• 한국분말야금학회:학술대회논문집
• /
• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
• /
• pp.788-789
• /
• 2006

Microstructure and soft magnetic properties of bulk amorphous and/or nanocrystalline $Fe_{73.5}Cu_1Nb_3Si_{13.5}B_9$ alloys prepared by consolidation at 5.5GPa were investigated. The relative density of the bulk sample 1 (from amorphous powders) was 98.5% and the grain sizes were about 10.6nm. While the relative density and grain sizes of bulk sample 2 (from nanocrystalline powders) are 98% and 20.1nm, respectively. Particularly, the bulk samples exhibited a good combined magnetic property: for Sample1, $M_s=125emu/g$ and $H_c=1.5Oe;$ for Sample2, $M_s=129emu/g$ and $H_c=3.3Oe$. The success of synthesizing the nanocrystalline Fe-based bulk alloys will be encouraging for the future development of bulk nanocrystalline soft magnetic alloys.

• 대한용접접합학회:학술대회논문집
• /
• 대한용접접합학회 2001년도 추계학술발표대회 개요집
• /
• pp.220-222
• /
• 2001

The average grain size, the grain-size distribution, the morphology and the microstructure are fundamental characteristics of a spraying powder. Now that the significance of the grain size for the pattern of properties of the powder has been recognised, greater consideration is also being given to it in standards and regulations. However, unfortunately, the processes according to which the grain size and the grain-size distribution must be determined are specified in the rarest of cases. The contribution therefore dealt with the comparison of different particle-size measuring techniques, such as diffraction spectroscopy, sedimentation, sieving and microscopic measurement. The comparability of the measured results was investigated on twelve plasma spraying powders with different compositions, nominal sizes and morphologies.

• 한국재료학회지
• /
• 제14권12호
• /
• pp.829-834
• /
• 2004

Annealing of $Cu(B)/Ti/SiO_2$ in vacuum has been carried out to investigate the effects of Ti underlayer on microstructure in $Cu(B)/Ti/SiO_2$ structures. For comparison, $Cu(B)/Ti/SiO_2$ structures was also annealed in vacuum. Three different temperature dependence of Cu growth can be seen in $Cu(B)/Ti/SiO_2$; B precipitates- pinned grain growth, abnormal grain growth, normal grain growth. The Ti underlayer having a strong affinity for B atoms reacts with the out-diffused B to the Ti surface and forms titanium boride at the Cu-Ti interface. The formation of titanium boride acts as a sink for the out-diffusion of B atoms. The depletion of boron in grain boundaries of Cu films, as results of the rapid diffusion of B along the grain boundaries and the insufficient segregation of B to the grain boundaries, induces grain boundaries to migrate and causes the abnormal grain growth. The increased bulk diffusion coefficient of B within Cu grains can be responsible for the normal grain growth occurring in the annealed $Cu(B)/Ti/SiO_2\;at\;600^{\circ}C$. In contrast, the $Cu/SiO_2$ structures show only the abnormal growth of grains and their sizes increasing as the temperature increases above $400^{\circ}C$.

• Journal of Advanced Marine Engineering and Technology
• /
• 제38권6호
• /
• pp.761-770
• /
• 2014

경기만 남부 지역에 발달되어 있는 수중사구의 형태 특성 및 변화를 알아보고 수중사구의 발달 제어요인을 파악하기 위해서 2004년 9월과 2006년 9월에 고해상도 다중빔음향측심기를 이용한 지형조사와 퇴적학적 조사를 실시하였다. 연구지역은 현재의 조류세기와 퇴적물 특성이 대형 수중사구가 충분히 발달, 유지될 수 있는 조건을 나타내고 있다. 시간에 따른 퇴적물 특성 변화, 즉, 입도의 감소는 초대형 수중사구의 파고를 감소시키고 있어, 입도가 연구지역 내 수중사구 크기 발달에 영향을 미치는 주요 요인임을 나타낸다.

• Journal of Welding and Joining
• /
• 제31권6호
• /
• pp.44-49
• /
• 2013

The influence of thermo-mechanical cycling on the microstructure and strength in the weld coarse-grained heat affected zone (CGHAZ) of Ti-Nb added low carbon HSLA steel was explored through Vickers hardness tests, nanoindentation experiments, scanning electron microscopy (SEM) and transmission electron microscopy (TEM) analysis. Undeformed and deformed CGHAZs were simulated using Gleeble simulator with different heat inputs of 30kJ/cm and 300kJ/cm. At high heat input of 300kJ/cm, the CGHAZ consisted of ferrite and pearlite and then their grain sizes were not affected by deformation. At low heat input of 30kJ/cm, the CGHAZ consisted of lath martensite and then the sizes of prior austenite grain, packet and lath width decreased with deformation. In addition, the fraction of particle increased with deformation and this is because the precipitation kinetics was accelerated by deformation. Meanwhile, the Vickers and nanoindentation hardness of deformed CGHAZ with 30kJ/cm heat input were higher than those of undeformed CGHAZ, which are due to the effect of grain refinement and precipitation strengthening.

• 한국원자력학회:학술대회논문집
• /
• 한국원자력학회 2002년도 추계학술발표회요약집
• /
• pp.290.2-290
• /
• 2002

• 한국수자원학회논문집
• /
• 제37권5호
• /
• pp.387-395
• /
• 2004

본 논문에서는 하상변동 및 유사입자의 시간적 공간적 분포를 동시에 모의할 수 있는 2차원 수치모형을 제시하였다. 사행수로의 하상변동은 만곡부의 외측에서는 하상이 세굴되고 훨씬 더 거친 입경의 재료로 구성되며, 만곡부의 내측에서는 하상이 상승하고, 세립토로 구성되었다. 또한 사행하천에서 흐름의 방향에 대한 입자분포 과정은 상류의 변곡점에서 시작하여, 하류 변곡점에서 마치게 되는 것을 보여주었다. 하천의 경계가 불규칙하고 복잡한 하천에서는 혼합사호 형성된 하천에서보다 균일사로 이루어진 하천에서 하상이 깊게 세굴되는 현상을 보여준다. 혼합사로 이루어진 하천에서의 공간적 입도 분포는 사행하천에서와 마찬가지로 하상이 퇴적되는 사행의 내측에서는 세립토로 구성되고 하상이 세굴되는 외측에서는 굵은 입자로 구성되는 것을 보여주었으며, 하천 폭이 좁은 부분에서는 하상의 세출 및 하상재료가 굵게 변화되는 것을 보여주었다.

• 한국전기전자재료학회:학술대회논문집
• /
• 한국전기전자재료학회 2001년도 하계학술대회 논문집
• /
• pp.170-173
• /
• 2001

Thin films of phase-pure perovskite (P $b_{0.72}$L $a_{0.28}$) $Ti_{0.93}$ $O_3$(PLT) were deposited in-situ onto Pt/Ti/ $SiO_2$/Si substrates by pulsed laser deposition. We have systematically investigated the variation of grain sizes depending on the process condition. Both in-situ annealing and ex-situ annealing treatments have been compared depending on the annealing time. Two-step process to grow (P $b_{0.72}$L $a_{0.28}$) $Ti_{0.93}$ $O_3$(PLT) films was adopted and verified to be useful to enlarge the grain size of the film and to enhance the leakage current characteristics. The grain sizes of PLT thin films were successfully controlled 260 to 350 nm by changing process parameters. Electrical properties including dielectric constant, ferroelectric characteristics, crystallization and leakage current of PLT thin films were shown to be strongly inf1uenced by grain size. Also PLT thin films on p-type(100) Si substrate will be fabricated by pulsed laser deposition technique using a Nd:YAG laser with different wavelengths of 355, 532 and 1064 nm. Effect of the variation of laser wavelength on dielectric properties will be discussed. Microstructural and electrical properties of the film were investigated by C-V measurement leakage current measurement and SEM.ent and SEM.

• KIEAE Journal
• /
• 제7권5호
• /
• pp.135-142
• /
• 2007

This is an experimental study on the structural characteristics of reinforced concrete beams using of the oyster shells as a substitute fine aggregate of concrete. In this study, the main factors consist of the grain sizes and the percentage of substitution of oyster shells to fine aggregate in the equal water cement ratio. The results of the study showed as followed. The initial load value of them represented similar constant within 10% of the maximum load value in each test beam. But the maximum load value and the ultimate load value decreased with increased grain size and the rate of substitution. As the grain size of oyster shells became smaller, the load values of them were somewhat higher. The deflection among deformation properties of reinforced concrete beams with oyster shells represented typical curves like that of normal reinforced concrete. In the deformation of steel and concrete, the deformation was proportionated to the load till yield point and from yield point until approaching the ultimate load point. One type was typical curve of the load and the deformation and the other type irregularly was changed to very small deformation for the load increase centering around load axis. After the analyzing structural behaviors and the properties of reinforced concrete test beams with oyster shells, the most excellent grain size of oyster shells represented 1.0mm and less or 5.0mm and less with taking uniformly, and the percentage of practicable substitution of them to fine aggregate was about 30%.

• 한국재료학회지
• /
• 제26권6호
• /
• pp.325-331
• /
• 2016

This paper presents a study of the tensile properties of austenitic high-manganese steel specimens with different grain sizes. Although the stacking fault energy, calculated using a modified thermodynamic model, slightly decreased with increasing grain size, it was found to vary in a range of $23.4mJ/m^2$ to $27.1mJ/m^2$. Room-temperature tensile test results indicated that the yield and tensile strengths increased; the ductility also improved as the grain size decreased. The increase in the yield and tensile strengths was primarily attributed to the occurrence of mechanical twinning, as well as to the grain refinement effect. On the other hand, the improvement of the ductility is because the formation of deformation-induced martensite is suppressed in the high-manganese steel specimen with small grain size during tensile testing. The deformation-induced martensite transformation resulting from the increased grain size can be explained by the decrease in stacking fault energy or in shear stress required to generate deformation-induced martensite transformation.