• Title/Summary/Keyword: Grain-oriented

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Anisortopy of the Silicon Nitride Prepared by Tape Casting

  • Park, Dong-Soo;Kim, Changd-Won;Park, Chan
    • The Korean Journal of Ceramics
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    • v.5 no.2
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    • pp.119-124
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    • 1999
  • Silicon nitride ceramics with highly oriented microstructure were prepared by tape casting a slurry containing 5 wt% of the silicon nitride whiskers. The whiskers were aligned in the casting direction and worked as seeds for the grain growth. The anisotropy was observed from the sintering shrinkage, Vickers indentation crack lengths, and XRD patterns. The cracks were much longer on the surface normal to the aligned grains than on the tape casting surface where the lateral cracks were also observed. The effect of sintering additives and the annealing treatment on the indentation crack length was examined. The sample with higher silica content had longer cracks than the one with lower silica content. The crack length anisotropy increased after annealing at 2123K.

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Microscopic Analysis of the Rock Cleavage for Jurassic Granite in Korea (주라기 화강암에 발달하는 결의 현미경학적 분석)

  • 박덕원;서용석;정교철;김영기
    • The Journal of Engineering Geology
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    • v.11 no.1
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    • pp.51-62
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    • 2001
  • Jurassic granites of three sites, Pocheon, Geochang and Habcheon, were analysed with respect to the characteristics of the rock cleavage. Microscopic analysis for the oriented thin sections of the specimens was conducted by using the scanline survey technique to measure microcrack direction, spacing and length. The results showed that the preferred orientations of microcrack developed in quartz and feldspar arc coincident with the orientation of quarry planes. The length of microcrack is related to grain size. The length of microcrack in coarse-grained granite is longer than that in relatively fine-grained granite. In all granites, microcracks related to the preferred orientations are well developed in order of rift, grain and hardway planes in number, length and density.

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Piezoelectric properties of (Bi0.5Na0.5)TiO3-BaTiO3 ceramics prepared by reactive templated grain growth method (Reactive Templated Grain Growth법에 의해 제조된 (Bi0.5Na0.5)TiO3-BaTiO3 세라믹스의 압전 특성)

  • Ahn, Byung-Guk
    • Journal of Sensor Science and Technology
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    • v.16 no.3
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    • pp.234-239
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    • 2007
  • Crystallographically {h00}-oriented $0.94(Bi_{0.5}Na_{0.5})TiO_{3}-0.06BaTiO_{3}$ (0.94BNT-0.06BT) ceramics was prepared by the Reactive Templated Grain Growth (RTGG) method using the $Bi_{4}Ti_{3}O_{12}$ template. The sheets prepared by tape-casting of slurries containing the templates and starting materials are cut, laminated, and pressed. Then burn-out and sintering was conducted. Also, to compare with the 0.94BNT-0.06BT ceramics prepared by the RTGG method another 0.94BNT-0.06BT ceramics was prepared by the solid-state method. In the optimum of this experiments range, the degree of orientation of the 0.94BNT-0.06BT ceramics prepared by the RTGG method was texture fraction${\approx}92%$ and the piezoelectric constant($d_{33}$) and coupling factor($k_{p}$) was obtained to $d_{33}{\approx}205{\;}pC/N$, $k_{p}{\approx}0.33%$, respectively.

Rapidly Solidified Fe-6.5wt% Si Alloy Powders for High Frequency Use

  • Park, Seung-Dueg;Yang, Choong-Jin
    • Journal of Magnetics
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    • v.2 no.1
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    • pp.12-15
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    • 1997
  • Fe-(3∼6.5wt%) Si alloy powders having a high magnetic induction(Bs) and a low core loss value for high frequency use were obtained by an extractive melt spinning as well as a centrifugal atomization technique. Sintered core rings made by the rapidly solidified Fe-6.5wt% Si powders exhibited the high frequency magnetic properties : megnetic induction(B8) of 1.23 T, coercivity(Hc) of 0.12 Oe, relative permeability(${\mu}$a) of 6321, and core loss(W10/50) of 1.27 W/kg from the rings of 1.1 mm thick. The magnetic induction values were found to be almost identical to those of non-oriented Fe-6.5wt% Si steel sheet and double the value of 6.5wt% Si sheet prepared by the CVD technique. The high frequency core losses(W) up to 10 kHz(W10/10k) were measured to be competitive to those of grain-oriented Fe-6.5wt% Si steel sheet.

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Controlling Preferred Orientation of ITO Thin Films by RF-Magnetron Sputtering Method

  • Park, Ju-O;Kim, Jae-Hyung;Lee, Joon-Hyung;Kim, Jeong-Joo;Cho, Sang-Hee
    • 한국정보디스플레이학회:학술대회논문집
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    • 2003.07a
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    • pp.818-821
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    • 2003
  • Sn-doped $In_{2}O_{3}$ (ITO) thin film is one of the materials widely on research not only in the academic fields but also in industrial fields because of their transparency, high conductivity and good adhesion characteristics on substrate. ITO thin films are usually preferred oriented to one of the (222), (400), and (440) planes during crystallization process, which is dependent on processing variables. The preferred orientation affects electrical, optical and etching properties of the films. In this study, thin films of preferred oriented in different orientation were fabricated by controlling processing variables. The crystallization behavior, grain size, surface roughness, transparency and electrical properties of the thin films in different orientation were examined.

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Effects of Oxides Added in the Base of Low Voltage ZnO Varistors (저전압용 ZnO 바리스터의 기본조성에 첨가된 산화물의 영향)

  • 진희창;마재평;박수현
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.26 no.8
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    • pp.1211-1216
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    • 1989
  • To enhance the breakdown properties of low voltage-oriented ZnO varistor, sample were fabricated with additive oxides and sintering conditions. Addition of TiO2 lowered breakdown voltage` nonlinear resistances were lowered about 10V/mm and nonlinear exponents were not lowered with respect to it with the basic composition. To the samples added TiO2, V2ko5, and Cr2O3, microstructures were observed by SEM, moreover Ti was detected at grainboundaries and within the grain by EDS. Addition of Si-oxides and Sb2O3 increased nonlinear exponent and also increased nonlinear resistance, by addition of TiO2 to these samples at the sintering conditions of 1250\ulcorner and 1 hour we could fabricate low voltage-oriented ZnO varistors with nonlinear exponent of 30 or more and with real breakdown voltage of 30V/mm.

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Measurement of Two Dimensional Magnetic Properties of Electrical Steel Sheets under Rotating Magnetic Fields (전기강판의 회전자계 하에서의 2차원 자계특성 측정)

  • Eum, Young-Hwan;Hong, Sun-Ki;Shin, Pan-Seok;Koh, Chang-Seop
    • The Transactions of the Korean Institute of Electrical Engineers B
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    • v.55 no.12
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    • pp.617-622
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    • 2006
  • It is necessary to measure precisely the magnetic characteristics of electrical steel sheets under rotating magnetic fields, to obtain an accurate numerical performance analysis of electric machines made of electrical steel sheets. In this paper, the two dimensional magnetic characteristics of an electrical steel sheet are measured and explained under rotating magnetic fields using a two-axes-excitation type single sheet tester (SST). Through experiments, the magnetic properties, under rotating magnetic fields, of a non-oriented and grain oriented electrical steel sheet were measured respectively. In addition, the iron losses due to not only the alternating magnetic fields, but also rotating magnetic fields were measured. These experimentally measured results can evidently be applied to the analysis of iron losses in electrical machines.

Physical correlation between annealing process and crystal structure and magneto-resistance of Bismuth thin films (열처리 공정과 비스무스 박막의 결정구조 및 자기저항 특성변화와의 물리적 관계)

  • Jang, Seok Woo;Seo, Young-Ho;An, Ho-Myoung
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.18 no.3
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    • pp.638-642
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    • 2014
  • In this study, we investigate on the crystal microstructure and magneto-resistance (MR) change of Bismuth(Bi) thin films for annealing process, in order to apply Bi thin films to the spin electronic devices. As-prepared Bi thin films show the randomly oriented find grains whose size was measured to about 100 nm and the very low MR (4.7 % at room temperature) while careful annealing results in not only grain growth up to ${\sim}2{\mu}m$ but also drastic MR improvement (404 % at room temperature). The drastic change in the MR after applying the annealing process is attributed to the grain growth decreasing grain boundary scattering of electron. Therefore, in this study, we confirm the annealing effect for the grain boundary formation and MR improvement of Bi thin films, and demonstrate the feasibility of spin electronic devices.

High Temperature Grain Growth Behavior of Aerosol Deposited BaTiO3 Film on (100), (110) Oriented SrTiO3 Single Crystal (상온분사분말공정에 의해 SrTiO3 (100), (110) Seed에 코팅된 BaTiO3의 고온 성장 거동 분석)

  • Lim, Ji-Ho;Lee, Seung Hee;Kim, Ki Hyun;Ji, Sung-Yub;Jung, Suengwoon;Park, Chun-kil;Jung, Han-Bo;Jeong, Dae-Yong
    • Korean Journal of Materials Research
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    • v.29 no.11
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    • pp.684-689
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    • 2019
  • Single crystals, which have complexed composition, are fabricated by solid state grain growth. However, it is hard to achieve stable properties in a single crystal due to trapped pores. Aerosol deposition (AD) is suitable for fabrication of single crystals with stable properties because this process can make a high density coating layer. Because of their unique features (nano sized grains, stress inner site), it is hard to fabricate single crystals, and so studies of grain growth behavior of AD film are essential. In this study, a $BaTiO_3$ coating layer with ${\sim}9{\mu}m$ thickness is fabricated using an aerosol deposition method on (100) and (110) cut $SrTiO_3$ single crystal substrates, which are adopted as seeds for grain growth. Each specimen is heat-treated at various conditions (900, 1,100, and $1,300^{\circ}C$ for 5 h). $BaTiO_3$ layer shows different growth behavior and X-ray diffraction depending on cutting direction of $SrTiO_3$ seed. Rectangular pillars at $SrTiO_3$ (100) and laminating thin plates at $SrTiO_3$ (110), respectively, are observed.

Orientation Control of $SrBi_2Ta_2O_9$ Thin Films on Pt (111) Substrates

  • Lee, Si-Hyung;Lee, Jeon-Kook;Choelhwyi Bae;Jung, Hyung-Jin;Yoon, Ki-Hyun
    • The Korean Journal of Ceramics
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    • v.6 no.2
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    • pp.116-119
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    • 2000
  • The a-axis and c-axis prefer oriented SBT thin films could be deposited on Pt(111)/Ti/$SiO_2$$650^{\circ}C$). The c-axis preferred orientation of SBT film can be obtained by Sr deficiency and high compressive stress. However, the a-axis-oriented grains can be formed under stoichiometric Sr content and nearly stress-free state.

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