• Macromolecular Research
• /
• v.12 no.4
• /
• pp.399-406
• /
• 2004

Glass-like carbon precursors shrink significantly during curing and carbonization, which leads to crack formation and bending. Cured furan resin powder and ethanol were added to furan resin to diminish the weight loss, to suppress the shrinkage and bending, and to readily release the gases evolved during polymerization and curing. Curing and carbonization were controlled by pressure and slow heating to avoid damage to the samples. The effect of the filler and ethanol on the fabrication process was examined by measuring the properties of the glass-like carbon, such as the specific gravity, bending strength, electrical resistivity, and microstructural change. The specific gravities of the filler-added glass-like carbons were higher than those of the ethanol-added samples because of the formation of macropores from the vaporization of ethanol during the curing and polymerization processes. Although the ethanol-added glass-like carbons exhibited lower bending strengths after carbonization than did the filler-added samples, the opposite result was observed after aging at 2,600$^{\circ}C$. We found that the macropores created from ethanol were contracted and removed upon heat treatment. The electrical resistivity of the glass-like carbon aged at 2,600$^{\circ}C$ was lower than those of the samples carbonized at 1,000$^{\circ}C$. We attribute this phenomenon to the fact that aging at high temperature led to well-developed microstructures, the removal of macropores, and the reduction of the surface area.

• Bulletin of the Korean Chemical Society
• /
• v.35 no.2
• /
• pp.357-364
• /
• 2014

Size controlled, $LiNi_{0.8}Co_{0.15}Al_{0.05}O_2$ cathode powders were prepared by co-precipitation method followed by heat treatment at temperatures between 750 and $850^{\circ}C$. The synthesized samples are characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and electrochemical performance. The synthesized $LiNi_{0.8}Co_{0.15}Al_{0.05}O_2$ after calcined at $750^{\circ}C$ has a good electrochemical performance with an initial discharge capacity of $190mAhg^{-1}$ and good capacity retention of 100% after 30 cycles at 0.1C ($17mAg^{-1}$). The capacity retention of $LiNi_{0.8}Co_{0.15}Al_{0.05}O_2$ after calcined at $750^{\circ}C$ is better than that at 800 and $850^{\circ}C$ without capacity loss at various high C rates. This is ascribed to the minimized cation disorder, a higher conductivity, and higher lithium ion diffusion coefficient ($D_{Li}$) observed in this material. In the differential scanning calorimetry DSC profile of the charged sample, the generation of heat by exothermic reaction was decreased by calcined at high temperature, and this decrease is especially at $850^{\circ}C$. This behavior implies that the high temperature calcinations of $LiNi_{0.8}Co_{0.15}Al_{0.05}O_2$ prevent phase transitions with the release of oxygen.

• International Journal of Internet, Broadcasting and Communication
• /
• v.13 no.2
• /
• pp.145-155
• /
• 2021

With the recent rapid improvement in the standards of life and westernization of dietary lifestyles, the consumption of high-calorie diets such as high-fat and high-protein red meat and instant foods has increased, while less vegetables containing dietary fiber are consumed. In addition to that, stress, erroneous dietary behaviors, and contaminated environments are linked to the risk of developing ulcerative colitis, which is on the rise. Another cause of ulcerative colitis is that involve laxative abuse, including repeated, frequent use of laxatives, and include such conditions as deteriorated bowel function, irritable bowel syndrome, diarrhea, intestinal inflammation, etc. The present study aimed to investigate the comparative evaluation of pharmacological efficacy between sulfasalazine alone and combination with herbal medicine on dextran sodium sulfate (DSS)-induced UC in mice. Balb/c mice received 5% DSS in drinking water for 7 days to induce colitis. Animals were divided into five groups (n = 9): group I-normal group, group II-DSS control group, group III-DSS + sulfasalazine (30 mg/kg), group IV-DSS + sulfasalazine (60 mg/kg), group V-DSS + sulfasalazine (30 mg/kg) + Radish Extract mixture (30 mg /kg) (SRE). DSS-treated mice developed symptoms similar to those of human UC, such as severe bloody diarrhea and weight loss. SRE supplementation, as well as sulfasalazine, suppressed colonic length and mucosal inflammatory infiltration. In addition, SRE treatment significantly reduced the expression of pro-inflammatory signaling molecules through suppression both mitogen-activated protein kinases (MAPK) and nuclear factor-kappa B (NF-κB) signaling pathways, and prevented the apoptosis of colon. Moreover, SRE administration significantly led to the up-regulation of antioxidant enzyme including SOD and Catalase. This is the first report that Radish extract mixture combined with sulfasalazine protects against experimental UC via the inhibition of both inflammation and apoptosis, very similar to the standard-of-care sulfasalazine.

• Journal of Periodontal and Implant Science
• /
• v.29 no.2
• /
• pp.311-326
• /
• 1999

This study was investigated to observe the effect of Treponema denticola(TDC) and Treponema lecithinolyticum(TLC) on cultured human periodontal ligament cells. Several experiments were performed including MTT test for the inhibition effect of cell proliferation, LDH test for the cytotoxicity , gelatin zymography for the gelatinase activation and observation of cell morphology change using the phase-contrast microscopy. The results were as follows. 1. The effect of concentration on cell proliferation with time showed an inhibitory effect at high concentration $(150{\mu}g/well)$ for TLC and at low concentration( $9.4{\mu}gwell$ ) for TDC. 2. The effect of time on cell proliferation with concentration showed an inhibitory effect at $150{\mu}g/well$ on 2-day incubation for TLC and at $9.4{\mu}g/well$ on 2-day incubation for TDC. 3. The effect of heat-treated TDC and TLC on the inhibition of cell proliferation showed the difference in the heat-treated group compared to the non-heat treated group for TDC, whereas no difference was found for TLC. 4. The morphological changes which were observed from the phase-contrast microscopy showed the difference in the test group compared to the control group. The loss of spindle-like appearance, cell-to-cell detachment and inhibition of cell proliferation were observed. 5. There was no difference of the cytotoxicity effect between the test group and the control group in the LDH test. 6. The active form of progelatinase A with molecular weight 72kDa was activated in both TDC and TLC on the gelatin zymography. Regarding to the above results, TDC and TLC have an effect on periodontal ligament cells by playing an inhibitory role in cell proliferation and appears to activate progelatinase A which degrades type IV collagen.

• Journal of the Korean Ceramic Society
• /
• v.39 no.2
• /
• pp.178-183
• /
• 2002

Zinc fluosilicate ($ZnSiF_6$, 15% aqueous solution) was prepared using zinc oxide (ZnO) and fluosilicic acid ($H_2SiF_6$) by soluiton synthetic method. The fluidity and hydration properties of cement which was added $ZnSiF_6$ (aq.) as an additive for cement were studied. At water to cement ratio (W/C) equals to 0.45, the initial fluidity and slump loss of cement paste which the addition of $ZnSiF_6$ (aq.) was increased from 1.0% to 4.0% based on cement weight were investigated. Initial fluidity of cement paste was measured by mini-slump test and slump loss was examined by measuring the fluidity variation of cement paste with time elapsed from 0 min to 120 min at intervals 30 min. Also, the effect of $ZnSiF_6$ addition on the setting and hydration of cement paste when $ZnSiF_6$ increased in the addition range 1.0% to 3.0% were investigated. The fluidity of cement paste which was added 2.1% $ZnSiF_6$ (aq.) presented the highest value among all addition ranges. The setting time of cement paste was retarded gradually and the heat evolution of hydrated cement was reduced with the increasing of $ZnSiF_6$ addition.

• KSBB Journal
• /
• v.4 no.1
• /
• pp.40-47
• /
• 1989

Changes of principal components of crude green tea were determined after 30 min. of heat treatment at 10$0^{\circ}C$, l15$^{\circ}C$, 14$0^{\circ}C$, 16$0^{\circ}C$. Four kinds of free sugars(sucrose, fructose, glucose, raffinose) and an unidentified sugar compound were separated in green tea by using High Performance LiQuid Chromatography (H.P.L.C.). 26-34 peaks were isolated as aroma compounds of green tea by means of Gas Liquid Chromatography(G.L.C). The typical aroma component of green tea such as linalool, furfural, benzyl alcohol and 13 other substances were identified. Contents of most compounds were decreased by heat treatment. Especially contents of free amino acids, free sugars, vitamin C and tannins were decreased remarkably, while those of total nitrogen and soluble nitrogen were hardly changed. The effect of heat treatment on organoleptic quality of tea extracts were examined by sensory evaluation of which result indicated the most favorable tea was produced at 115$^{\circ}C$. The Percentages of loss in contents of total sugars, reducing sugars, vitamin C, free amino acids and tannins at 115$^{\circ}C$ were 17%, 16%, 36%, 12% and 15% respectively, while those were 38%, 53%, 55%, 74% and 23% at 16$0^{\circ}C$.

• Journal of the Korean Wood Science and Technology
• /
• v.42 no.4
• /
• pp.407-419
• /
• 2014

The analysis of shape before and after heating, Surface moisture content, Moisture weight change and surface heat distribution by fixed type microwave heating in forms of flat veneer and veneer roll of Korean pine, pitch pine, larch and yellow poplar was conducted. The results were as follows: In case of flat veneer, the quality after microwave heating was comparatively good, but it was somewhat warped. These phenomena may be due to transformation by nonuniform drying stress and stronger effect of local irradiation on the veneers when heating veneer owing to the characteristics of fixed type microwave equipment. In case of the features of roll-shaped veneer heated by microwave, the quality after heating was comprehensively excellent. Especially there was no warping unlike flat veneer. Heat distribution and diffusion were also very stable for roll-shaped veneer and such heat distribution had much influence on surface moisture content and moisture weight loss. Accordingly, the veneer roll would show sufficient drying efficiency in fixed type microwave equipment through a scrutinized examination on generating power and irradiation time according to species and thickness of veneer.

• Korean Journal of Air-Conditioning and Refrigeration Engineering
• /
• v.27 no.4
• /
• pp.195-200
• /
• 2015

The thermal performance in the channels with two-wall rectangular convergent/divergent cross-sectional areas along the axial distance was investigated experimentally. The ribbed rectangular convergent/divergent channels were manufactured with a fixed rib height (e) = 10 mm and the ratio of rib spacing (p) to height (e) = 10. Three different parallel angled ribs (a = $30^{\circ}$, $45^{\circ}$, and $60^{\circ}$) were each placed on the channel's one sided wall only. The convergent channel of $D_{ho}/D_{hi}=0.67$ and the divergent channel of $D_{ho}/D_{hi}=1.49$ were considered. The ribbed divergent channel produced better thermal performance than the ribbed convergent channel in three different restrictions; identical flow rate, identical pumping power, and identical pressure loss.

• Proceedings of the Korean Institute of Building Construction Conference
• /
• 2015.11a
• /
• pp.166-167
• /
• 2015

Because of energy crisis at all around the world, there is many method and system which for improving energy efficiency has appeared in construction industry. And then, 20% of entire building energy loss is emissed to exterior of buildings, that is important to building's entire energy efficiency. So, many research has been conducted for imporve exterior energy efficiency and generally it called insulation of wall. Method for wall insulation can be classified interior system and exterior system which defined installation place of insulation board whether interior or exterior of structural wall. However, interior system has thermal problem such as thermal-bridge which can be necessarily occur condensation. and exterior system has constructional problem such as difficult to construction because exterior and finish work so expensive construction cost than other insulation method. Thus, sandwich insulation wall system has been appeared for solving these problems. Sandwich insulation system must using wall connecting things because both side walls is divided by center insulation. At this, Through the heat at wall connecter, it can be occured thermal-bridge and broken insulation board when under construction will be bring negative effect by reducing wall thickness and insulation deficit. At this study, we were compared previous sandwich insulation system and analysis these system's problem for develop the improving constructability and performance of sandwich insulation system.

• Journal of IKEEE
• /
• v.20 no.2
• /
• pp.171-173
• /
• 2016

In this study, we fabricate a high efficiency heater consisting of the indium tin oxide (ITO) nanoparticle (NP)-paste and polydimethylsiloxane (PDMS) and investigate the effect of PDMS on temperature maintenance of the heater through the comparison with the PDMS-free ITO film heater. Compared to the ITO film heater, the temperature of the PDMS/ITO film heater lasts 1.5 times longer. And the power consumption of the PDMS/ITO film heater is reduced by 35%, owing to the low thermal conductivity of the PDMS layer.