• Title/Summary/Keyword: Hardness variation

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Characteristics of 14K white gold by age-hardening treatment

  • Yun, Don-Gyu;Seo, Jin-Gyo;Sin, So-Ra;Park, Jong-Wan
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2012.05a
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    • pp.107.1-107.1
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    • 2012
  • Because of beautiful glossy and color, the value of gold leverage is very high in Europe. For improve the quality of white gold, we performed heat treatment on 14K white gold alloys at various age-hardening conditions. Age-hardening behavior and the related phase transformation changes were studied to elucidate the hardening mechanism of 14K white gold alloys. For solid solution treatment [ST], casted 14K white gold alloy specimens were treated at high temperature ($750^{\circ}C$) during 30 minute, and the specimens dropped to water for quenching immediately. For Age-hardening treatment [AT], the specimens were treated at various temperatures ($250^{\circ}C{\sim}300^{\circ}C$). After the heat treatment, we observed increased hardness from 144 Hv to 214 Hv by Vicker's hardness tester. Variation of the grain size measured by optical microscopy (OM) and scanning electron microscopy (SEM) images. By electron probe micro-analysis (EPMA) mapping analysis, we investigated that irregular particles were changed uniformly. After heat treatment, 14K white gold alloys showed improved hardness and became uniformity of grain size by age-hardening treatment.

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Effect of fluorine gas addition for improvement of surface wear property of DLC thin film deposited by using PECVD (PECVD를 이용한 DLC 박막의 표면 마모 특성 향상을 위한 플루오린 첨가의 영향)

  • Park, Hyun-Jun;Kim, Jun-Hyung;Moon, Kyoung-Il
    • Journal of the Korean institute of surface engineering
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    • v.54 no.6
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    • pp.357-364
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    • 2021
  • In this study, DLC films deposited by PECVD were evaluated to the properties of super-hydrophobic by CF4 treatment. The structure of DLC films were confirmed by Raman Spectra whether or not mixed sp3 (like diamond) peak and sp2 (like graphite) peak. And the hydrogen contents in the DLC films (F-DLC) were measured by RBS analysis. In addition, DLC films were analyzed by scratch test for adhesion, nano-indentation for hardness and tribo-meter of Ball-on-disc type for friction coefficient. In the result of analysis, DLC films had traditional structure regardless of variation of hardness at constant conditions. Also adhesion of DLC film was increased as higher material hardness. Otherwise, friction coefficient was increased as lower material hardness. The DLC films were treated by CF4 plasma treatment to enhance the properties of super-hydrophobic. And the DLC films were measured by ESEM(Enviromental Scanning Electron Microscope) for water condensation.

Effect of Laser Beam Diameter on the Microstructure and Hardness of 17-4 PH Stainless Steel Additively Manufactured by Direct Energy Deposition (레이저 빔 직경 변화에 따른 17-4 PH 스테인리스 강 DED 적층 조형체의 미세조직 및 경도 변화)

  • Kim, Woo Hyeok;Go, UiJun;Kim, Jeoung Han
    • Journal of Powder Materials
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    • v.29 no.4
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    • pp.314-319
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    • 2022
  • The effect of the laser beam diameter on the microstructure and hardness of 17-4 PH stainless steel manufactured via the directed energy deposition process is investigated. The pore size and area fraction are much lower using a laser beam diameter of 1.0 mm compared with those observed using a laser beam diameter of 1.8 mm. Additionally, using a relatively larger beam diameter results in pores in the form of incomplete melting. Martensite and retained austenite are observed under both conditions. A smaller width of the weld track and overlapping area are observed in the sample fabricated with a 1.0 mm beam diameter. This difference appears to be mainly caused by the energy density based on the variation in the beam diameter. The sample prepared with a beam diameter of 1.0 mm had a higher hardness near the substrate than that prepared with a 1.8 mm beam diameter, which may be influenced by the degree of melt mixing between the 17-4 PH metal powder and carbon steel substrate.

Variation of Hardness & Electrical conductivity for Cu-P and Cu-Cr Contact Tips During GMA Welding Process (GMA용접 중 Cu-P와 Cu-Cr계 콘택트팁의 경도와 전기전도도 변화)

  • 김가희;김희진;김남훈;유회수
    • Proceedings of the KWS Conference
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    • 2004.05a
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    • pp.191-193
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    • 2004
  • GMA(Gas Metal Arc)용접에서는 콘택트 팁이 토치 선단에 위치하여 용접 와이어를 송급하여 준다. 이러한 콘택트 팁의 주된 기능은 용접 전류를 와이어에 전송시켜주고, 와이어를 용접하고자 하는 위치로 유도하는 것이다. (중략)

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THE EFFECT OF FERMENTED FOODS ON THE COLOR AND HARDNESS CHANGE OF DENTURE BASE ACRYLIC RESINS (발효음식이 의치상레진의 색상 및 표면경도 변화에 미치는 영향)

  • Jeon, Yeol-Mae;Lim, Heon-Song;Shin, Soo-Yeon
    • The Journal of Korean Academy of Prosthodontics
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    • v.42 no.4
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    • pp.344-355
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    • 2004
  • Statement of problem: For a long time, many of denture base acrylic resins have been used for edentulous and partial edentulous patients because of easy manipulation and good mechanical properties, but its esthetic aspect has not been commented enough. Denture base acrylic resins also has caused esthetic problems due to discoloration or staining as in esthetic restoration. Many researches and reports have treated the problems and accomplished esthetic improvement. But these researches and reports dealt with general food colors or beverages, not with fermented foods. Purpose: This study is designed to assess what fermented foods, such as soy sauce, gochujang, and toenjang that many of Koreans have taken in, influence on the color and hardness variation of denture base acrylic resins. Materials and methods: For the procedure, twelve disks per 4 denture base acrylic resins were fabricated with a thickness of 2mm and 16mm in diameter. Each seven specimen were measured for discoloration with spectrophotometer, while the others, five specimen, for surface hardness change with Barcol hardness tester, over time. Each 12 specimen were immersed into the 4 beakers of fermented foods(soy sauces, gochujangs, toenjangs, deionized water), and $L^{*},a^{*}$, and $b^*$ values were measured for the color difference$({\Delta}E^*)$, on the 1st, 7th, and 28th day with spectrophotometer, with the measurement of surface hardness change. Each data observed was processed statistically. Results: The findings are as follows; Discoloration 1. All of denture base resins was not influenced by the kind of fermented foods, except for $QC20^{(R)}$ 2. Soy sauce and red pepper paste caused more change for denture base resins than deionized water and soy bean paste, except for Perform$^{(R)}$ 3. Most significant change was shown in Lucitone 199$^{(R)}$, whereas Perform$^{(R)}$ results in the least change for all immersed solution, with no statistical significance. Hardness change 1. Barcol hardness values in deposited specimens have been changed low degree, but with significant statistical change according to the kind of food and duration. 2. Lucitone$^{(R)}$ 199 as significantly lower Barcol hardness value than others do. Conclusion: Based on the above results, it suggests that the habitual intake of fermented foods is not helpful for the color stability of denture base acrylic resins because Soy sauce and red pepper paste mainly caused discoloration and surface hardness change. Particularly $Lucitone199^{(R)}$ shows specific discoloration and low surface hardness values. Therefore, it is recommended giving caution patients with denture of $Lucitone199^{(R)}$ especially against the habitual intake of fermented foods like soy sauce and red pepper paste.

Variations of Seed Hardness in Local Populations of Pisum sativum (완두(Pisum sativum)의 지역개체군 간 종자경실도 변이)

  • Kim, Chang-Ho
    • Journal of Life Science
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    • v.21 no.6
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    • pp.901-906
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    • 2011
  • In order to investigate the variations on the seed hardness of Pisum sativum distributed in southern area of Korean peninsula, 10 local strains (Choonseong. Ganghwa, Pocheon, Hadong, Haman, Geumneung, Yeongyang, Boseong, Gochang, Namweon), which located from $34^{\circ}26"N$ to $38^{\circ}11"N$, were selected according to their latitudes and geographical distances. The seeds of these strains were collected and their contents of mannose and galactose were analyzed. Mannose contents in the seeds were variable in the range between the highest 10.351 mg/g (Ganghwa) and the lowest 5.962 mg/g (Yeongyang). The contents of galactose were also represented remarkable differences from 7.050 mg/g (Yeongyang) to 19.314 mg/g (Hadong). The local strains were classified into 3 variation types such as the south central type (Namweon, Yeongyang, Geumneung, Gochang), the central type (Choonseong. Ganghwa, Pocheon) and the southern type (Haman, Hadong) and 1 strange strains (Boseong) according to the geographical climatic type, isopleth of warmth index and the ratio of mannose to galactose, which indicate the hardness of seeds in Leguminosae, ranged from 0.46 to 0.94. The variation types are very significant genecologically as an evidence for microevolution related to natual and artificial selection in cultivated plants.

Wear Characteristics of Automotive Disc Brakes: Effect of Gray Cast Iron Microstructures (자동차 브레이크용 디스크의 미세조직에 따른 편마모 특성에 관한 연구)

  • Lee, Jae-Young;Kim, Seong-Jin;Han, Chang-Joo;Jang, Ho
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2002.05a
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    • pp.235-239
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    • 2002
  • The objective of the experiment is to investigate the effect of microstructures of gray cast iron oil wear characteristics of automotive disc brakes. Six different gray cast iron rotors were manufactured by changing carbon equivalent and cooling rate. The change of DTV (disc thickness variation) before and after wear tests was measured to examine the wear properties according to the microstructures of gray iron discs since the DTV generation is caused by the circumferential uneven wear. Experimental results showed that the morphology of graphite flake and hardness in gray cast iron were crucially associated with the change of DTV. In particular, the DTV changes of rotor decrease when the length and area fraction of graphite flake in brake rotors increase and hardness of brake discs reduces.

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The Influence of Annealing Temperature on Mechanical Properties and Friction Coefficient of Coating Layer in Galvannealed Sheet Steel (용융아연도금강판에서 어닐링 온도변화에 따른 화합물화가 도금층 기계적 특성 및 마찰계수에 미치는 영향)

  • Jeon J.S.;Lee J. M.;;Kim D. J.;Kang Y.S.;Kim B. M.
    • Transactions of Materials Processing
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    • v.14 no.8 s.80
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    • pp.696-703
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    • 2005
  • In the modern days, a galvannealed sheet steel (GA) instead of a cold rolled steel sheet has been widely used as an alternative to extend the life of automotive body. Accordingly, the mechanical properties of GA for automobiles were taken into account and studied by examining their variation with annealing temperature. To clarify the effect of surface features on the mechanical and frictional properties of GA, the several tests such as nanoindentation, Vickers hardness and nano scratch test were executed. The frictional characteristics of coating layers of GA were examined through nano scratch test in this study. The friction coefficient of coating layers on the surface was obtained from the nano scratch. The variation of friction coefficient versus velocity and pressure was taken into consideration in this paper. Hardness and elastic modulus of coating layer were increased as increasing annealing temperature.

A Comparative Study on Tribological Characteristics between Ni-P Electroless Plating and TiAlN Coating on Anodized Aluminum Alloy (아노다이징된 알루미늄 합금에 대한 TiAlN 코팅, 무전해 Ni-P 도금의 트라이볼로지 특성 비교)

  • Lee, Gyu-Sun;Bae, Sung-Hoon;Lee, Young-Ze
    • Tribology and Lubricants
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    • v.26 no.1
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    • pp.68-72
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    • 2010
  • A ceramic coating is a surface treatment method that is being used widely in the industrial field, recently. Ni-P plating is also being used widely because of its corrosion resistance and low cost. An anodizing method is applicable to aluminum alloy. An anodizing method generates a thick oxide layer on the surface and then, that heightens hardness and protects the surface. These surface treatments are applied to various mechanical components and treated surfaces relatively move one another. In this study, tribological characteristics of Ni-P plating and TiAlN coating on anodized Al alloy are compared. The counterpart, anodized Al alloy, is worn out abrasively by Ni-P plating and TiAlN coating that have higher hardness. Abrasively worn debris accumulated on the surfaces of Ni-P plating and TiAlN coating, and then transferred layer is formed. This transferred layer affects the amplitude of variation of friction coefficient, which is related to noise and vibration. The amplitude of variation of friction coefficient of Ni-P plating is lower than those of TiAlN coating during the tests.