• Korean Journal of Soil Science and Fertilizer
• /
• v.50 no.5
• /
• pp.482-488
• /
• 2017

The measurement based on reliable standard operating procedures (SOPs) is important for consistent information. The objective of this study is to investigate reliable SOPs of soil physical methods, including core method for bulk density, Yamanaka hardness, and air permeameter method for air permeability. The coefficients of variation in bulk density (core method), Yamanaka hardness, and air permeability were ranged of 1~6%, 8~13%, and 10~84%, respectively. The variation in situ measurement such as bulk density, hardness, and air permeability due to spatial variability at measuring site was larger due to the number of replicates, organic matter content, and soil texture. Nevertheless, air permeability had different values as different number of replicates, and thus, it is thought that more replicates can result in higher reliability. It suggested that investigation of soil physical properties for the target sites should required to consider about soil texture, organic matter content, and number of replications before measurement. In conclusion, core sampling for bulk density measurement in upland soil recommended to perform in 3 repetitions with 2 inch core, and 3 inch core sampling for higher organic matter content.

• Journal of the Korean Society for Heat Treatment
• /
• v.11 no.1
• /
• pp.54-61
• /
• 1998

Since Cr-Mo-V steel has excellent fracture and creep properties at elevated temperature, they are extensively used as steam turbine components such as the turbine rotor. However, the turbine rotor steel used to suffer material degradation during long term service. Therefore, the assessment of the safety and residual life of the turbine rotor is periodically required during service. One of the most convenient techniques for that is the hardness method mainly due to its simplicity and nondestructive characteristics. In this research, six specimens with different aging times of turbine rotor steel were artificially prepared by an isothermal heat treatment at $630^{\circ}C$. The micro Vickers hardnesses of specimens were measured at room temperature. The relationships between the fracture properties and the hardness ratio were investigated. And also an indirect method to evaluate the residual life of degraded turbine rotor was proposed based on the micro Vickers hardness measurement.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.33 no.4
• /
• pp.346-352
• /
• 2009

In the present study, the Weibull statistical analysis using the Monte-Carlo simulation has been performed to investigate the micro-Vickers hardness measurement reliability considering the variability. Experimental indentation test were performed with a micro-Vickers hardness tester for as-received and quenching and tempering specimens in SCM440 steels. The distribution of micro-Vickers hardness is found to be 2-parameter Weibull distribution function. The mean values and coefficients of variation (COV) for both data set are compared with results based on Weibull statistical analysis. Finally, Monte-Carlo simulation was performed in order to evaluate the effect of sample size on the micro-Vickers hardness measurement reliability. For the parent distribution with shape parameter 30.0 and scale parameter 200.0 (COV=0.040), the number of sample data required to obtain the true Weibull parameters was founded by 20. For the parent distribution with shape parameter 10.0 and scale parameter 200.0 (COV=0.1240), the number of sample data required to obtain the true Weibull parameters was founded by 30.

• Transactions of Materials Processing
• /
• v.19 no.1
• /
• pp.25-31
• /
• 2010

To achieve desired microstructure and mechanical property of a manufacturing product, heat treatment process is applied as a secondary process after forging. Especially, quenching process is used for improving strength, hardness, and wear resistance since phase transformation occurs owing to rapid heat transfer from the surface of the specimen. In the present paper, a study on surface temperature measurement for water quenching of eutectoid steel was investigated. In order to determine the temperature history in experiments, three different measuring schemes were used by varying installation techniques of K-type thermocouples. Depending on the measured temperature distribution at the surface of the specimen, convective heat transfer coefficients were numerically determined as a function of temperature by the inverse finite element analysis considering the latent heat generation due to phase transformation. Based on the inversely determined convective heat transfer coefficient, temperature, phase, and hardness distributions in the specimen after water quenching were numerically predicted. By comparing the experimental and computational hardness distribution at three different locations in the specimen, the best temperature measuring scheme was determined. This work clearly demonstrates the effect of temperature measurement on the final mechanical property in terms of hardness distribution.

• Journal of the Korea Academia-Industrial cooperation Society
• /
• v.17 no.12
• /
• pp.98-106
• /
• 2016

Measurements of the elastic modulus and hardness using a nano indentation machine rely on the equation for the fitted contact area, which is valid for only sink-in materials. For most soft engineering materials that involve pile-up behavior rather than sink-in, the contact area equation underestimates the contact area and thus overestimates the elastic modulus and hardness. This study proposes a correction method to amend erroneous hardness measurements in pile-up situations. The method is a supplemental derivation to the original hardness measurement with the known value of the elastic modulus. The method was examined for soft engineering metals, Al 6061 T6 and C 12200, via tensile tests, nano indentation tests, impression observations, and finite element analysis. The proposed technique shows reasonable agreement with the analytical results accounting for strain gradient plasticity from a previous study.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 1998.03a
• /
• pp.168-174
• /
• 1998

In the present study, a method for measuring the relative density by the hardness measurement was proposed for sintered metal powder compacts. It is based on the indentation force equation, by which the relative density is related with the hardness, that was obtained by the finite element analysis of rigid-ball indentation on sintered metal powder compacts. For verifying the method, it was applied to prediction of density distributions in sintered and sintered-and-forged Fe-0.5%C-2%Cu powder compacts.

• Journal of the Korean Society for Heat Treatment
• /
• v.14 no.6
• /
• pp.336-344
• /
• 2001

For the establishment of the world wide unified scales of the Rockwell hardness test with conical indenters, round robin test was carried from 1998 to 2000. The pilot laboratory was MPA-NRW and 12 laboratories from 11 countries participated In this RRT. Rockwell hardness of 74 specially prepared blocks was measured for the scales of C, A, D, 45N, 30N, and 15N and the results were compared. It was found that the geometric form of indenter affects on the results very significantly and standardization in the measurement and evaluation of indenter should be established in short time for the reliable hardness measurement. KRISS showed good results in general for all of the ranges except 15N scale which showed relatively large difference compare to the mean value. It was concluded that poor control in loading velocity of the dash pot was the major reason.

• Journal of the Korean institute of surface engineering
• /
• v.53 no.2
• /
• pp.80-86
• /
• 2020

This paper is concerned with type of imperfections present within the anodic oxide films on AA2024 and surface hardness of the anodic film measured after ink-impregnation. The anodic oxide films were formed for 25 min at 40 mA/㎠ and 15±0.5℃ and 300 rpm of magnet stirring rate in 20% sulfuric acid solution. The ink-impregnation allows clear observations of not only the imperfections within the anodic oxide films but also an indentation mark on the oxide film surface made by a pyramidal-diamond penetrator for the hardness measurement. There were observed four different regions in the anodic oxide films on AA2024 and the surface hardness of the anodic oxide films appeared to be crucially dependent on the type of defects, showing 60~100 H_v on the oxide surface region I with large size black defect, 100~140 H_v on the oxide surface region II with large size grey defect, 140~170 H_v on the oxide surface region III with mall size black and/or grey defects and 170~190 H_v on the oxide surface region IV without defects. The pyramidal indentation marks were observed to be distorted in the regions with a large size black and grey defects, while no distortion of the indentation mark was observed in the regions with small size defects and without visible defects.

• Journal of the Korean Society of Manufacturing Technology Engineers
• /
• v.22 no.3
• /
• pp.394-401
• /
• 2013

A new Rockwell hardness (HRC) model using a volumetric parameter by a least square and fractal interpolation method is suggested. The results are also investigated in comparison to real measured hardness data. For this purpose, the measurement of an indented volume is performed using a confocal laser scanning microscope (CLSM), and the captured height encoded image (HEI) is used as an original surface for the calculation of the indented volume. After configuring the surface, the constructed volume is calculated and used as an independent variable for HRC hardness modeling. The hardness model is established using an experimental modeling technique involving a least square algorithm and fractal interpolating model, and this suggested model can be used to reliably predict the Rockwell hardness. These techniques can also be applied to the modeling of the Brinnell and Vickers hardnesses using a volumetric variable.

• Proceedings of the Korean Society of Precision Engineering Conference
• /
• 1996.11a
• /
• pp.933-937
• /
• 1996

In this paper, the behavior of plastic zone in the notch tip was studied under Loye's Micro Vickers Hardness Measurement Method. The direction forming maximum plastic zone was estimated by finite element analysis. In the experiments, cold rolling sheet SGCD3, SK5 and hot rolling sheet SS41, S4SC was used to study the influence of carbon contents on plastic zone. The standard hardness test specimen and the notch hardness test specimen was made and loaded cyclically. The specimen was aged to stabilize the hardness. After aging treatment, the notch specimen was made and simple tension load of 50% yield strength was applied. The hardness test at the notch tip until the hardness data of standard hardness specimen was checked was performed.