessment shows that the predictions agree well with the experimental data within 25% error bounds.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 1997년도 특별강연 및 추계학술발표 개요집
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• pp.81-85
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• 1997

This paper was conducted the fatigue crack growth test on the base metal and weld joint of bimaterial(carbon-stainless steel), carbon steel and stainless steel. As the result, the fatigue crack growth rate of weld joint on the stainless-stainless steel is faster than stainless base metal, and weld joint on the carbon-carbon steel heat affected zone is slower than carbon base metal. And fatigue crack growth rate of carbon-stainless steel weld joint and heat affected zone is similar to the behavior of stainless base metal. In conclusion, weld joint of bimaterial is stable in the fatigue crack growth behavior.

• 한국표면공학회지
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• 제28권6호
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• pp.376-385
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• 1995

Copper-chromium multilayers with a nominal bilayer thickness of about 400 $\AA$ (200 $\AA$ each) were prepared by dc magnetron sputtering and the evolution of microstructure during heat treatment was investigated by using x-ray diffractometry(XRD), Auger electron spectroscopy(AES) and transmission electron microscopy(TEM). It was observed that an amorphous phase with a thickness of about 40 $\AA$ was formed at the interfaces of the as-deposited Cu/Cr multilayered film using cross-sectional TEM. At elevated temperatures, the Cu(111) reflection showed increasing intensity and decreasing line-width as a result of copper grain growth. The intermixed amorphous phase disappeared after annealing at $250^{\circ}C$ for 1 h and the multilayer structure was stable up to $400^{\circ}C$ for 1 h annealing. At $600^{\circ}C$ annealing, it was observed that the multilayer structure was completely destroyed and copper and chromium phases were fully intermixed.

• 한국분말재료학회지
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• 제9권1호
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• pp.32-37
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• 2002

In the present study of IGC (Inert Gas Condensation) evaporation-condensation processing study, the effects of IGC convection gas on the crystallographic structure, size and shape of tin oxide nanoparticles were investigated. In addition, the phase transformation of tin oxide nanoparticles was studied after heat treatment. IGC processing was conducted at 1000℃ for 1 hr. The mixture gas of oxygen and helium was used as a convection gas. Metastable tetragonal SnO nanoparticles were obtained at a lower convection gas pressure, whereas amorphous tin oxide nanoparticles were obtained at a higher one. The formation of amorphous phase could be explained by the rapid quenching of the vaporized atoms. The resultant nanoparticles size was about 10 nm with a rounded shape. The tin oxide nanoparticles prepared by IGC were almost transformed to the stable tetragonal SnO₂ after heat treatment.