• Title/Summary/Keyword: HR Quality

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Determination of capsaicinoids in red pepper powder using ultra high performance liquid chromatography (초고속 액체크로마토그래피를 이용한 고춧가루의 capsaicinoids 분석)

  • Namgung, Bae;Lee, Yunyeol;Ha, Jaeho
    • Analytical Science and Technology
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    • v.26 no.4
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    • pp.256-261
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    • 2013
  • The efficiency of the two extractions (refluxing extraction and heating-block extraction) was compared to develop the simple analytical method for the determination of capsaicinoids, including capsaicin and dihydrocapsaicin in red pepper powder. For the method development, the parameters, including particle size, extraction time and sample size, were evaluated using ultra high performance liquid chromatography (u-HPLC). It was found that the most effective extraction time of the refluxing extraction was 3 hr. The higher extraction efficiency was obtained with the fine particle of a mild red pepper powder, while the particle size did not affect the extraction efficiency in case of the hot red pepper powder. The higher extraction efficiency was obtained with the small size of sample taken because of the ratio of the large extracting solvent to sample amount. The extraction efficiency of the refluxing method was 3-9% higher than that of the heating-block method, however, the heating-block method could be applied to the determination of capsaicinoids in the red pepper powder for the purpose of quality control of the product.

Performance Analysis of the KOMPSAT-1 Orbit Determination Using GPS Navigation Solutions (GPS 항행해를 이용한 아리랑 1호의 궤도결정 성능분석 연구)

  • Kim, Hae-Dong;Choi, Hae-Jin;Kim, Eun-Kyou
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.32 no.4
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    • pp.43-52
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    • 2004
  • In this paper, the performance of the KOMPSAT-1 orbit determination (OD) accuracy at the ground station was analyzed by using the flight data. The Bayesian least squares estimation was used for the orbit determination and the assessment of the orbit accuracy was evaluated based on orbit overlap comparisons. We also compared the result from OD using GPS navigation solutions with NORAD TLE and the result from OD using range data. Furthermore, the effect of observation type and OBT drift on the accuracy was investigated. As a consequence, It is shown that the OD accuracy using only GPS position data is on the order of 5m RMS (Root Mean Square) with 4 hrs arc overlap for the 30hr arc and the GPS velocity data is not proper as a observation for the OD due to its inferior quality. The significant deterioration of the accuracy due to the critical clock bias was not founded by means of the comparison of OD result from other observations.

Fabrication of YB$_{a2}Cu_3O_{7-{\delta}}/SrTiO_3/YB_{a2}Cu_3O_{7-{\delta}}$ multilayer structure for ground plane of single flux quantum digital circuit (단자속 양자 디지털 회로의 접지면을 위한 YB$_{a2}Cu_3O_{7-{\delta}}/SrTiO_3/YB_{a2}Cu_3O_{\7-{\delta}}$ 다층 구조의 제작)

  • Jang, Ju-Eok;Kim, Young-Hwan;Kim, Young-Hwan;Lee, Jong-Min;Park, Jong-Hyeog;Kang, Joon-Hee
    • 한국초전도학회:학술대회논문집
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    • v.9
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    • pp.71-74
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    • 1999
  • We have fabricated high-T$_c$ superconducting YBa$_2Cu_3O_{7-{\delta}}\;/SrTiO_3/\;YBa_2Cu_3O_{7-{\delta}}$ (YBCO/STO/YBCO) multilayer structure on (001) $SrTiO_3$ substrate by using pulsed laser deposition technique for applying to ground plane of single flux quantum digital circuits. In this structure, the top and bottom YBCO layers were connected through the holes in the STO insulating layer. The critical temperature of the two YBCO layers connected each other was 86 K after annealing at 500 $^{\circ}C$ in $O_2$ atm for about 60 hr. This result shows that the annealing process is very important fabricating YBCO/STO/YBCO multilayer structure An experiment to optimize the fabrication process of YSCO/ST0/YBCO multilayer structure with good quality is in progress.

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A Study on Coagulation and MF Membrane Process for the Reuse of Sewage Effluent (하수처리장 방류수의 응집 및 정밀여과 처리공정에 관한 연구)

  • Paik, Ke-Jin
    • Journal of environmental and Sanitary engineering
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    • v.20 no.3 s.57
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    • pp.36-43
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    • 2005
  • Prior to the study of the sewage treatment methods, water quality for Gwangju sewage of fluent was investigated from January to December, 2004 for sewage water reuse. Monthly mean values of BOD, SS, turbidity, total phosphorus and color were 4.1 mg/L, 2.9 mg/L, 0.8 NTU, 1.3 mg/L, and 27 unit, respectively. Jar-test was performed to investigate the removal efficiency of pollutants under the coagulation conditions of fast mixing for 5 min, slow mixing for 15 min and precipitation for 1hr. Here, alum and polyaluminium chloride (PAC) were used as coagulants to reduce color, turbidity, total phosphorus (TP) and total organic carbon (TOC) in sewage effluents. The results showed that PAC gave better efficiency in removing turbidity and dissolved phosphorus than alum. It was also found from the relative molecular weight (RMW) distribution analysis that organic matter over 1,000 Dalton (Da) was easily removed by coagulation and subsequently MF treatment, while it was not effective for less than 500 Da. Based on tis result, Natural organic matter (NOM) with lower molecular weight (< 500 Da) may cause harmful disinfectant by-product (DBP) after chlorine treatment. Thus, activated carbon adsorption seems to be required for the complete removal of DBP in the hybrid system.

Performance Evaluation of a Double Layer Biofilter System to Control Urban Road Runoff (I) - System Design - (이중층 토양 여과시설을 이용한 도로 강우 유출수 처리성능 평가 (I) - 시설 설계인자 결정을 중심으로 -)

  • Cho, Kang Woo;Kim, Tae Gyun;Lee, Byung Ha;Lee, Seul Bi;Song, Kyung Guen;Ahn, Kyu Hong
    • Journal of Korean Society of Water and Wastewater
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    • v.23 no.5
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    • pp.599-608
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    • 2009
  • This manuscript covers the results of field investigation and lab-scale experiments to design a double-layered biofilter system to control urban storm runoff. The biofilter system consisted of a coarse soil layer (CSL) for filtration and fine soil layer (FSL) for adsorption and biological degradation. The variations of flow rate and water quality of runoff from a local expressway were monitored for seven storm events. Laboratory column experiments were performed using seven kinds of soil and mulch to maximize pollutants removal. The site mean concentration (SMC) of storm runoff from the drainage area (runoff coefficient: 0.92) was measured to be 203 mg/L for SS, 307 mg/L for $TCOD_{Cr}$, 12.3 mg/L for TN, 7.3 mg/L for ${NH_4}^+-N$, and 0.79 mg/L for TP, respectively. This study employed a new design concept, to cover the maximum rainfall intensity with one month recurrence interval. Effective storms for last ten years (1998-2007) in seoul suggested the design rainfull intensity to be 8.8 mm/hr Single layer soil column showed the maximum removal rate of pollutants load when the uniformity coefficient of CSL was 1.58 and the silt/clay contents of FSL was virtually 7%. The removal efficiency during operation of double layer soil column was 98% for SS and turbidity, 75% for TCODCr, 56% for ${NH_4}^+-N$, 87% for TP, and 73-91% for heavy metals. The hydraulic conductivity of the soil column, 0.023 cm/sec, suggested that the surface area of the biofilter system should be about 1% of the drainage area to treat the rainfall intensity of one month recurrence interval.

The Effects of an Exercise Program on Physical Fitness, Cardiopulmonary Function and Life Satisfaction for Adult Women (운동프로그램이 성인여성의 체력, 심폐기능 및 생활만족도에 미치는 효과)

  • Chang, Chun-Ja;Yoo, Jae-Hee;Lee, Myung-Hee;Kim, Cha-Nam;In, Hee-Kyo;Lee, Kun-Ja
    • Research in Community and Public Health Nursing
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    • v.16 no.2
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    • pp.177-185
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    • 2005
  • Purpose: This study was to examine the effects of an exercise program on physical fitness, cardiopulmonary function and life satisfaction for adult women. Method: The exercise program combined dance and resistance training. The subject group consisted of 114 women aged between 33 and 60. Three 8-week sessions consisted of 55-80% HR max for 60-90 minutes a day and 3 times a week from March to November, 2004. Data were collected through pre- and post-exercise tests before and after each session. Data were collected with dynamometer, sphygmomamometer, spirometer and structured questionnaires. Data were analyzed employing descriptive statistics and paired t-test with SPSS/PC(10.0version) program. Results: There were significantly positive changes in muscle strength, flexibility, balance quality, forced vital capacity and life satisfaction, but no significantly positive changes in agility and blood pressure. Conclusion: This study showed that an exercise program has partially positive effects for adult women. The results of this study suggest that there should be programs of continuous exercise at community health centers for adult women's health.

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Growth and characterization of ZnIn$_2$S$_4$ single crystal thin film using Hot Wall Epitaxy method (Hot Wall Epitaxy (W)에 의한 ZnIn$_2$S$_4$ 단결정 박막 성장과 특성)

  • 윤석진;홍광준
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07a
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    • pp.266-272
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    • 2002
  • The stochiometric mixture of evaporating materials for the ZnIn$_2$S$_4$ single crystal thin film was prepared from horizontal furnace. To obtain the ZnIn$_2$S$_4$ single crystal thin film, ZnIn$_2$S$_4$ mixed crystal was deposited on throughly etched semi-insulating GaAs(100) in the Hot Wall Epitaxy(HWE) system. The source and substrate temperature were 610 $^{\circ}C$ and 450 $^{\circ}C$, respectively and the growth rate of the ZnIn$_2$S$_4$ single crystal thin film was about 0.5 $\mu\textrm{m}$/hr. The crystalline structure of ZnIn$_2$S$_4$ single crystal thin film was investigated by photo1uminescence and double crystal X-ray diffraction(DCXD) measurement. The carrier density and mobility of ZnIn$_2$S$_4$ single crystal thin film measured from Hall effect by van der Pauw method are 8.51${\times}$10$\^$17/ cm$\^$-3/, 291 $\textrm{cm}^2$/V$.$s at 293 $^{\circ}$K, respectively. From the photocurrent spectrum by illumination of perpendicular light on the c - axis of the ZnIn$_2$S$_4$ single crystal thin film, we have found that the values of spin orbit splitting ΔSo and the crystal field splitting ΔCr were 0.0148 eV and 0.1678 eV at 10 $^{\circ}$K, respectively. From the photoluminescence measurement of ZnIn$_2$S$_4$ single crystal thin film, we observed free excition (E$\_$X/) typically observed only in high quality crystal and neutral donor bound exciton (D$^{\circ}$,X) having very strong peak intensity. The full width at half maximum and binding energy of neutral donor bound excition were 9 meV and 26 meV, respectively. The activation energy of impurity measured by Haynes rule was 130 meV.

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A Study On Cause Analysis and Improvement About Malfunction of Proximity Sensor Exposed High Temperature (근접센서의 고온 고장발생에 관한 원인분석 및 개선 연구)

  • Park, Jin-Saeng
    • Transactions of the KSME C: Technology and Education
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    • v.3 no.3
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    • pp.175-181
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    • 2015
  • Because internal space of combat vehicle reachs about $80^{\circ}C$ at high temperature period, Proximity Sensor exposed high temperature and humidity, which has function to sense the distance and transfer signal for control unit, have enlarged sensing distance and finally locked on. Malfunction of sensing itself occur frequently, therefore we carried out cause analysis and improvement. We accomplish improvement activity secondly. Through-out many trial and error, we find out that malfunction of sensor occur at high temperature circumstance. To improve, the another Emitter Coil is added to increase voltage difference and improve sensing accuracy about 5~10 times. And we accomplish design improvement to dull temperature and humity change after increasing molding surface to add vibration and shock resistance. We prove that the improved product do not fail after enduring 136hr at $85^{\circ}C$ temperature and 85% relative humidity circumstance chamber.

Chemical Composition of Post-Harvest Biomass Burning Aerosols in Gwangju, Korea

  • Kim, Young-J.;Ryu, Seong-Y.;Kang, Gong-U.
    • Proceedings of the Korean Environmental Sciences Society Conference
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    • 2003.11a
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    • pp.79-84
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    • 2003
  • The main objective of this study was to investigate the chemical characteristics of post-harvest biomass burning aerosols from field burning of barley straw in late spring and rice straw in late fall in rural area in Korea. 12-hr integrated intensive sampling of $PM_{10}$ and $PM_{2.5}$ biomass burning aerosols had been conducted continuously at Gwangju, Korea 4-15 June 2001 and 8 October-14 November 2002. The fine and coarse particles of biomass burning aerosols were collected for mass, ionic, elemental, and carbonaceous species analysis. Average fine and coarse mass concentrations of biomass burning aerosols were measured to be 129.6, 24.2 ${{\mu}gm}^{-3}$ in June 2001 and 47.1, 33.2 ${{\mu}gm}^{-3}$ in October to November 2002, respectively. Exceptionally high level of $PM_{2.5}$ concentration up to 157.8 ${{\mu}gm}^{-3}$ well above 24-hour standard was observed during the biomass burning event days under stagnant atmosphere condition. During biomass burning periods dominant ionic species were $Cl^{-}$, ${NO_3}^{-}$, ${SO_4}^{2-}$, and ${NH_4}^{+}$ in fine and coarse mode. In the fine mode $Cl^{-}$ and ${KCl}^{+}$ were unusually rich due to the high content of the semiarid vegetation. High OC values and OC/EC ratios were also measured during the biomass burning periods. Increased amount of fine aerosols with high enrichment, which were originated from biomass burning of post-harvest agricultural waste, resulted in extremely severe particulate air pollution and visibility degradation in the region. Particulate matters from open field burning of agricultural wastes cause great adverse impact on local air quality and regional climate.

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The Effect of Organic Solvents on the Activity for the Synthesis of 12wt% Co-based FT Catalyst (12wt% Co 담지 FT 촉매 제조시 유기용매가 촉매활성에 미치는 영향연구)

  • LEE, JIYUN;HAN, JA-RYOUNG;CHUNG, JONGTAE;BAEK, YOUNGSOON
    • Transactions of the Korean hydrogen and new energy society
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    • v.26 no.4
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    • pp.339-346
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    • 2015
  • The synthesis of Fischer-Tropsch (FT) oil is the catalytic hydrogenation of CO to give a range of products, which can be used for the production of high-quality diesel fuel, gasoline and linear chemicals. This studied catalyst was prepared Cobalt-supported alumina and silica by the incipient wet impregnation of the nitrates of cobalt, promoter and organic solvent with supports. Cobalt catalysts were calcined at $350^{\circ}C$ before being loaded into the FT reactors. After the reduction of catalyst has been carried out under $450^{\circ}C$ for 24h, FT reaction of the catalyst has been carried out at GHSV of 4,000/hr under $200^{\circ}C$ and 20atm. From these experimental results, we have obtained the results as following; In case of $SiO_2$ catalysts, the activity of 12wt% $Cobalt-SiO_2$ synthesized by organic solvent was about 2 or 3 times higher than the activity of 12wt% $Cobalt-SiO_2$ catalyst synthesized without organic solvent. In particular, the activity of the $Cobalt-SiO_2$ catalyst prepared in the presence of an organic solvent P was two to three times higher than that of the $Cobalt-SiO_2$ catalyst prepared without the organic solvent. Effect of Cr and Cu metal as a promoter was found little. 200 h long-term activity test was performed with a $Co/SiO_2$ catalyst prepared in the presence of an organic solvent of Glyoxal solution.