• 제목/요약/키워드: Grinding characteristics

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한반도 중서부 청동기시대 유물의 융합과학적 연구: 서산 신송리유적 석기의 재질특성과 산지추정 (Interdisciplinary Study on Bronze Age Artifacts in Midwestern Korea: Material Characteristics and Provenance Presumption for Stone Artifacts of the Sinsongri Site in Seosan)

  • 이찬희;김란희;어언일
    • 보존과학회지
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    • 제30권2호
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    • pp.205-217
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    • 2014
  • 이 연구에서는 서산 신송리유적에서 출토된 청동기시대 석기를 대상으로 재질분석과 석재의 원산지를 검토하였다. 연구대상 석기는 점판암제 석재 1점, 석촉 반제품 2점, 갈판 1점 및 안산암질암 석촉 반제품 1점이다. 점판암은 유적지 일대에서 쉽게 관찰할 수 있는 암석이나, 안산암질암은 10km 이상 떨어진 부석면 간월도와 안면읍 황도리 등에서 산출된다. 석기 구성암석과 추정산지 암석에 대한 비교분석 결과, 점판암제 석기는 재질 및 암석광물학적 특징이 거의 동일하였으나, 안산암질암 석기는 추정산지 암석과 일부 다른 특징이 나타났다. 주원소, 미량원소, 호정 및 불호정원소에 대한 비교에서도 점판암제 석기와 추정산지 암석은 동일한 경향을 보였으나, 안산암질암 석기와 추정산지 암석은 다소 차이가 있다. 따라서 신송리유적에서 출토된 점판암제 석기는 유적 주변에 분포하는 암석을 원료로 제작한 자급형 석기로 해석된다. 그러나 안산암질암 석기는 외래형 석기로 추정되며, 광역적 조사를 비롯한 주변 유적에서 출토된 화산암제석기에 대한 연구를 병행하여 종합적 해석이 필요할 것으로 판단된다.

도석의 탈철에 관한 Oxalic acid의 영향에 관한 연구 (Effect of oxalic acid on the iron content of pottery stone)

  • 김경남;박현
    • 한국결정성장학회지
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    • 제14권6호
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    • pp.257-261
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    • 2004
  • 태백 도석은 주로 quartz와 함께 kaolinite가 포함되어 있다. 도석의 특성분석은 XRD, XRF, TG--DTA, SEM등을 이용하여 결정상과 화학성분 등을 분석하였다. 원석의 화학조성은 71.75wt%$SiO_2$, 22.10wt%$Al_2O_3$, 1.86wt%CaO, 2.97wt%$K_2O$, 0.62 wt%$Fe_2O_3$ 등이다. 3mm 크기의 도석을 $80^{\circ}C$의 10% 수산 농도에서 침출하면 탈철은 0.62wt%에서 0.24wt%로 감소하고 백색도가 증가하였다. 도석의 분쇄는 planetary ball mill을 이용하여 지르코니아 볼로 분쇄하였으며, 입도 크기는 25$\mu\textrm{m}$ 크기로 균일하게 분쇄되었다.

규조토 분진 측정 및 분석 방법의 비교에 관한 연구 (A Study on Evaluation for Sampling and Analytical Methods of Diatomaceous Earth Dust)

  • 임현술;김지용;정희경
    • 한국산업보건학회지
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    • 제5권2호
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    • pp.212-225
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    • 1995
  • This study was performed in a diatomite factory located at Pohang City, Kyeongsangbuk-Do. The major objectives were to evaluate sampling and analytical methods of diatomaceous earth dust. Concentrations of total and respirable diatomaceous earth dust were measured. Size distribution of dust was analyzed by a personal cascade impactor and the particle size analyzer which is an application of multiple diffraction method. Also crystalline silica in respirable and total dust samples was analyzed quantitatively by X-ray diffraction and Fourie Transform Infrared Spectroscopy(FTIR). The results were as follows: The airborne total and respirable dust concentrations, particle size distribution, and cristalline silica(quartz) concentrations showed approximately a log-normal distribution. The means of totaldust concentrations at flour maufacturing, fire brick grinding and packaging processes exceeded the Korean and American Conference of Governmental Industrial Hygienists standards, $10mg/m^3$. The size distribution of diatomaceous earth dust was log-normal and identified as the rspirable particle mass and thoracic particle mass. The crystalline silica in respirable and total dust samples was identified to quartz and contained about 10 % in those samples. Finally, it is necessary to study the applicability of multiple diffraction for particle size distribution to compare the ACGIH's size selective sampling with other materials containing crystalline silica. Also, advanced quantitative study to X-ray diffraction and FTIR methods shoud be carried out 10 verify general and specific characteristics for respirable crystalline silica.

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조선소 근로자의 직종과 혈청 암배아성 항원 농도와의 관련성 (A Relationship between Serum Carcinoembryonic Antigen Concentrations and Job Titles of a Shipyard Workers)

  • 정갑열;김정원;예병진
    • 한국산업보건학회지
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    • 제23권2호
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    • pp.41-49
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    • 2013
  • Objectives: The purpose of this study was to clarify the association between serum carcinoembryonic antigen (CEA) and type of work in the shipbuilding industry. Methods: 1,072 final study subjects were admitted to a general hospital from April through July 2010 for the purpose of medical examination. Data on general characteristics such as age, smoking history, alcohol history and exercise habits was gathered through structured self-administered questionnaires. Information on job factors was collected from a medical examination, by interview and through company personnel data. Serum CEA levels were measured after eight hours' fasting and were analyzed by a radioimmunoassay. Results: On univariate analysis, the mean serum CEA level was significantly higher among married (p=0.02), older age (p<0.01), longer work time (p<0.01), smokers (p<0.01), lower education (p<0.01), and indirect and direct exposure groups (p<0.01). On multiple regression analysis, serum CEA level was influenced by smoking (p=0.001), duration of work (p=0.019), and direct exposure group (p<0.001). However, among the direct exposure group, serum CEA level was not significantly different between welding, mounting, electro-device constructive work, grinding and cleaning, and painting. Conclusions: The goal of this research was to determine if there were differences between serum CEA levels according to occupational role among shipyard workers. The direct exposure group of shipyard workers had a relatively higher level of serum CEA than did the indirect exposure group and office workers, most likely due to occupational exposure.

곡면 FRP 패널 부재 연속시공을 위한 연결부 화학적 접합 특성에 관한 연구 (A study on chemical bonding characteristics of the interface between curved FRP panels for consecutive structural assembly)

  • 이규필;신휴성;정우태
    • 한국터널지하공간학회 논문집
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    • 제14권1호
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    • pp.79-91
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    • 2012
  • 곡면 FRP 패널 부재는 생산방식 및 생산설비 등의 제한으로 일정한 폭을 갖는 제품으로 생산되며, 이러한 곡면 FRP 부재를 이용하여 제작 공장 또는 현장에서 FRP 부재간 연결을 통한 연속 시공으로 목적대상 구조물을 시공할 수 있다. FRP 부재간 연결방법은 크게 화학적 연결, 기계적 연결, 그리고 복합적인 연결방법 등이 있으며, 이 가운데 접착용 수지를 이용한 화학적 연결이 가장 보편적으로 적용되고 있다. 따라서 FRP 부재의 연결부 최적화설계를 위하여 표면처리 조건 및 접착제 종류 등을 매개변수로 직접전단 시험을 수행하였다. 시험결과 sand paper를 이용한 연마 또는 sand blasting으로 FRP 부재 표면 처리 조건 및 에폭시 또는 아크릴계 접착제가 가장 효과적인 접합방식인 것으로 나타났다.

Lactobacillus acidophilus와 Saccharomyces cerevisiae를 이용한 남은 음식물의 생균 사료화에 대한 공기주입의 영향 (Effect of aeration for the probiotic feed production from food wastes by Lactobacillus acidophilus and Saccharomyces cerevisiae)

  • 이경석;이기영;오창석;이대규;김영준
    • 유기물자원화
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    • 제11권4호
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    • pp.114-119
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    • 2003
  • 본 연구는 남은 음식물의 사료화를 목적으로 Lactobacillus acidophilus와 Saccharomyces cerevisiae를 이용하여 남은 음식물을 발효시켜 고품질의 생균사료를 생산하기 위하여 실시하였다. 액상으로 충분히 마쇄시킨 남은 음식물 시료에 공기주입량을 0v.v.m 0rpm, 0.25v.v.m 100rpm, 0.5v.v.m 200rpm과 1v.v.m 500rpm으로 다르게 조절하여 $30^{\circ}C$에서 발효시킨 결과 0.5v.v.m 200rpm의 조건에서 생균수가 $4.5{\times}10^9CFU/m{\ell}$로 가장 높은 것으로 나타났다. 또한 공기주입량을 조절함으로써 최종 발효물의 pH를 조절할 수 있었고 사료로서의 기호성에 알맞고 보존성도 좋은 4-5의 pH범위를 얻을 수 있었다.

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n형 $Bi_2(Te,Se)_3$ 가압소결체의 열전특성 (Thermoelectric Properties of the n-type $Bi_2(Te,Se)_3$ Processed by Hot Pressing)

  • 박동현;노명래;김민영;오태성
    • 마이크로전자및패키징학회지
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    • 제17권2호
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    • pp.49-54
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    • 2010
  • n형 $Bi_2(Te,Se)_3$ 분말을 용해/분쇄법으로 제조하여 가압소결 후, 가압소결체의 열전특성을 $Bi_2(Te,Se)_3$ 잉곳과 비교하였으며, $Bi_2(Te,Se)_3$ 열전분말의 기계적 밀링처리가 가압소결체의 열전특성에 미치는 영향을 분석하였다. $Bi_2(Te,Se)_3$ 잉곳은 $24.2{\times}10^{-4}W/m-K^2$의 power factor를 나타내었으며, 이를 가압소결함으로써 power factor가 $27.3{\sim}32.3{\times}10^{-4}W/m-K^2$로 향상되었다. 기계적 밀링처리한 분말로 제조한 $Bi_2(Te,Se)_3$ 가압소결체는 $100^{\circ}C$에서 1.02의 무차원 성능지수를 나타내었으며, $130^{\circ}C$에서 외인성-내인성 천이거동을 나타내었다.

세퍼레이터 백필터 집진 미립자시멘트 (SBFC : Separator Bag Filter Cement)의 활용성 검토 (Investigation for Utilization of Separator Bag Filter Cement)

  • 김경민;박상준;유재강;이의배
    • 한국건설순환자원학회논문집
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    • 제5권3호
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    • pp.78-83
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    • 2010
  • 본 연구에서는 SBFC의 기본 성능을 분석하고, 페이스트 및 모르터에서의 공학적 특성을 검토하여, 향후 경제적인 조강콘크리트 개발을 위한 방안으로 활용하고자 하였다. 실험결과 SBFC의 우수한 조기강도 발현 성능을 확인 할 수 있었고, 유동성을 고려했을 때 OPC와 SBFC와의 적정 혼입율을 도출하여 사용하는 것이 바람직 할 것으로 판단된다.

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범용 위험도 평가서를 이용한 조선업체 작업에서의 누적외상성질환에 대한 인간공학적 분석 (An Application of a Baseline Checklist for Risk Assessment of Cumulative Trauma Disorders in Shipyard Workers)

  • 박동현;한상환
    • 한국산업보건학회지
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    • 제8권1호
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    • pp.24-35
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    • 1998
  • Cumulative trauma disorders(CTDs) have been a growing problems for US and European industries with higher incidence rate every year. The increase and their associated costs has led companies to form committes and implement programs to address this problem. In our country, we have just started to recognize and to work on the problems in industry. This study conducted an ergonomic analysis for typical jobs of ship building industry which was not usually surveyed for CTD problem. A baseline CTD checklist which was supposed to do a risk assessment was developed and applied in this study. Initially, we considered five major parts in the checklist which consisted of personal, frequency, posture, force, and miscellaneous information. Most jobs in ship building industry were much different from typical assembly work and VDT work that have been major part of the previous CTD studies. Specifically, job characteristics in terms of frequency and posture were quite different. There were relatively long cycle time, awkward postures for whole body (not just for upper extremities). Also, CTD risk scores based on checklist were a lot higher than the scores for VDT jobs which was a case of preceding application of the checklist. Specifically, grinding jobs turned out to be the most risky one in terms of CTDs. In conclusion, usual CTD prevention guidelines are not likely to he effective in this type of industry. An individual job based interventions are strongly suggested to have a good control of CTD problems in ship building industry.

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Effect of Sample Preparation on Prediction of Fermentation Quality of Maize Silages by Near Infrared Reflectance Spectroscopy

  • Park, H.S.;Lee, J.K.;Fike, J.H.;Kim, D.A.;Ko, M.S.;Ha, Jong Kyu
    • Asian-Australasian Journal of Animal Sciences
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    • 제18권5호
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    • pp.643-648
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    • 2005
  • Near infrared reflectance spectroscopy (NIRS) has become increasingly used as a rapid, accurate method of evaluating some chemical constituents in cereal grains and forages. If samples could be analyzed without drying and grinding, then sample preparation time and costs may be reduced. This study was conducted to develop robust NIRS equations to predict fermentation quality of corn (Zea mays) silage and to select acceptable sample preparation methods for prediction of fermentation products in corn silage by NIRS. Prior to analysis, samples (n = 112) were either oven-dried and ground (OD), frozen in liquid nitrogen and ground (LN) and intact fresh (IF). Samples were scanned from 400 to 2,500 nm with an NIRS 6,500 monochromator. The samples were divided into calibration and validation sets. The spectral data were regressed on a range of dry matter (DM), pH and short chain organic acids using modified multivariate partial least squares (MPLS) analysis that used first and second order derivatives. All chemical analyses were conducted with fresh samples. From these treatments, calibration equations were developed successfully for concentrations of all constituents except butyric acid. Prediction accuracy, represented by standard error of prediction (SEP) and $R^2_{v}$ (variance accounted for in validation set), was slightly better with the LN treatment ($R^2$ 0.75-0.90) than for OD ($R^2$ 0.43-0.81) or IF ($R^2$ 0.62-0.79) treatments. Fermentation characteristics could be successfully predicted by NIRS analysis either with dry or fresh silage. Although statistical results for the OD and IF treatments were the lower than those of LN treatment, intact fresh (IF) treatment may be acceptable when processing is costly or when possible component alterations are expected.